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ADI DAYS - Andrew Ruggiero
1. Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
1
STRAIN RATE AND TEMPERATURE EFFECTS
ON THE FLOW STRESS OF ADI
A. Ruggieroa, G. Iannittib, E. Veneric, F. Vettorec , N. Bonoraa
a University of Cassino and SL, DICeM, Cassino, Italy
b TECHDYN Engineering, I-00199 Rome, Italy
cZanardi Fonderie S.p.A, I-37046 Minerbe (VR), Italy
2. BACKGROUND
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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• Cast irons are widely used in industrial practice mainly
for the production of components through the
process of casting
• ADI matrix microstructure: ausferrite
• Excellent property combinations of strength, ductility,
and toughness
• Valid substitute for steel for structural applications
References
[1] Böhme* and Reissig, Adv. Eng. Mat. 2015, 17, No. 8
[2] Keough and Hayrynen, SAE, 2000, paper no 248871
3. BACKGROUND
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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• Designers show lack of confidence
• Dread of a presumed low ductility
under impulsive loading
• Charpy impact test results
4. AIM OF THE WORK
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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• To investigate the constitutive response of the ADI 1050-6
under different conditions of strain rate and temperature
• To analyze the strain rate effect on the ductility
• To develop a constitutive model for the design of components
operating under both static and dynamic conditions
5. MATERIALS
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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DESIGNATION
UTS
(MPa)
YIELD
STRESS
(MPa)
ELONGATION
%
HARDNE
SS
(BR)
ADI 1050 1050 700 6 320-380
ADI 1200 1200 850 3 340-420
HSiADI 1450 1040 8.9 400
42CrMo4 1200 800 11 -
[3]
References
[3] J. R. Keough, K. L. Hayrynen and G. L. Pioszak, AFS Proc. 2010, Schaumburg, IL USA
6. EXPERIMENTAL CHARACTERIZATION
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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TEST STRAIN RATE TEMPERATURE
QUASI-STATIC TENSILE 0.001/s -60°C, 25°C e +70°C
Quasi-static characterization
• Instron 5586 (electromechanic)
• Local deformation measurements (DIC)
• Low temperature (liquid CO2)
• Induction heating
7. EXPERIMENTAL CHARACTERIZATION
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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Characterization at high strain rate
• Direct Tension Split Hopkinson Pressure Bar
• Low temperature (liquid CO2)
• High frame rate camera
TEST STRAIN RATE TEMPERATURE
DYNAMIC TENSILE 600/s -60°C e 25°C
DYNAMIC TENSILE 1200/s -60°C e 25°C
8000 mm
3000 mm 3000 mm
1000 mm
A
A
A-A
1200 mm
specimenclamp
8. EXPERIMENTAL RESULTS: local strains
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
8
Local deformation map
Remarks
• Uniform strain over the gage length up to failure. No necking
0 0.05 0.1 0.15 0.2
0
200
400
600
800
1000
1200
1400
1600
Deformazione
Sforzo(MPa)
T= 298 K
T= 213 K
T= 343 K
Stress
Strain
9. EXPERIMENTAL RESULTS: temperature effect
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
9
Remarks
• At low temperatures, the work hardening rate increases,
whereas the apparent yield strength seems to decrease slightly
• Same behavior at different strain rates
0 0.05 0.1 0.15 0.2
0
200
400
600
800
1000
1200
1400
1600
Deformazione
Sforzo(MPa)
T= 298 K
T= 213 K
T= 343 K
0 0.05 0.1 0.15 0.2 0.25
0
200
400
600
800
1000
1200
1400
1600
Deformazione
Sforzo(MPa)
HpkGS_2
HpkGS_7
HpkGS_11
HpkGS_15
Quasistatic test Dynamic test
T=213 K
T=298 K
10. Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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Remarks
• Strain rate affects the material yield stress
• Under dynamic loading, necking occurs just before failure
T=25°C
Stress
Stress
EXPERIMENTAL RESULTS: strain rate effect on the flow stress
T=-60°C
11. EXPERIMENTAL RESULTS: strain rate effects on yield stress and ductility
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
11
Remarks
• Absence of the knee in the initial yield stress vs. strain rate diagram
• As for the ADI 1200, the failure strain increases with the strain rate
10-4
10-3
10-2
10-1
100
101
102
103
104
600
700
800
900
1000
1100
1200
1300
1400
ADI 1050 (present work)
ADI1200 (Bohmer and Reissig, 2015)
Linear Fit of Sheet1 B"R02"
Yieldstress,R0.2%
[MPa]
STRAIN RATE [1/s]
10-4
10-3
10-2
10-1
100
101
102
103
104
0.00
0.05
0.10
0.15
0.20
0.25
0.30
0.35
0.40
ADI1050 T=298K
ADI1200 (Bohmer and Reissig, 2015)
ADI1050 T=213K
FAILURESTRAIN
STRAIN RATE [1/s]
12. EXPERIMENTAL RESULTS: failure mode
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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HpkGS5 RT 1200s-1
HpkGS7 RT 1200s-1
13. STRENGTH MODEL
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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0 100 200 300 400
0
1000
2000
3000
4000
5000
6000
7000
8000
9000
Temperatura (K)
AeB(MPa)
A
Fit A
B
Fit B
AS (MPa) ma B0 (MPa) mb n C
1207 160 10805 160 0.6 0.014 1.0
&n
A T B T 1 Cln *
S
a
0
b
T
A A 1 exp
m
T
B B exp
m
Modified Johnson-Cook
14. MODEL VERIFICATION
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
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0 0.5 1 1.5 2 2.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1E-3 s-1
, T=298 K
FEM
0 0.5 1 1.5 2 2.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1E-3 s-1
, T=213 K
FEM
0 0.5 1
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1E-3 s-1
, T=313 K
FEM
0 0.5 1 1.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=600 s-1
, T=213 K
FEM
0 0.5 1
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1200 s-1
, T=213 K
FEM
0 0.5 1 1.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=600 s-1
, T=298 K
FEM
0 0.5 1 1.5
0
5000
10000
Allungamento (mm)
Forza(N)
d/dt=1200 s-1
, T=213 K
FEM
15. CONCLUSIONS
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
15
• Experimental results show an increase of up to 10% in ductility with increasing the strain rate
• Possible differences in the failure mechanism at different strain rates were observed
• Strain rate affects the initial yield stress (typical of a BCC structure)
• Absence of the knee in the initial yield stress vs strain rate diagram (typical of a FCC structure)
• Temperature affects the work hardening rate mainly (typical of a FCC structure)
• The proposed constitutive model describes with good accuracy the phenomenological
behavior that the ADI 1050 shows in the ranges of strain rate and temperature analyzed
16. ONGOING WORK
Austempering, A Technology for Substitution
ADI DAYS 2016 6th – 7th October Minerbe
16
• To analyze further the peculiar effects of strain
rate and temperature on the flow stress
Micro mechanical modeling for evaluating
the effects of residual stress
To investigate the composite structure of
the ausferrite
• To analyze the stress triaxiality effect on the ductility at
different strain rates and temperatures
• To develop a damage model
0 0.5 1 1.5 2
0
0.5
1
1.5
2
2.5
3
TF
DeformazionearotturaEquivalentfailurestrain
m eqTriaxiality factor