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© Zetec Inc. All rights reserved
HTHA Detection
Application Solution
© Zetec Inc. All rights reserved
• Inspection Challenge
• Recommended Solution & Results
• Probe Innovation
• Benefits of Zetec Solution
Overview
2
© Zetec Inc. All rights reserved
• High Temperature Hydrogen Attack (HTHA) occurs in steels
operating at high temperature, above 205°C (400°F) in hydrogen
environments, in refinery, petrochemical and chemical facilities
• HTHA is the result of hydrogen dissociating and dissolving in
the steel, and then reacting with carbides to form methane,
which accumulates at grain boundaries, and eventually leads to
the fissures and cracking
• Early stages of HTHA are very difficult to detect, because of the
small size of the methane voids, typically < 0.1 mm (0.004”),
i.e. much smaller than the applied ultrasonic wavelength
Inspection Challenge
3
© Zetec Inc. All rights reserved
HTHA in heat exchanger caused catastrophic fire at a refinery
(WA, USA) in April 2010
Consequences of HTHA Damage
4
© Zetec Inc. All rights reserved
• Efficient and robust inspection strategy, combining
multiple ultrasonic examination techniques
• “Damage specific” operator training on specimens
with confirmed HTHA (e.g. Lavender International)
• Carefully selected UT and phased array probes
• portable PA UT unit, with all tools and
features to efficiently set up and deploy all
recommended examination techniques : TOFD,
TULA, beamforming phased array UT and live TFM
Recommended Solution
5
© Zetec Inc. All rights reserved
• TOFD, using high-quality UT probes, is a rapid and robust technique
for initial screening of base material and welded regions (HAZ)
• Probe size and frequency depend on material type and wall thickness
• Increased grain noise (short indications) and clustering (beehive) in
A-Scan signals are indicative for early stage HTHA
Examination Technique - TOFD
6
Courtesy of Lavender International
© Zetec Inc. All rights reserved
• TULA (TOFD Ultra Low Angle), conventional T/R
UT probes at 10 MHz, are well suited for initial
screening of thicker base material
• As for TOFD, increased back-scattering and
clustering in A-Scan signals are indicative for HTHA
Examination Technique - TULA
7
HTHA
« cluster »
Courtesy of Lavender International
© Zetec Inc. All rights reserved
• Standard PA UT, with 10 MHz LW DLA probe, used for secondary
inspection
• Carefully selected focusing, using 32 or 64 active elements, is key to
detect clusters of small methane voids and micro-fissures
Examination Technique – PA UT
8
HTHA
Courtesy of Lavender International
© Zetec Inc. All rights reserved
• TFM, with 10 MHz LW DLA probe, used for secondary inspection
• Confirmation and discrimination between HTHA damage and
inclusions, using strong “total focusing” capability
Examination Technique – TFM
9
HTHA
Courtesy of Lavender International
HTHA
Induced Crack
Inclusions
© Zetec Inc. All rights reserved
• TFM (frame 512 x 512), with large 10 MHz probe, in direct contact
for secondary inspection of thick flange specimen, T = 90 mm (3.5”)
• Confirmation and characterization of HTHA damage with strong
“total focusing” capability (virtual beam shown)
Examination Technique – TFM
10
HTHA
« cluster »
Courtesy of Lavender International
© Zetec Inc. All rights reserved
DLA 10 MHz Probe (Pitch & Catch)
Probe Innovation – LW Inspection
11
• Integrated DLA probe, NDT Paintbrush compatible
• 2 x 64 elements, small pitch for improved TFM imaging
• DLA “Autofocusing” for improved resolution in passive plane,
with beamforming PA UT as well as TFM
active plane
1 mm
passive plane
2 mm
Depth of field
15 mm
© Zetec Inc. All rights reserved
AL-TFM 5 MHz Probe (Pulse-Echo)
Probe Innovation – SW Inspection
12
• AL- type housing, using standard AL- 55SW wedge
• 64 elements, small pitch for improved TFM imaging in HAZ
under weld cap
• Curved active element for improved resolution in passive plane
active plane
1 mm
passive plane
1 mm
Depth of field
20 mm
© Zetec Inc. All rights reserved
• Fully integrated, portable PA UT unit
• Excellent 64 active element PA UT
• 2 high-SNR TOFD channels at 200 V
• 12” Hi-Res multi-touch display
• Best-in class « live » TFM
• Parallel recording of PA UT & TFM
• Bipolar pulse (150Vpp) option
• Driven by UtraVision Touch
Successfully used for Lavender HTHA Certification !
- Versatile PA UT Unit
13
© Zetec Inc. All rights reserved
• Complete offering of high-quality standard and
application specific PA UT probes required for
efficient detection and characterization of HTHA
damage
• portable PA UT unit, includes all
required tools and features to efficiently set up and
deploy all recommended examination techniques :
TOFD, TULA, phased array UT and live TFM
Benefits of Zetec Solution
14

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Solution: High Temperature Hydrogen Attack (HTHA) Inspection Challenge

  • 1. © Zetec Inc. All rights reserved HTHA Detection Application Solution
  • 2. © Zetec Inc. All rights reserved • Inspection Challenge • Recommended Solution & Results • Probe Innovation • Benefits of Zetec Solution Overview 2
  • 3. © Zetec Inc. All rights reserved • High Temperature Hydrogen Attack (HTHA) occurs in steels operating at high temperature, above 205°C (400°F) in hydrogen environments, in refinery, petrochemical and chemical facilities • HTHA is the result of hydrogen dissociating and dissolving in the steel, and then reacting with carbides to form methane, which accumulates at grain boundaries, and eventually leads to the fissures and cracking • Early stages of HTHA are very difficult to detect, because of the small size of the methane voids, typically < 0.1 mm (0.004”), i.e. much smaller than the applied ultrasonic wavelength Inspection Challenge 3
  • 4. © Zetec Inc. All rights reserved HTHA in heat exchanger caused catastrophic fire at a refinery (WA, USA) in April 2010 Consequences of HTHA Damage 4
  • 5. © Zetec Inc. All rights reserved • Efficient and robust inspection strategy, combining multiple ultrasonic examination techniques • “Damage specific” operator training on specimens with confirmed HTHA (e.g. Lavender International) • Carefully selected UT and phased array probes • portable PA UT unit, with all tools and features to efficiently set up and deploy all recommended examination techniques : TOFD, TULA, beamforming phased array UT and live TFM Recommended Solution 5
  • 6. © Zetec Inc. All rights reserved • TOFD, using high-quality UT probes, is a rapid and robust technique for initial screening of base material and welded regions (HAZ) • Probe size and frequency depend on material type and wall thickness • Increased grain noise (short indications) and clustering (beehive) in A-Scan signals are indicative for early stage HTHA Examination Technique - TOFD 6 Courtesy of Lavender International
  • 7. © Zetec Inc. All rights reserved • TULA (TOFD Ultra Low Angle), conventional T/R UT probes at 10 MHz, are well suited for initial screening of thicker base material • As for TOFD, increased back-scattering and clustering in A-Scan signals are indicative for HTHA Examination Technique - TULA 7 HTHA « cluster » Courtesy of Lavender International
  • 8. © Zetec Inc. All rights reserved • Standard PA UT, with 10 MHz LW DLA probe, used for secondary inspection • Carefully selected focusing, using 32 or 64 active elements, is key to detect clusters of small methane voids and micro-fissures Examination Technique – PA UT 8 HTHA Courtesy of Lavender International
  • 9. © Zetec Inc. All rights reserved • TFM, with 10 MHz LW DLA probe, used for secondary inspection • Confirmation and discrimination between HTHA damage and inclusions, using strong “total focusing” capability Examination Technique – TFM 9 HTHA Courtesy of Lavender International HTHA Induced Crack Inclusions
  • 10. © Zetec Inc. All rights reserved • TFM (frame 512 x 512), with large 10 MHz probe, in direct contact for secondary inspection of thick flange specimen, T = 90 mm (3.5”) • Confirmation and characterization of HTHA damage with strong “total focusing” capability (virtual beam shown) Examination Technique – TFM 10 HTHA « cluster » Courtesy of Lavender International
  • 11. © Zetec Inc. All rights reserved DLA 10 MHz Probe (Pitch & Catch) Probe Innovation – LW Inspection 11 • Integrated DLA probe, NDT Paintbrush compatible • 2 x 64 elements, small pitch for improved TFM imaging • DLA “Autofocusing” for improved resolution in passive plane, with beamforming PA UT as well as TFM active plane 1 mm passive plane 2 mm Depth of field 15 mm
  • 12. © Zetec Inc. All rights reserved AL-TFM 5 MHz Probe (Pulse-Echo) Probe Innovation – SW Inspection 12 • AL- type housing, using standard AL- 55SW wedge • 64 elements, small pitch for improved TFM imaging in HAZ under weld cap • Curved active element for improved resolution in passive plane active plane 1 mm passive plane 1 mm Depth of field 20 mm
  • 13. © Zetec Inc. All rights reserved • Fully integrated, portable PA UT unit • Excellent 64 active element PA UT • 2 high-SNR TOFD channels at 200 V • 12” Hi-Res multi-touch display • Best-in class « live » TFM • Parallel recording of PA UT & TFM • Bipolar pulse (150Vpp) option • Driven by UtraVision Touch Successfully used for Lavender HTHA Certification ! - Versatile PA UT Unit 13
  • 14. © Zetec Inc. All rights reserved • Complete offering of high-quality standard and application specific PA UT probes required for efficient detection and characterization of HTHA damage • portable PA UT unit, includes all required tools and features to efficiently set up and deploy all recommended examination techniques : TOFD, TULA, phased array UT and live TFM Benefits of Zetec Solution 14