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EEXXPPEERRTT DDEESSIIGGNN 
BByy:: NNoooosshhiinn NNoosshhiirrvvaannii
a Analysis of volatile arroommaa ccoommppoouunnddss ooff ffrreesshh 
cchhiillllii ((CCaappssiiccuumm aannnnuuuumm)) dduurriinngg ssttaaggeess ooff 
mmaattuurriittyy uussiinngg ssoolliidd pphhaassee mmiiccrrooeexxttrraaccttiioonn 
((SSPPMMEE))
Software for Design of 
Experiments 
 Design Expert is a piece of software designed to 
help with the design and interpretation of 
multi-factor experiments
 Optimization of SPME extraction of 
selected aroma compounds was done 
using a central composite design (CCD) 
 consisting of a 22 factorial design with 
 resulting in 13 treatments
 For the optimization method, CCD is one 
of the most useful design for estimating a 
multifactor response surface which keeps 
to a minimum number of experiments 
 And allows the simultaneous variation of 
all the experimented factors studied and 
the distinguishing of interaction among 
them
Experimental design showing 
coded and uncoded variables
The evaporation of the volatile compounds can 
be adequately represented by the model 
equations as shown in Table
Results from response surface 
methodology (RSM) showed that heating 
at 60ºC for 30 min gave the optimum 
parameter, as indicated by the high 
desirability
 This study, therefore, tried developing a 
mathematical model capable of predicting the 
aw at fixed temperature (25º C ) of some foods, 
from easily measured, pertinent 
physicochemical food properties, namely pH 
and Brix values. 
 The study established a predictive model in 
simulated food solutions (SFS), which 
contained varying levels of water, sucrose and 
acid. 
 The predictive performance of the established 
model was assessed through validations using
 The SFS were formulated based on the 
data supplied to and processed using the 
Design Expert Version 7.0.3 software 
package 
 A Central Composite Rotatable Design 
(CCRD) was applied, to determine the 
appropriate combinations of various levels 
of pH and Brix
Response surface plot showing the 
influences of pH and Brix on aw
Optimization ooff tthhee bbaassiicc ffoorrmmuullaattiioonn ooff aa 
ttrraaddiittiioonnaall bbaakkeedd ccaassssaavvaa ccaakkee uussiinngg rreessppoonnssee 
ssuurrffaaccee mmeetthhooddoollooggyy
 Effects of amount of ingredients such as 
sugar (10–30%) and coconut milk (15– 
35%) on the textural characteristics 
(hardness and chewiness) and sensory 
qualities (colour, firmness, cassava flavour 
and overall acceptability) of cakes were 
investigated.
 The three coded levels of sugar: 
 -1 (10%), 
 0 (20%), 
 1(30%) 
 coconut milk: 
 -1 (15%), 
 0 (25%), 
 1(35%)
Central composite design arrangement and 
experimental result for the response 
variables
 Optimum formulation of baked cassava cake 
was 25% of sugar and 20% of coconut milk.
Expert design in food

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Expert design in food

  • 1. EEXXPPEERRTT DDEESSIIGGNN BByy:: NNoooosshhiinn NNoosshhiirrvvaannii
  • 2. a Analysis of volatile arroommaa ccoommppoouunnddss ooff ffrreesshh cchhiillllii ((CCaappssiiccuumm aannnnuuuumm)) dduurriinngg ssttaaggeess ooff mmaattuurriittyy uussiinngg ssoolliidd pphhaassee mmiiccrrooeexxttrraaccttiioonn ((SSPPMMEE))
  • 3. Software for Design of Experiments  Design Expert is a piece of software designed to help with the design and interpretation of multi-factor experiments
  • 4.  Optimization of SPME extraction of selected aroma compounds was done using a central composite design (CCD)  consisting of a 22 factorial design with  resulting in 13 treatments
  • 5.  For the optimization method, CCD is one of the most useful design for estimating a multifactor response surface which keeps to a minimum number of experiments  And allows the simultaneous variation of all the experimented factors studied and the distinguishing of interaction among them
  • 6. Experimental design showing coded and uncoded variables
  • 7. The evaporation of the volatile compounds can be adequately represented by the model equations as shown in Table
  • 8. Results from response surface methodology (RSM) showed that heating at 60ºC for 30 min gave the optimum parameter, as indicated by the high desirability
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  • 12.  This study, therefore, tried developing a mathematical model capable of predicting the aw at fixed temperature (25º C ) of some foods, from easily measured, pertinent physicochemical food properties, namely pH and Brix values.  The study established a predictive model in simulated food solutions (SFS), which contained varying levels of water, sucrose and acid.  The predictive performance of the established model was assessed through validations using
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  • 14.  The SFS were formulated based on the data supplied to and processed using the Design Expert Version 7.0.3 software package  A Central Composite Rotatable Design (CCRD) was applied, to determine the appropriate combinations of various levels of pH and Brix
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  • 20. Response surface plot showing the influences of pH and Brix on aw
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  • 25. Optimization ooff tthhee bbaassiicc ffoorrmmuullaattiioonn ooff aa ttrraaddiittiioonnaall bbaakkeedd ccaassssaavvaa ccaakkee uussiinngg rreessppoonnssee ssuurrffaaccee mmeetthhooddoollooggyy
  • 26.  Effects of amount of ingredients such as sugar (10–30%) and coconut milk (15– 35%) on the textural characteristics (hardness and chewiness) and sensory qualities (colour, firmness, cassava flavour and overall acceptability) of cakes were investigated.
  • 27.  The three coded levels of sugar:  -1 (10%),  0 (20%),  1(30%)  coconut milk:  -1 (15%),  0 (25%),  1(35%)
  • 28. Central composite design arrangement and experimental result for the response variables
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  • 38.  Optimum formulation of baked cassava cake was 25% of sugar and 20% of coconut milk.