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Gypsum
Uses and Desirable Qualities of
Gypsum Products
 Gypsum:
 Mineral that is widely found in nature
 Ideal for making replicas of the patient’s mouth
 The replicas are called:
 Diagnostic casts (also called study models)
 Working casts (also called working models)
 Dies
 The production of gypsum casts requires meticulous attention to
detail.
 Inaccurate or incomplete casts are of little use to the dentist.
2
Properties and Behaviors of
Gypsum Products
 Chemical properties
Mineral gypsum = dihydrate of calcium sulfate
Ground to produce a powered hemihydrate
Model plaster: Commonly used for diagnostic casts (study
models)
Dental stone: Used for working casts (master casts)
Die stone
3
 The figure shows diagnostic casts made from
gypsum: a working cast with a stone base and a high-
strength stone anatomic portion, and a die made
from high-strength stone with metal plating.
Properties and Behaviors of
Gypsum Products
 Even though gypsum is always basically the same, different dental plasters
are formed according to how the material is processed.
 If the material is heated in open vats at approximately 115° C, the resulting
hemihydrate is porous and irregular in shape.
 This process will form model plaster.
 If the heating process is done under pressure, in the presence of steam
and at a higher temperature, a more uniformly shaped and less porous
form of hemihydrate is produced.
 This is referred to as dental stone.
 A further increase in pressure and heat will produce a material called die
stone.
Properties and Behaviors of
Gypsum Products
Physical properties
Main differences in physical forms dependent on
variations in size, shape, and porosity of the powders
Strength, hardness, and resistance to abrasion
Strength of gypsum products related to the amount of water
used to produce the study or working cast
6
Properties and Behaviors of
Gypsum Products
 Factors that affect the strength of gypsum products also
affect their hardness.
 Increased porosity of the particles makes it necessary to use
more water to convert the hemihydrate particles back to
dihydrate particles.
Properties and Behaviors of
Gypsum Products
Dimensional accuracy
Control setting expansion
Setting expansion occurs with all gypsum products.
Plaster has the highest rate of expansion.
Stones have the lowest rate of expansion.
Setting expansion is the result of growth of crystals as they join
together.
Some expansion is acceptable, but large amounts of expansion
will keep the end result from fitting.
It is important to control setting expansion.
8
Properties and Behaviors of Gypsum Products
 Reproduction of detail
 The greater the porosity of the final gypsum product, the less surface detail is
produced.
 Even products that have the least amount of porosity have surface
irregularities visible at the microscopic level.
 Solubility
 Set gypsum products are not highly soluble in water.
 Solubility is directly related to the porosity of the material; therefore plaster is
much more soluble than stone.
 Exposing models to water for prolonged periods should be avoided.
Classification of Gypsum Products
 The desired physical properties and the behavior necessary for a
particular use determine the criteria for selection of a gypsum
product.
 If you are pouring up diagnostic models, plaster is typically used.
 Impression plaster (type I)
 Rarely used today
 Model plaster (type II)
 Frequently used for diagnostic casts
 Durable but relatively weak material
10
Classification of Gypsum Products
 Dental stone (type III)
 Buff stone
 Ideal for making full or partial denture models, orthodontic models, and
casts
 usually used to make an appliance, such as orthodontic retainers,
whitening trays, sports guards, and partials.
 Dental stone, high-strength/low-expansion (type IV)
 Often referred to as die stones or densite
 Used to fabricate crowns and bridges
 Dental stone, high-strength/high-expansion (type V)
 Good to use with the newer base metals because of casting shrinkage
11
Manipulation of Gypsum Products
 Material selection
 Selection of a gypsum product should be based on the desired properties of the material.
 It is important that the mix have sufficient flow to reproduce details of the impression.
 Proportioning (water-to-powder ratio)
 Water should be measured with a graduated cylinder, and powder should be weighed on a
scale.
 Too much water will make the mix weak.
 Too little water, and the mix will not flow. Detail will be lost
 Mixing: Spatulation
 Most commonly, plaster and stone are mixed in a flexible rubber bowl with a broad metal
spatula.
 Mechanical devices are used when control of spatulation is critical.
12
 Initial setting time and working time
 The first step is to add the water to the bowl.
 Sift the powder into the water, and mix with a broad spatula and spatulate the material until smooth.
 It takes about 1 minute to mix the material thoroughly.
 After mixing for 1 minute, the working time begins.
 During this time, the semifluid mixture is poured into the impression with the help of a mechanical vibrator.
 After mixing, about 5 minutes of working time is available.
 As the viscosity of the mixture increases, the flow characteristics will be decreased and the product loses its
glossy appearance.
 This loss of gloss indicates that the gypsum has reached its initial set (8-16 minutes)
 Final setting time
 The final set is reached once the material is hard and the exothermic reaction cools completely.
 Most manufacturers recommend that about 1 hour should pass before the impression is separated from the cast.
 Gypsum products continue to harden and are two to three times harder after 24 hours
 If the impression is removed too soon, the model or teeth will break.
 If left too long, the impression will dry out (moisture absorbed by alginate) and will possibly snap off the teeth.
Manipulation of Gypsum Products
 Control of setting times:
 Altering the water-to-powder ratio
 Decrease water; decrease working time; more difficult to manipulate; air bubbles (only
when pouring base)
 Increase water; increase working time; weaker by 50%
 Spatulation
 Longer and more rapid; will also increase setting expansion
 Temperature
 Increase temp; decrease working time
 Accelerators and retarders
 It is impossible to accelerate the final set of a mixture without also accelerating
the initial set, thereby reducing the working time.
Manipulation of Gypsum Products
Fabricating and trimming
diagnostic/working casts
Diagnostic and working casts have two
parts:
Anatomic portion
replicates the hard and soft structures
Art portion
aids in handling and articulating the casts.
15
Manipulation of Gypsum Products
 The anatomic portion is poured by vibrating small increments of
flowable gypsum into the duplicated oral imprints.
 The mixture should be poured slowly in small increments under
vibration and allowed to flow from one tooth impression to the next,
pushing out air ahead of itself as it fills the entire impression, thus
eliminating air voids.
Double-Pour Technique
 Involves two separate mixes and two separate setting times.
 The anatomic portion of one or both arches is poured and is left in
the upright position.
 Approximately 10 minutes after the loss of gloss, a second mix is
produced for the art portion(s).
 This mixture is placed on a glass tile or in a base former.
 The filled impression is inverted onto the base, and the peripheries of
the two portions are joined.
Single-Step Method
 One mix of gypsum is produced to pour the anatomic and
art portions of the cast.
 After the impression is poured, the remaining material is
used for the base.
 This material is placed on a glass tile or in a base former, the
impression is inverted onto it, and the peripheries of the two
portions are joined.
Boxing Method
 A strip of wax is used to surround the impression,
forming a wall into which the gypsum is poured.
 The wax should not distort the impression.
 It should extend at least 0.5 inch higher than the
highest point of the impression and create a base that
is parallel to the occlusal plane.
 The figure shows pouring the art portion of a cast by
boxing; model former and inversion on patty base.
Manipulation of Gypsum Products
 Storage
Gypsum products can absorb water from the environment
Gypsum should be stored in airtight, moisture-proof containers
Humidity and close proximity to water sources will adversely affect
the powder.
20
Manipulation of Gypsum Products
 Cleanup
 Bowls, spatulas, mechanical vibrators, and mixing devices should be
cleaned of all traces of gypsum as soon as possible after manipulation
 Gypsum mixing and handling equipment must be kept
meticulously clean.
 Set gypsum will accelerate the setting times of a mixture.
21
Manipulation of Gypsum Products
 On setting of the gypsum, the impression, tray, and the cast
must be separated.
 When the impression is poured, care should be taken to
make sure the gypsum does not flow onto the tray, locking it
into the set gypsum.
 Separating the impression from the cast
Gently ease a lab knife under the impression tray and lift the tray
slightly in several areas
Care should be taken to not tilt too far in one direction or force the
impression and cast apart
Broken teeth may result
22
Manipulation of Gypsum Products
Infection control and safety issues
Routine disinfection of impressions should be done
in the dental office.
Disinfection of impressions is the best way to
prevent the introduction of contaminants into the
laboratory area.
Manipulation of Gypsum Products
 Trimming
Cast or study model
Models are trimmed with a model trimmer to produce an attractive,
symmetric model with easy access to all anatomic portions of the model and
a base of sufficient bulk for stability.
Bases made from dental stones should be soaked in water for 5 to 10
minutes before trimming to saturate the stone, making it easier to trim.
The cast should be trimmed so that proportionately the base makes up one
third and the anatomic portion two thirds of the total depth.
Model for whitening trays
Casts used to make whitening trays are trimmed down much further than
traditional casts and symmetry is not of concern with casts used to make
whitening trays.
24
Manipulation of Gypsum Products
 Metal-plated and epoxy dies and resin-reinforced die
stone
Type IV and V gypsum products are commonly used die
materials
Silver or copper plating can create metal-plated dies that are
highly resistant to abrasion
Type IV and V gypsum are very hard, but they are susceptible to
abrasion during carving of wax patterns.
25
Manipulation of Gypsum Products
Investment materials:
Used to form metal castings through the lost wax
technique
These materials, which combine gypsum and silica, are
able to produce models sufficiently strong to allow
molten metal to be poured into them.
26

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Chapter 16: Gypsum

  • 2. Uses and Desirable Qualities of Gypsum Products  Gypsum:  Mineral that is widely found in nature  Ideal for making replicas of the patient’s mouth  The replicas are called:  Diagnostic casts (also called study models)  Working casts (also called working models)  Dies  The production of gypsum casts requires meticulous attention to detail.  Inaccurate or incomplete casts are of little use to the dentist. 2
  • 3. Properties and Behaviors of Gypsum Products  Chemical properties Mineral gypsum = dihydrate of calcium sulfate Ground to produce a powered hemihydrate Model plaster: Commonly used for diagnostic casts (study models) Dental stone: Used for working casts (master casts) Die stone 3
  • 4.  The figure shows diagnostic casts made from gypsum: a working cast with a stone base and a high- strength stone anatomic portion, and a die made from high-strength stone with metal plating.
  • 5. Properties and Behaviors of Gypsum Products  Even though gypsum is always basically the same, different dental plasters are formed according to how the material is processed.  If the material is heated in open vats at approximately 115° C, the resulting hemihydrate is porous and irregular in shape.  This process will form model plaster.  If the heating process is done under pressure, in the presence of steam and at a higher temperature, a more uniformly shaped and less porous form of hemihydrate is produced.  This is referred to as dental stone.  A further increase in pressure and heat will produce a material called die stone.
  • 6. Properties and Behaviors of Gypsum Products Physical properties Main differences in physical forms dependent on variations in size, shape, and porosity of the powders Strength, hardness, and resistance to abrasion Strength of gypsum products related to the amount of water used to produce the study or working cast 6
  • 7. Properties and Behaviors of Gypsum Products  Factors that affect the strength of gypsum products also affect their hardness.  Increased porosity of the particles makes it necessary to use more water to convert the hemihydrate particles back to dihydrate particles.
  • 8. Properties and Behaviors of Gypsum Products Dimensional accuracy Control setting expansion Setting expansion occurs with all gypsum products. Plaster has the highest rate of expansion. Stones have the lowest rate of expansion. Setting expansion is the result of growth of crystals as they join together. Some expansion is acceptable, but large amounts of expansion will keep the end result from fitting. It is important to control setting expansion. 8
  • 9. Properties and Behaviors of Gypsum Products  Reproduction of detail  The greater the porosity of the final gypsum product, the less surface detail is produced.  Even products that have the least amount of porosity have surface irregularities visible at the microscopic level.  Solubility  Set gypsum products are not highly soluble in water.  Solubility is directly related to the porosity of the material; therefore plaster is much more soluble than stone.  Exposing models to water for prolonged periods should be avoided.
  • 10. Classification of Gypsum Products  The desired physical properties and the behavior necessary for a particular use determine the criteria for selection of a gypsum product.  If you are pouring up diagnostic models, plaster is typically used.  Impression plaster (type I)  Rarely used today  Model plaster (type II)  Frequently used for diagnostic casts  Durable but relatively weak material 10
  • 11. Classification of Gypsum Products  Dental stone (type III)  Buff stone  Ideal for making full or partial denture models, orthodontic models, and casts  usually used to make an appliance, such as orthodontic retainers, whitening trays, sports guards, and partials.  Dental stone, high-strength/low-expansion (type IV)  Often referred to as die stones or densite  Used to fabricate crowns and bridges  Dental stone, high-strength/high-expansion (type V)  Good to use with the newer base metals because of casting shrinkage 11
  • 12. Manipulation of Gypsum Products  Material selection  Selection of a gypsum product should be based on the desired properties of the material.  It is important that the mix have sufficient flow to reproduce details of the impression.  Proportioning (water-to-powder ratio)  Water should be measured with a graduated cylinder, and powder should be weighed on a scale.  Too much water will make the mix weak.  Too little water, and the mix will not flow. Detail will be lost  Mixing: Spatulation  Most commonly, plaster and stone are mixed in a flexible rubber bowl with a broad metal spatula.  Mechanical devices are used when control of spatulation is critical. 12
  • 13.  Initial setting time and working time  The first step is to add the water to the bowl.  Sift the powder into the water, and mix with a broad spatula and spatulate the material until smooth.  It takes about 1 minute to mix the material thoroughly.  After mixing for 1 minute, the working time begins.  During this time, the semifluid mixture is poured into the impression with the help of a mechanical vibrator.  After mixing, about 5 minutes of working time is available.  As the viscosity of the mixture increases, the flow characteristics will be decreased and the product loses its glossy appearance.  This loss of gloss indicates that the gypsum has reached its initial set (8-16 minutes)  Final setting time  The final set is reached once the material is hard and the exothermic reaction cools completely.  Most manufacturers recommend that about 1 hour should pass before the impression is separated from the cast.  Gypsum products continue to harden and are two to three times harder after 24 hours  If the impression is removed too soon, the model or teeth will break.  If left too long, the impression will dry out (moisture absorbed by alginate) and will possibly snap off the teeth.
  • 14. Manipulation of Gypsum Products  Control of setting times:  Altering the water-to-powder ratio  Decrease water; decrease working time; more difficult to manipulate; air bubbles (only when pouring base)  Increase water; increase working time; weaker by 50%  Spatulation  Longer and more rapid; will also increase setting expansion  Temperature  Increase temp; decrease working time  Accelerators and retarders  It is impossible to accelerate the final set of a mixture without also accelerating the initial set, thereby reducing the working time.
  • 15. Manipulation of Gypsum Products Fabricating and trimming diagnostic/working casts Diagnostic and working casts have two parts: Anatomic portion replicates the hard and soft structures Art portion aids in handling and articulating the casts. 15
  • 16. Manipulation of Gypsum Products  The anatomic portion is poured by vibrating small increments of flowable gypsum into the duplicated oral imprints.  The mixture should be poured slowly in small increments under vibration and allowed to flow from one tooth impression to the next, pushing out air ahead of itself as it fills the entire impression, thus eliminating air voids.
  • 17. Double-Pour Technique  Involves two separate mixes and two separate setting times.  The anatomic portion of one or both arches is poured and is left in the upright position.  Approximately 10 minutes after the loss of gloss, a second mix is produced for the art portion(s).  This mixture is placed on a glass tile or in a base former.  The filled impression is inverted onto the base, and the peripheries of the two portions are joined.
  • 18. Single-Step Method  One mix of gypsum is produced to pour the anatomic and art portions of the cast.  After the impression is poured, the remaining material is used for the base.  This material is placed on a glass tile or in a base former, the impression is inverted onto it, and the peripheries of the two portions are joined.
  • 19. Boxing Method  A strip of wax is used to surround the impression, forming a wall into which the gypsum is poured.  The wax should not distort the impression.  It should extend at least 0.5 inch higher than the highest point of the impression and create a base that is parallel to the occlusal plane.  The figure shows pouring the art portion of a cast by boxing; model former and inversion on patty base.
  • 20. Manipulation of Gypsum Products  Storage Gypsum products can absorb water from the environment Gypsum should be stored in airtight, moisture-proof containers Humidity and close proximity to water sources will adversely affect the powder. 20
  • 21. Manipulation of Gypsum Products  Cleanup  Bowls, spatulas, mechanical vibrators, and mixing devices should be cleaned of all traces of gypsum as soon as possible after manipulation  Gypsum mixing and handling equipment must be kept meticulously clean.  Set gypsum will accelerate the setting times of a mixture. 21
  • 22. Manipulation of Gypsum Products  On setting of the gypsum, the impression, tray, and the cast must be separated.  When the impression is poured, care should be taken to make sure the gypsum does not flow onto the tray, locking it into the set gypsum.  Separating the impression from the cast Gently ease a lab knife under the impression tray and lift the tray slightly in several areas Care should be taken to not tilt too far in one direction or force the impression and cast apart Broken teeth may result 22
  • 23. Manipulation of Gypsum Products Infection control and safety issues Routine disinfection of impressions should be done in the dental office. Disinfection of impressions is the best way to prevent the introduction of contaminants into the laboratory area.
  • 24. Manipulation of Gypsum Products  Trimming Cast or study model Models are trimmed with a model trimmer to produce an attractive, symmetric model with easy access to all anatomic portions of the model and a base of sufficient bulk for stability. Bases made from dental stones should be soaked in water for 5 to 10 minutes before trimming to saturate the stone, making it easier to trim. The cast should be trimmed so that proportionately the base makes up one third and the anatomic portion two thirds of the total depth. Model for whitening trays Casts used to make whitening trays are trimmed down much further than traditional casts and symmetry is not of concern with casts used to make whitening trays. 24
  • 25. Manipulation of Gypsum Products  Metal-plated and epoxy dies and resin-reinforced die stone Type IV and V gypsum products are commonly used die materials Silver or copper plating can create metal-plated dies that are highly resistant to abrasion Type IV and V gypsum are very hard, but they are susceptible to abrasion during carving of wax patterns. 25
  • 26. Manipulation of Gypsum Products Investment materials: Used to form metal castings through the lost wax technique These materials, which combine gypsum and silica, are able to produce models sufficiently strong to allow molten metal to be poured into them. 26

Notas do Editor

  1. Refer students to Procedures 16-2 and 16-3 (pp. 293-295 in the textbook).
  2. Refer the students to Procedure 16-4 (pp. 295-296 in the textbook).
  3. Refer students to Procedure 16-6 (pp. 298-299 in the textbook).