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Metal Quality and Technology
         in Europe
   means Added Value ?
            Gary Mahon
         gary.mahon@innovaltec.com
Scope


  The European Industry Landscape

  Evaluating Billet Quality

  Innovative Scrap Processing

  Global R&D Trends

  Managing Knowledge Assets

  Does Europe have a Sustainable Advantage ?




                                               © Innoval Technology Ltd
                                                      IP07-047, Slide 3
EU-25 Aluminium Flow Chart (2005)




                                    Sustainability of the European Aluminium Industry 2006,
                                                           European Aluminium Association.


                                                                     © Innoval Technology Ltd
                                                                            IP07-047, Slide 4
Primary Aluminium Regional Balances




                                      Expect more Billet from these regions



                                                 Sustainability of the European Aluminium Industry 2006,
                                                                        European Aluminium Association.


                                                                                  © Innoval Technology Ltd
                                                                                         IP07-047, Slide 5
Extruded Metal Quality
 Geometric Tolerances           Surface Properties
Weight per metre             Reflectivity
Dimensional accuracy         Topography
Bow                          Uniformity
Flatness                     Anodising Response

 Mechanical Properties                   Defects
Strength                     Die lines
Toughness                    Speed tears
Formability                  Stains
Fatigue                      Pick-up
           Other             Scratches
Corrosion resistance         Blisters
Welded Properties            Marks

                                      Influenced by billet quality

                                                                     © Innoval Technology Ltd
                                                                            IP07-047, Slide 6
Examples of Composition Control on Quality

                     Intermetallics                                        Surface Pick-up
             100                                                   125
             90
                                                                                                           0.09 Mn
             80                                                    100




                                              Exit Speed (m/min)
             70
             60                                                    75
   % Alpha




             50
                                                                                                           0.06 Mn
             40                                                    50
             30     0.03 Mn                                                                                0.03 Mn
             20     0.06 Mn                                        25
                    0.09 Mn                                              Pick-up
             10
                                                                         OK
              0                                                     0
              0.40 0.45 0.50 0.55 0.60 0.65                         0.40 0.45 0.50 0.55 0.60 0.65
                         wt.% Si                                                   wt.% Si
                                                                                                  Brassard et al
                                                                                                         Alcan
                                                                                                         ET’04

                                                                                             © Innoval Technology Ltd
                                                                                                    IP07-047, Slide 7
Metal Cleanliness with Prefil®: Pressure Filtration


N-Tec
                                                      1400



                                                      1200
                                                                   CLEAN
                                                                (High Flow Rate)
                                                                                          Increasing Inclusion




                                         Weight (g)
                                                      1000                                      Content


                                                      800



                                                      600
                                                                                                            High
                                                      400                                                 Inclusion
                                                                                                           Content
                                                      200                                               (Low Flow Rate)

                                                        0
                                                            0          30          60              90             120              150
                                                                                        Time (s)




                                                                                                        © Innoval Technology Ltd
                                                                                                               IP07-047, Slide 8
Prefil® Metallographic Inclusion Analysis

                                              Aluminium
N-Tec




                                              Inclusion band


                                                                            Defect Mapping




                                                                                                                  Degasser
                                                                                  Transfer


                                                                                                        Launder
                                                               Smelter




                                                                                                                                      Casting
                                                                                             Holder
                                              Filter grains




                                                                         Melter




                                                                                                                             Filter
                  Wide Inclusion Band
                   Many Inclusions
                                                      Al4C3
                                                    (TiV)B2
                                           Al Borocarbides
                                     Al2O3 films & particles
                                     MgO films & particles
                                    Spinel films & particles
                                                        AlN
                                       Refractory particles
                                              Fe Mn oxides
                                                  Bone ash
                                                               Note this is not a comprehensive list

                                                                                                      © Innoval Technology Ltd
                                                                                                             IP07-047, Slide 9
Example of Analysis of Billet Defect - Cracking

                                    Detailed Metallography
                                    SEM & EDX
                                    Fingerprint against defect library
                                    Root-cause analysis
                           250 µm


      Grain Structure




                                                           Al                                       MgO
                                              O
                                                                                                    Water
                                                      Mg
                                          C

                                                                                 Ca

                                                           Si       S
           10 µm                                                        Cl            Ca

                        SEM SEI                   1             2            3        4    keV


                                                                EDX spectrum
                                                                                           © Innoval Technology Ltd
                                                                                                 IP07-047, Slide 10
Evaluation of Billet Quality – Intermetallics
                       25
                                                                           p
                                                                                                                 Alpha:       46        %
                       20
                                                                                                                 Beta:      54    %
         App. Conc. Fe+Mn
                                                                                                                      Alpha Standard
                       15
                                                                                                                       Beta Standard

                       10


                            5


                            0
                                0.0   0.5   1.0   1.5             2.0       2.5           3.0            3.5          4.0             4.5        5.0
                                                                   App. Conc. Si

                                                                  100
                                                                                   Bottom                              Middle                                Top
                                                                  95

                                                                  90

                                                        % alpha   85
                                                                  80

                                                                  75
                                                                  70
                                                                  65

                                                                  60
                                                                  55

                                                                  50
  Red superimposed image of Mg2Si                                        Edge      Mid radius   Center         Edge      Mid radius     Center     Edge     Mid radius   Center




                                                                                                                                                       © Innoval Technology Ltd
                                                                                                                                                             IP07-047, Slide 11
Evaluation of Billet Quality


  Billet is the critical starting point for extrusion Quality

  Expect new Billet Suppliers from developing Countries

  Evaluation techniques exist to measure billet quality

  Technical Audit of Suppliers




     Need to insist that billet suppliers are meeting your requirements




                                                                  © Innoval Technology Ltd
                                                                        IP07-047, Slide 12
Environmental Benefits of Aluminium Recycling


           100                            Aluminium Smelting is highly energy
 Energy                                   intensive.
Required   80
  (%)
                                          Remelting of recycled aluminium
                                          consumes only 5% of the energy
           60
                                          required for primary production.
           40                             Recycling is far less Greenhouse Gas
                                          intense.
           20
                                          Alcoa utilises about 20% recycled metal
            0                             for fabricated products.
                    New       Recycled
                 Aluminium   Aluminium
                                          Alcoa is publicly committed to 50% of
                                          fabricated products from recycled metal
                                          by 2020.


                                                                     Conference Board Session on Sustainability
                                         Randy Overbey President, Alcoa Primary Metals Development, June 2005


                                                                                          © Innoval Technology Ltd
                                                                                                IP07-047, Slide 13
Growth of Old Scrap (Post Use)


                                  16000
                                               Other
                                  14000
                                               Consumer Durables
    Old scrap (thousand tonnes)




                                  12000        Engineering
                                               Packaging
                                  10000
                                               Building
                                  8000         Other Transport
                                               Automotive
                                  6000

                                  4000

                                  2000

                                     0
                                          1950 1960 1970 1980 1990 2000 2003 2004 2010 2020

                                                                        Global Aluminium Recycling Committee
                                                                                                       2005




                                                                                                       © Innoval Technology Ltd
                                                                                                             IP07-047, Slide 14
Up-Cycling of Light Alloys from Recycled Scrap




  Aim to prevent down-grading of wrought-alloy Old Scrap into casting alloys.

  Deliver Value-Added products for Recyclers

  Based on Melt Conditioning by high shear of liquid metal.

  Family of technologies developed at Brunel University.

  £1.2M over three years from UK Technology Strategy Board

  Innoval is Lead Partner and Technical Manager.

  Started March 2007.




                                                                     © Innoval Technology Ltd
                                                                           IP07-047, Slide 15
High-Shear Twin-Screw Melt-Conditioning




                                               Feeding DC Caster


       Centre                                                      Edge




                         Mg-alloy AZ31 Φ60mm billet



                                                                     © Innoval Technology Ltd
                                                                           IP07-047, Slide 16
Examples of Potential of Melt Conditioning


                                     Mg-Alloy AZ91D
                                                                                                               LM25 (Al-10.3Si-0.3Cu-0.16Mn)
               300                                                       8                                     12
                                    Yield    UTS       Elongation
                                                                         7                                                                MC
               250                                                                                             10
                                                                                                                                          HPDC




                                                                                              Elongation (%)
                                                                         6
Yield, UTS (MPa)




               200




                                                                             Elongation (%)
                                                                                                               8
                                                                         5

               150                                                       4                                     6

                                                                         3
               100                                                                                             4
                                                                         2
                   50                                                                                          2
                                                                         1

                    0                                                    0                                     0
                        100%Scrap           50%Scrap           Primary                                              0.4   0.6    0.8      1          1.2
                                                                                                                           Fe Content (wt.%)

                        Quality unaffected by scrap recycling                                          Fe tolerance increased by 0.37wt%



                                                                                                                                           © Innoval Technology Ltd
                                                                                                                                                 IP07-047, Slide 17
Impact of Technology Development not always in Europe



          SME’s                    Independent              Global Companies
  Entrepreneurs                Investing in long-term       Usually invest most in
                               sustainability of their      technology development
  Development usually
                               operations
  undertaken in                                             Make financially driven
  technologically advanced     Need to protect and          decisions to satisfy
  regions                      enforce IPR position to      shareholders
                               prevent copying
  If necessary, will licence                                Often put plant in lowest
  globally to get return on    Developer has first mover    cost region regardless of
  investment                   advantage, but for limited   where technology
                               lifetime                     developed




         Needs a continuous through-put of ideas and innovations




                                                                         © Innoval Technology Ltd
                                                                               IP07-047, Slide 18
R&D Policy Response


                                  EU Framework 7
      Collaborative and International
      50% funding (75% for SME’s)
      Focus on science, technology development and exploitation for benefit of EU


                         UK Technology Strategy Board
      Collaborative within UK
      50% funding
      Need supply chain in place for exploitation


                                University Education
      EU is continuing to invest in producing a high number of science and
      engineering graduates.




                                                                             © Innoval Technology Ltd
                                                                                   IP07-047, Slide 19
Value-Added Opportunities




                                                   Design
                                                   Die Coatings
                                New Profiles &
                                                   Cost Reduction to enable
                                  Processes        penetration into new markets




                             New           Finishing
 High Strength Aerospace    Alloys        Operations
 Alloys
 Weldable medium strength
 6000-series Alloys
                                                            Product Differentiation
 Metal Matrix Composites
                                                            Technically demanding
                                                            products




                                                                   © Innoval Technology Ltd
                                                                         IP07-047, Slide 20
World Labour Costs by Region




            Investing in State-of-the-Art Equipment



                                                      Sustainability of the European Aluminium Industry 2006,
                                                                             European Aluminium Association.


                                                                                       © Innoval Technology Ltd
                                                                                             IP07-047, Slide 21
State-of-the-Art Equipment is Not Sufficient

  Realisation that investment in world class equipment does not on its own give
  world class products.
  Many examples in aluminium rolling mills and extrusion plants.
     Return on investments taking longer than planned
     Cannot match quality of world-class products
     Need expertise that equipment suppliers do not possess




   Equipment manufacturers looking to partner with product specialists
                    to deliver a complete package


                                                                     © Innoval Technology Ltd
                                                                           IP07-047, Slide 22
Managing Knowledge Assets

  Important to maximise the knowledge that exists in existing employees
     Staff with valuable knowledge which is not exploited
     Loss of long-serving, knowledgeable employees
     Share knowledge of manufacturing to improve product quality
     Determine gaps in the knowledge base (R&D programme)
     Standardise operations and develop “Best Practice”


  Knowledge Management using K-Maps
     Based on ‘The Voice of the Customer’ or QFD (Quality Function Deployment)
     Team-based Workshop approach involving
      – Manufacturing
      – Technology
      – Sales




                                                                         © Innoval Technology Ltd
                                                                               IP07-047, Slide 23
Knowledge Mapping Matrix




                               How to Build a K-Map

                           Assemble those with knowledge

                           Define Product Attributes

                           Define the Process Stages

                           Define the strength of relationship

                           Develop content via Intranet




                                                 © Innoval Technology Ltd
                                                       IP07-047, Slide 24
K-Map Summary Level




                      © Innoval Technology Ltd
                            IP07-047, Slide 25
K-Map Case Study - Enthovens Pb Battery Recycling


  Actual Standard Operating Practice captured and
  agreed by all shifts for the Refinery.
  14% increase in output.
  3% reduction in fuel use.
  Improved Team Work throughout Plant.
  Currently using P-Map to compare Key Performance
  Indicators and develop “Best Practice” across 10
  European sites.




                                                     © Innoval Technology Ltd
                                                           IP07-047, Slide 26
Summary

 European extruders currently have a technical advantage


 To keep this advantage we need to
    Keep a robust manufacturing infrastructure
    Maintain high quality throughout the supply chain
    Invest in innovation and new technology
    Fund dynamic and exciting aluminium R&D programmes
    Manage highly qualified and innovative European nationals




                                                        gary.mahon@innovaltec.com

                                                                   © Innoval Technology Ltd
                                                                         IP07-047, Slide 27

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Metal Quality and Technology in Europe means Added Value?

  • 1. Metal Quality and Technology in Europe means Added Value ? Gary Mahon gary.mahon@innovaltec.com
  • 2. Scope The European Industry Landscape Evaluating Billet Quality Innovative Scrap Processing Global R&D Trends Managing Knowledge Assets Does Europe have a Sustainable Advantage ? © Innoval Technology Ltd IP07-047, Slide 3
  • 3. EU-25 Aluminium Flow Chart (2005) Sustainability of the European Aluminium Industry 2006, European Aluminium Association. © Innoval Technology Ltd IP07-047, Slide 4
  • 4. Primary Aluminium Regional Balances Expect more Billet from these regions Sustainability of the European Aluminium Industry 2006, European Aluminium Association. © Innoval Technology Ltd IP07-047, Slide 5
  • 5. Extruded Metal Quality Geometric Tolerances Surface Properties Weight per metre Reflectivity Dimensional accuracy Topography Bow Uniformity Flatness Anodising Response Mechanical Properties Defects Strength Die lines Toughness Speed tears Formability Stains Fatigue Pick-up Other Scratches Corrosion resistance Blisters Welded Properties Marks Influenced by billet quality © Innoval Technology Ltd IP07-047, Slide 6
  • 6. Examples of Composition Control on Quality Intermetallics Surface Pick-up 100 125 90 0.09 Mn 80 100 Exit Speed (m/min) 70 60 75 % Alpha 50 0.06 Mn 40 50 30 0.03 Mn 0.03 Mn 20 0.06 Mn 25 0.09 Mn Pick-up 10 OK 0 0 0.40 0.45 0.50 0.55 0.60 0.65 0.40 0.45 0.50 0.55 0.60 0.65 wt.% Si wt.% Si Brassard et al Alcan ET’04 © Innoval Technology Ltd IP07-047, Slide 7
  • 7. Metal Cleanliness with Prefil®: Pressure Filtration N-Tec 1400 1200 CLEAN (High Flow Rate) Increasing Inclusion Weight (g) 1000 Content 800 600 High 400 Inclusion Content 200 (Low Flow Rate) 0 0 30 60 90 120 150 Time (s) © Innoval Technology Ltd IP07-047, Slide 8
  • 8. Prefil® Metallographic Inclusion Analysis Aluminium N-Tec Inclusion band Defect Mapping Degasser Transfer Launder Smelter Casting Holder Filter grains Melter Filter Wide Inclusion Band Many Inclusions Al4C3 (TiV)B2 Al Borocarbides Al2O3 films & particles MgO films & particles Spinel films & particles AlN Refractory particles Fe Mn oxides Bone ash Note this is not a comprehensive list © Innoval Technology Ltd IP07-047, Slide 9
  • 9. Example of Analysis of Billet Defect - Cracking Detailed Metallography SEM & EDX Fingerprint against defect library Root-cause analysis 250 µm Grain Structure Al MgO O Water Mg C Ca Si S 10 µm Cl Ca SEM SEI 1 2 3 4 keV EDX spectrum © Innoval Technology Ltd IP07-047, Slide 10
  • 10. Evaluation of Billet Quality – Intermetallics 25 p Alpha: 46 % 20 Beta: 54 % App. Conc. Fe+Mn Alpha Standard 15 Beta Standard 10 5 0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 App. Conc. Si 100 Bottom Middle Top 95 90 % alpha 85 80 75 70 65 60 55 50 Red superimposed image of Mg2Si Edge Mid radius Center Edge Mid radius Center Edge Mid radius Center © Innoval Technology Ltd IP07-047, Slide 11
  • 11. Evaluation of Billet Quality Billet is the critical starting point for extrusion Quality Expect new Billet Suppliers from developing Countries Evaluation techniques exist to measure billet quality Technical Audit of Suppliers Need to insist that billet suppliers are meeting your requirements © Innoval Technology Ltd IP07-047, Slide 12
  • 12. Environmental Benefits of Aluminium Recycling 100 Aluminium Smelting is highly energy Energy intensive. Required 80 (%) Remelting of recycled aluminium consumes only 5% of the energy 60 required for primary production. 40 Recycling is far less Greenhouse Gas intense. 20 Alcoa utilises about 20% recycled metal 0 for fabricated products. New Recycled Aluminium Aluminium Alcoa is publicly committed to 50% of fabricated products from recycled metal by 2020. Conference Board Session on Sustainability Randy Overbey President, Alcoa Primary Metals Development, June 2005 © Innoval Technology Ltd IP07-047, Slide 13
  • 13. Growth of Old Scrap (Post Use) 16000 Other 14000 Consumer Durables Old scrap (thousand tonnes) 12000 Engineering Packaging 10000 Building 8000 Other Transport Automotive 6000 4000 2000 0 1950 1960 1970 1980 1990 2000 2003 2004 2010 2020 Global Aluminium Recycling Committee 2005 © Innoval Technology Ltd IP07-047, Slide 14
  • 14. Up-Cycling of Light Alloys from Recycled Scrap Aim to prevent down-grading of wrought-alloy Old Scrap into casting alloys. Deliver Value-Added products for Recyclers Based on Melt Conditioning by high shear of liquid metal. Family of technologies developed at Brunel University. £1.2M over three years from UK Technology Strategy Board Innoval is Lead Partner and Technical Manager. Started March 2007. © Innoval Technology Ltd IP07-047, Slide 15
  • 15. High-Shear Twin-Screw Melt-Conditioning Feeding DC Caster Centre Edge Mg-alloy AZ31 Φ60mm billet © Innoval Technology Ltd IP07-047, Slide 16
  • 16. Examples of Potential of Melt Conditioning Mg-Alloy AZ91D LM25 (Al-10.3Si-0.3Cu-0.16Mn) 300 8 12 Yield UTS Elongation 7 MC 250 10 HPDC Elongation (%) 6 Yield, UTS (MPa) 200 Elongation (%) 8 5 150 4 6 3 100 4 2 50 2 1 0 0 0 100%Scrap 50%Scrap Primary 0.4 0.6 0.8 1 1.2 Fe Content (wt.%) Quality unaffected by scrap recycling Fe tolerance increased by 0.37wt% © Innoval Technology Ltd IP07-047, Slide 17
  • 17. Impact of Technology Development not always in Europe SME’s Independent Global Companies Entrepreneurs Investing in long-term Usually invest most in sustainability of their technology development Development usually operations undertaken in Make financially driven technologically advanced Need to protect and decisions to satisfy regions enforce IPR position to shareholders prevent copying If necessary, will licence Often put plant in lowest globally to get return on Developer has first mover cost region regardless of investment advantage, but for limited where technology lifetime developed Needs a continuous through-put of ideas and innovations © Innoval Technology Ltd IP07-047, Slide 18
  • 18. R&D Policy Response EU Framework 7 Collaborative and International 50% funding (75% for SME’s) Focus on science, technology development and exploitation for benefit of EU UK Technology Strategy Board Collaborative within UK 50% funding Need supply chain in place for exploitation University Education EU is continuing to invest in producing a high number of science and engineering graduates. © Innoval Technology Ltd IP07-047, Slide 19
  • 19. Value-Added Opportunities Design Die Coatings New Profiles & Cost Reduction to enable Processes penetration into new markets New Finishing High Strength Aerospace Alloys Operations Alloys Weldable medium strength 6000-series Alloys Product Differentiation Metal Matrix Composites Technically demanding products © Innoval Technology Ltd IP07-047, Slide 20
  • 20. World Labour Costs by Region Investing in State-of-the-Art Equipment Sustainability of the European Aluminium Industry 2006, European Aluminium Association. © Innoval Technology Ltd IP07-047, Slide 21
  • 21. State-of-the-Art Equipment is Not Sufficient Realisation that investment in world class equipment does not on its own give world class products. Many examples in aluminium rolling mills and extrusion plants. Return on investments taking longer than planned Cannot match quality of world-class products Need expertise that equipment suppliers do not possess Equipment manufacturers looking to partner with product specialists to deliver a complete package © Innoval Technology Ltd IP07-047, Slide 22
  • 22. Managing Knowledge Assets Important to maximise the knowledge that exists in existing employees Staff with valuable knowledge which is not exploited Loss of long-serving, knowledgeable employees Share knowledge of manufacturing to improve product quality Determine gaps in the knowledge base (R&D programme) Standardise operations and develop “Best Practice” Knowledge Management using K-Maps Based on ‘The Voice of the Customer’ or QFD (Quality Function Deployment) Team-based Workshop approach involving – Manufacturing – Technology – Sales © Innoval Technology Ltd IP07-047, Slide 23
  • 23. Knowledge Mapping Matrix How to Build a K-Map Assemble those with knowledge Define Product Attributes Define the Process Stages Define the strength of relationship Develop content via Intranet © Innoval Technology Ltd IP07-047, Slide 24
  • 24. K-Map Summary Level © Innoval Technology Ltd IP07-047, Slide 25
  • 25. K-Map Case Study - Enthovens Pb Battery Recycling Actual Standard Operating Practice captured and agreed by all shifts for the Refinery. 14% increase in output. 3% reduction in fuel use. Improved Team Work throughout Plant. Currently using P-Map to compare Key Performance Indicators and develop “Best Practice” across 10 European sites. © Innoval Technology Ltd IP07-047, Slide 26
  • 26. Summary European extruders currently have a technical advantage To keep this advantage we need to Keep a robust manufacturing infrastructure Maintain high quality throughout the supply chain Invest in innovation and new technology Fund dynamic and exciting aluminium R&D programmes Manage highly qualified and innovative European nationals gary.mahon@innovaltec.com © Innoval Technology Ltd IP07-047, Slide 27