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When polymers are filled with nanosized inorganic materials produce nanohybrids with optimized properties1. The optimization of the properties occurs because the behaviour of polymers when they are restricted in space or when they are close to surfaces can be very different from that in the bulk2. Polymer dispersion, morphology and crystallization are investigated in hydrophilic poly(ethylene oxide) and two kinds of silica nanoparticles of different sizes, pursuing to understand the case of severely confined polymers. Hybrids with different ratio between the two silica nanoparticles were synthesized in order to achieve the highest confinement. The crystalline behavior of the hybrids was examined through Differential Scanning Calorimetry (DSC) and X-Ray Diffraction (XRD).The polymer chains that were able to crystallize under confinement showed a different crystalline bahavior with a lower Tm and lower crystallinity. Under severe confinement the polymer was not able to crystallize at all.
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Lee 1 a_d
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8:00 9:00 10:00 11:00 12:00 13:00 14:00 15:00 16:00 17:00 18:00 19:00 20:00 21:00 22:00 23:00 Segunda-feiraTerça-feiraQuarta-feiraQuinta-feiraSexta-feira InstitutoSuperiordeEngenhariadeCoimbra Lic.Eng.Eletrotécnica-LEE1A1SD Coimbra,8-10-2010OPresidentedoISEC (Prof.DoutorNunoFerreira,Prof.Adjunto) AplEng_1D OT6 EE_LAI1 AplEng_1D OT5 EE_LAI2 AplEng_1D OT4 EE_LAB_Energia AplEng_1D OT3 EE_E0_15 AplEng_1D OT2 EE_LAI2 AplEng_1D OT1 EE_LAI2 Elec-I_1D OT4 EE_E0_21 Elec-I_1D OT3 EE_E0_21 IP_1D T1 EE_E0_15 FisGe_1D P4 G_LabFísica FisGe_1D P3 G_LabFísica FisGe_1D P2 G_LabFísica FisGe_1D P1 G_LabFísica FisGe_1D TP4 G_LabFísica FisGe_1D TP3 G_LabFísica FisGe_1D TP2 G_LabFísica FisGe_1D TP1 G_LabFísica FisGe_1D T1 EE_E0_15 AlgLin_1D TP3 G1_100 AlgLin_1D TP2 G1_99 AM1_1D T1 G0_A2 AM1_1D T1 EE_E0_15 AM1_1D TP1 G1_126 AM1_1D TP2 G1_99 AM1_1D TP3 G1_99 AM1_1D TP4 G1_99 AM1_1D OT1 G1_100 AM1_1D OT2 G1_99 AM1_1D OT3 G1_99 AM1_1D OT4 G1_99 AlgLin_1D T1 EE_E0_15 AlgLin_1D T1 G0_A2 AlgLin_1D TP1 G1_99 IP_1D T1 EE_E0_15 IP_1D P1 EE_LAI1 IP_1D P2 EE_LAI1 IP_1D P3 EE_LAI1 IP_1D P4 EE_LAI1 IP_1D P5 EE_LAI1 IP_1D P6 EE_LAI2 IP_1D P7 EE_LAI2 IP_1D P9 EE_LAI1 Elec-I_1D T1 EE_E0_15 Elec-I_1D T1 EE_E0_15 Elec-I_1D TP1 EE_LAB_Med Elec-I_1D TP2 EE_LAB_EL Elec-I_1D TP3 EE_LAB_Med Elec-I_1D TP4 EE_LAB_Med Elec-I_1D TP5 EE_LAB_Med Elec-I_1D TP6 EE_LAB_Med Elec-I_1D TP7 EE_LAB_SD Elec-I_1D TP8 EE_LAB_SD Elec-I_1D TP9 EE_LAB_SD Elec-I_1D TP10 EE_LAB_SD Elec-I_1D OT1 EE_E0_21 Elec-I_1D OT2 EE_E0_21
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