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Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
1
STRAIN RATE AND TEMPERATURE EFFECTS
ON THE FLOW STRESS OF ADI
A. Ruggieroa, G. Iannittib, E. Veneric, F. Vettorec , N. Bonoraa
a University of Cassino and SL, DICeM, Cassino, Italy
b TECHDYN Engineering, I-00199 Rome, Italy
cZanardi Fonderie S.p.A, I-37046 Minerbe (VR), Italy
BACKGROUND
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
2
• Cast irons are widely used in industrial practice mainly
for the production of components through the
process of casting
• ADI matrix microstructure: ausferrite
• Excellent property combinations of strength, ductility,
and toughness
• Valid substitute for steel for structural applications
References
[1] Böhme* and Reissig, Adv. Eng. Mat. 2015, 17, No. 8
[2] Keough and Hayrynen, SAE, 2000, paper no 248871
BACKGROUND
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
3
• Designers show lack of confidence
• Dread of a presumed low ductility
under impulsive loading
• Charpy impact test results
AIM OF THE WORK
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
4
• To investigate the constitutive response of the ADI 1050-6
under different conditions of strain rate and temperature
• To analyze the strain rate effect on the ductility
• To develop a constitutive model for the design of components
operating under both static and dynamic conditions
MATERIALS
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
5
DESIGNATION
UTS
(MPa)
YIELD
STRESS
(MPa)
ELONGATION
%
HARDNE
SS
(BR)
ADI 1050 1050 700 6 320-380
ADI 1200 1200 850 3 340-420
HSiADI 1450 1040 8.9 400
42CrMo4 1200 800 11 -
[3]
References
[3] J. R. Keough, K. L. Hayrynen and G. L. Pioszak, AFS Proc. 2010, Schaumburg, IL USA
EXPERIMENTAL CHARACTERIZATION
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
6
TEST STRAIN RATE TEMPERATURE
QUASI-STATIC TENSILE 0.001/s -60°C, 25°C e +70°C
Quasi-static characterization
• Instron 5586 (electromechanic)
• Local deformation measurements (DIC)
• Low temperature (liquid CO2)
• Induction heating
EXPERIMENTAL CHARACTERIZATION
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
7
Characterization at high strain rate
• Direct Tension Split Hopkinson Pressure Bar
• Low temperature (liquid CO2)
• High frame rate camera
TEST STRAIN RATE TEMPERATURE
DYNAMIC TENSILE 600/s -60°C e 25°C
DYNAMIC TENSILE 1200/s -60°C e 25°C
8000 mm
3000 mm 3000 mm
1000 mm
A
A
A-A
1200 mm
specimenclamp
EXPERIMENTAL RESULTS: local strains
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
8
Local deformation map
Remarks
• Uniform strain over the gage length up to failure. No necking
0 0.05 0.1 0.15 0.2
0
200
400
600
800
1000
1200
1400
1600
Deformazione
Sforzo(MPa)
T= 298 K
T= 213 K
T= 343 K
Stress
Strain
EXPERIMENTAL RESULTS: temperature effect
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
9
Remarks
• At low temperatures, the work hardening rate increases,
whereas the apparent yield strength seems to decrease slightly
• Same behavior at different strain rates
0 0.05 0.1 0.15 0.2
0
200
400
600
800
1000
1200
1400
1600
Deformazione
Sforzo(MPa)
T= 298 K
T= 213 K
T= 343 K
0 0.05 0.1 0.15 0.2 0.25
0
200
400
600
800
1000
1200
1400
1600
Deformazione
Sforzo(MPa)
HpkGS_2
HpkGS_7
HpkGS_11
HpkGS_15
Quasistatic test Dynamic test
T=213 K
T=298 K
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
10
Remarks
• Strain rate affects the material yield stress
• Under dynamic loading, necking occurs just before failure
T=25°C
Stress
Stress
EXPERIMENTAL RESULTS: strain rate effect on the flow stress
T=-60°C
EXPERIMENTAL RESULTS: strain rate effects on yield stress and ductility
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
11
Remarks
• Absence of the knee in the initial yield stress vs. strain rate diagram
• As for the ADI 1200, the failure strain increases with the strain rate
10-4
10-3
10-2
10-1
100
101
102
103
104
600
700
800
900
1000
1100
1200
1300
1400
ADI 1050 (present work)
ADI1200 (Bohmer and Reissig, 2015)
Linear Fit of Sheet1 B"R02"
Yieldstress,R0.2%
[MPa]
STRAIN RATE [1/s]
10-4
10-3
10-2
10-1
100
101
102
103
104
0.00
0.05
0.10
0.15
0.20
0.25
0.30
0.35
0.40
ADI1050 T=298K
ADI1200 (Bohmer and Reissig, 2015)
ADI1050 T=213K
FAILURESTRAIN
STRAIN RATE [1/s]
EXPERIMENTAL RESULTS: failure mode
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
12
HpkGS5 RT 1200s-1
HpkGS7 RT 1200s-1
STRENGTH MODEL
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
13
0 100 200 300 400
0
1000
2000
3000
4000
5000
6000
7000
8000
9000
Temperatura (K)
AeB(MPa)
A
Fit A
B
Fit B
AS (MPa) ma B0 (MPa) mb n C
1207 160 10805 160 0.6 0.014 1.0
            &n
A T B T 1 Cln *
  
    
  
 
  
 
S
a
0
b
T
A A 1 exp
m
T
B B exp
m
Modified Johnson-Cook
MODEL VERIFICATION
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
14
0 0.5 1 1.5 2 2.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1E-3 s-1
, T=298 K
FEM
0 0.5 1 1.5 2 2.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1E-3 s-1
, T=213 K
FEM
0 0.5 1
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1E-3 s-1
, T=313 K
FEM
0 0.5 1 1.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=600 s-1
, T=213 K
FEM
0 0.5 1
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1200 s-1
, T=213 K
FEM
0 0.5 1 1.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=600 s-1
, T=298 K
FEM
0 0.5 1 1.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1200 s-1
, T=213 K
FEM
CONCLUSIONS
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
15
• Experimental results show an increase of up to 10% in ductility with increasing the strain rate
• Possible differences in the failure mechanism at different strain rates were observed
• Strain rate affects the initial yield stress (typical of a BCC structure)
• Absence of the knee in the initial yield stress vs strain rate diagram (typical of a FCC structure)
• Temperature affects the work hardening rate mainly (typical of a FCC structure)
• The proposed constitutive model describes with good accuracy the phenomenological
behavior that the ADI 1050 shows in the ranges of strain rate and temperature analyzed
ONGOING WORK
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
16
• To analyze further the peculiar effects of strain
rate and temperature on the flow stress
 Micro mechanical modeling for evaluating
the effects of residual stress
 To investigate the composite structure of
the ausferrite
• To analyze the stress triaxiality effect on the ductility at
different strain rates and temperatures
• To develop a damage model
0 0.5 1 1.5 2
0
0.5
1
1.5
2
2.5
3
TF
DeformazionearotturaEquivalentfailurestrain
  m eqTriaxiality factor

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ADI DAYS - Andrew Ruggiero

  • 1. Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 1 STRAIN RATE AND TEMPERATURE EFFECTS ON THE FLOW STRESS OF ADI A. Ruggieroa, G. Iannittib, E. Veneric, F. Vettorec , N. Bonoraa a University of Cassino and SL, DICeM, Cassino, Italy b TECHDYN Engineering, I-00199 Rome, Italy cZanardi Fonderie S.p.A, I-37046 Minerbe (VR), Italy
  • 2. BACKGROUND Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 2 • Cast irons are widely used in industrial practice mainly for the production of components through the process of casting • ADI matrix microstructure: ausferrite • Excellent property combinations of strength, ductility, and toughness • Valid substitute for steel for structural applications References [1] Böhme* and Reissig, Adv. Eng. Mat. 2015, 17, No. 8 [2] Keough and Hayrynen, SAE, 2000, paper no 248871
  • 3. BACKGROUND Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 3 • Designers show lack of confidence • Dread of a presumed low ductility under impulsive loading • Charpy impact test results
  • 4. AIM OF THE WORK Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 4 • To investigate the constitutive response of the ADI 1050-6 under different conditions of strain rate and temperature • To analyze the strain rate effect on the ductility • To develop a constitutive model for the design of components operating under both static and dynamic conditions
  • 5. MATERIALS Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 5 DESIGNATION UTS (MPa) YIELD STRESS (MPa) ELONGATION % HARDNE SS (BR) ADI 1050 1050 700 6 320-380 ADI 1200 1200 850 3 340-420 HSiADI 1450 1040 8.9 400 42CrMo4 1200 800 11 - [3] References [3] J. R. Keough, K. L. Hayrynen and G. L. Pioszak, AFS Proc. 2010, Schaumburg, IL USA
  • 6. EXPERIMENTAL CHARACTERIZATION Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 6 TEST STRAIN RATE TEMPERATURE QUASI-STATIC TENSILE 0.001/s -60°C, 25°C e +70°C Quasi-static characterization • Instron 5586 (electromechanic) • Local deformation measurements (DIC) • Low temperature (liquid CO2) • Induction heating
  • 7. EXPERIMENTAL CHARACTERIZATION Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 7 Characterization at high strain rate • Direct Tension Split Hopkinson Pressure Bar • Low temperature (liquid CO2) • High frame rate camera TEST STRAIN RATE TEMPERATURE DYNAMIC TENSILE 600/s -60°C e 25°C DYNAMIC TENSILE 1200/s -60°C e 25°C 8000 mm 3000 mm 3000 mm 1000 mm A A A-A 1200 mm specimenclamp
  • 8. EXPERIMENTAL RESULTS: local strains Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 8 Local deformation map Remarks • Uniform strain over the gage length up to failure. No necking 0 0.05 0.1 0.15 0.2 0 200 400 600 800 1000 1200 1400 1600 Deformazione Sforzo(MPa) T= 298 K T= 213 K T= 343 K Stress Strain
  • 9. EXPERIMENTAL RESULTS: temperature effect Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 9 Remarks • At low temperatures, the work hardening rate increases, whereas the apparent yield strength seems to decrease slightly • Same behavior at different strain rates 0 0.05 0.1 0.15 0.2 0 200 400 600 800 1000 1200 1400 1600 Deformazione Sforzo(MPa) T= 298 K T= 213 K T= 343 K 0 0.05 0.1 0.15 0.2 0.25 0 200 400 600 800 1000 1200 1400 1600 Deformazione Sforzo(MPa) HpkGS_2 HpkGS_7 HpkGS_11 HpkGS_15 Quasistatic test Dynamic test T=213 K T=298 K
  • 10. Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 10 Remarks • Strain rate affects the material yield stress • Under dynamic loading, necking occurs just before failure T=25°C Stress Stress EXPERIMENTAL RESULTS: strain rate effect on the flow stress T=-60°C
  • 11. EXPERIMENTAL RESULTS: strain rate effects on yield stress and ductility Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 11 Remarks • Absence of the knee in the initial yield stress vs. strain rate diagram • As for the ADI 1200, the failure strain increases with the strain rate 10-4 10-3 10-2 10-1 100 101 102 103 104 600 700 800 900 1000 1100 1200 1300 1400 ADI 1050 (present work) ADI1200 (Bohmer and Reissig, 2015) Linear Fit of Sheet1 B"R02" Yieldstress,R0.2% [MPa] STRAIN RATE [1/s] 10-4 10-3 10-2 10-1 100 101 102 103 104 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 ADI1050 T=298K ADI1200 (Bohmer and Reissig, 2015) ADI1050 T=213K FAILURESTRAIN STRAIN RATE [1/s]
  • 12. EXPERIMENTAL RESULTS: failure mode Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 12 HpkGS5 RT 1200s-1 HpkGS7 RT 1200s-1
  • 13. STRENGTH MODEL Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 13 0 100 200 300 400 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 Temperatura (K) AeB(MPa) A Fit A B Fit B AS (MPa) ma B0 (MPa) mb n C 1207 160 10805 160 0.6 0.014 1.0             &n A T B T 1 Cln *                   S a 0 b T A A 1 exp m T B B exp m Modified Johnson-Cook
  • 14. MODEL VERIFICATION Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 14 0 0.5 1 1.5 2 2.5 0 5000 10000 Allungamento (mm) Forza(N) d/dt=1E-3 s-1 , T=298 K FEM 0 0.5 1 1.5 2 2.5 0 5000 10000 Allungamento (mm) Forza(N) d/dt=1E-3 s-1 , T=213 K FEM 0 0.5 1 0 5000 10000 Allungamento (mm) Forza(N) d/dt=1E-3 s-1 , T=313 K FEM 0 0.5 1 1.5 0 5000 10000 Allungamento (mm) Forza(N) d/dt=600 s-1 , T=213 K FEM 0 0.5 1 0 5000 10000 Allungamento (mm) Forza(N) d/dt=1200 s-1 , T=213 K FEM 0 0.5 1 1.5 0 5000 10000 Allungamento (mm) Forza(N) d/dt=600 s-1 , T=298 K FEM 0 0.5 1 1.5 0 5000 10000 Allungamento (mm) Forza(N) d/dt=1200 s-1 , T=213 K FEM
  • 15. CONCLUSIONS Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 15 • Experimental results show an increase of up to 10% in ductility with increasing the strain rate • Possible differences in the failure mechanism at different strain rates were observed • Strain rate affects the initial yield stress (typical of a BCC structure) • Absence of the knee in the initial yield stress vs strain rate diagram (typical of a FCC structure) • Temperature affects the work hardening rate mainly (typical of a FCC structure) • The proposed constitutive model describes with good accuracy the phenomenological behavior that the ADI 1050 shows in the ranges of strain rate and temperature analyzed
  • 16. ONGOING WORK Austempering, A Technology for Substitution ADI DAYS 2016 6th – 7th October Minerbe 16 • To analyze further the peculiar effects of strain rate and temperature on the flow stress  Micro mechanical modeling for evaluating the effects of residual stress  To investigate the composite structure of the ausferrite • To analyze the stress triaxiality effect on the ductility at different strain rates and temperatures • To develop a damage model 0 0.5 1 1.5 2 0 0.5 1 1.5 2 2.5 3 TF DeformazionearotturaEquivalentfailurestrain   m eqTriaxiality factor