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International INTERNATIONAL Journal of Mechanical JOURNAL Engineering OF and MECHANICAL Technology (IJMET), ISSN ENGINEERING 
0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
AND TECHNOLOGY (IJMET) 
ISSN 0976 – 6340 (Print) 
ISSN 0976 – 6359 (Online) 
Volume 5, Issue 7, July (2014), pp. 184-192 
© IAEME: www.iaeme.com/IJMET.asp 
Journal Impact Factor (2014): 7.5377 (Calculated by GISI) 
www.jifactor.com 
184 
 
IJMET 
© I A E M E 
EXPERIMENT INVESTIGATION OF EDM PARAMETER MRR AND TWR 
WITH MULTI WALL CARBON NANO TUBES 
Prof. Yashesh Darji1, Prof. Pankaj L Koradiya2, Prof. Jigesh R.Shah3 
1, 2(C U Shah College of Engineering  Technology, Mechanical Department, 
Wadhwancity surendranagar, Gujarat, India) 
3(C U Shah College of Engineering  Technology, Automobile Department, 
Wadhwancity surendranagar, Gujarat, India) 
ABSTRACT 
Electric discharge machining is non conventional machining process used for machining of 
hard materials which cannot be machined by conventional machining process. Electric discharge 
machining is an electro sparking method of metal working involving an electric erosion effect. A 
pulse discharge occurs in a small gap between the work piece and the electrode and removes the 
unwanted material from the parent metal through melting and vaporizing. 
Powder-mixed electrical discharge machining is one of the latest techniques for improving 
material removal rate and also decreased tool wear ratio, How ever its utilization in the 
manufacturing industry is very low because many fundamental issues of this new development such 
as machining mechanism cost effectiveness of powder and powder concentration in the working 
fluid together with safety and environmental impact among other are not well understood. 
This work investigation the machining characteristics of EN-31 with aluminum as tool 
electrode during EDM process, The multi wall carbon nano tube is mixed with dielectric fluids in 
EDM process to analyze the MRR, TWR. Regression model were developed to predict the out put 
parameter in EDM process. In the development of predictive models, machining parameter of peak 
current, pulse on time and pulse off time were considered as model variables. The collection of 
experimental data adopted full factorial method. Analysis of variance (ANOVA) to determine the 
significant parameter affecting the out put parameter. Later EN-31 steel was analyzed and the 
parameters are optimized using design expert software, regression equations are compared with and 
without MWCNT using EDM process. The average 19% of MRR was improved where TWR was 
8.51% decreased with respect to input parameter. 
Keywords: Electrical discharge machining (EDM), Carbon nanotubes (CNT), Material removal rate, 
tool wear rate, full factorial method, Regression Analysis.
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
185 
INTRODUCTION 
 
Electrical discharge machining (EDM) is one of the most successful and widely accepted 
processes for production of complicated shapes and tiny apertures with high accuracy. This method 
is commonly used for profile truing of metal bond diamond wheel, micro nozzle fabrication, drilling 
of composites and manufacturing of moulds, and dies in hardened steels. These hard and brittle 
materials fabricated by conventional machining operation cause excessive tool wear and expense. 
The mechanical properties of tool steels have been studied extensively for many years. During EDM, 
the tool and the work piece are separated by a small gap, and submerged in dielectric fluid. The 
discharge energy produces very high temperatures on the surface of the work piece at the point of the 
spark. The specimen is subject to a temperature rise of up to 40,000 K causing a minute part of the 
work piece to be melted and vaporized. The top surface of work piece subsequently resolidifies and 
cools at very high rate. EDM technology is increasingly being used in tool, die and mould making 
industries, for machining of heat treated tool steels and advanced materials (super alloys, ceramics 
and metal matrix composites) requiring high precision, complex shapes and high surface finish. 
Traditional machining technique is often based on the material removal  tool wear rate. carbon 
nanotubes (CNTs). Ozlem and Cengiz (2008) pro-posed roughness values obtained from the 
experiments that have been modeled by using the genetic expression programming (GEP) method 
and a mathematical relationship has been suggested between the GEP model and SR and parameters 
affecting it. Moreover, EDM has been used by applying copper, copper–tungsten (W–Cu) and 
graphite electrodes to the same material with experimental parameters designed in accordance with 
the Taguchi method. Yan-Cherng et al. (2009) developed the force assisted standard EDM machine. 
The effects of magnetic force on EDM machining characteristics were explored. Moreover, this work 
adopted an L18 orthogonal array based on Taguchi method to conduct a series of experiments and 
statistically evaluated the experimental data by analysis of variance (ANOVA). Ko-Ta et al. (2007) 
proposed a methodology for modeling and analysis of the rapidly resolidified layer of spheroidal 
graphite (SG) cast iron in the EDM process using the response surface methodology. The results of 
ANOVA indicate that the proposed mathematical model obtained can adequately describes the 
performance within the limits of the factors being studied. 
ABOUT CARBON NANO TUBE 
CNTs are related to graphite. The molecular structure of graphite resembles stacked, one-atom- 
thick sheets of chicken wire, a planar network of interconnected hexagonal rings of carbon 
atoms. In conventional graphite, the sheets of carbon are stacked on top of one another, allowing 
them to easily slide over each other. That is why graphite is not hard, but it feels greasy and can be 
used as a lubricant. When grapheme sheets are rolled into a cylinder and their edges joined, they 
form MWCNT (Table 3). Only the tangents of the graphitic planes come into contact with each 
other, and hence their properties are more like those of a molecule as mentioned in the above passage 
clearly. Furthermore, the high-frequency carbon-carbon bond vibrations provide an intrinsic thermal 
conductivity higher than even diamond. The TEM images of multi wall carbon nano tubes are shown 
in Figure 1 were received from Cheap tubes Inc., USA. CNT nano fluids, is of special interests to 
researchers because of the novel properties of CNTs -extraordinary strength, unique electrical 
properties and efficient conductors of heat. CNTs are fullerene-related structures that consist of 
either a grapheme cylinder or a number of concentric cylinders (Wen and Ding, 2004). Choi et al. 
(2001) measured the effective thermal conductivity of MWCNTs dispersed in synthetic (poly-- 
olefin) oil and reported the enhancement up to a 150% in conductivity at approximately 1 vol% 
CNT, which is by far the highest thermal conductivity enhancement ever achieved in a liquid 
(Lockwood and Zhang, 2005). Solid lubricants are useful for conditions when conventional liquid
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
lubricants are inadequate such as high temperature and extreme contact pressures. Their lubricating 
properties are attributed to a layered structure on the molecular level with weak bonding between 
layers. Such layers are able to slide relative to each other with minimal applied force, thus giving 
them their low friction properties. CNT is having high strength to weight ratio used in aero space 
industry. Young’s modulus of CNT is over 1 TPa versus 70 GPa for aluminium, steel 200 Gpa and 
700 GPa for C-fibre. The strength to weight ratio is 500 times greater than aluminium. Maximum 
strain will be 10% much higher than any material. Thermal conductivity of 3,000 W/mK in the axial 
direction is with small values in the radial direction. Conductivity of CNTs is 109 A/cm2 and copper 
is 106 A/cm2. CNT’s having very high current carrying capacity, excellent field emitter and high 
aspect ratio. Model Hommel Tester TR500 SR tester is a multi-application measuring instrument for 
component surface quality evaluation. It is capable of checking the work piece SR on plane, cylinder, 
groove and bearing raceway. 
186 
 
In this paper, CNT mixed dielectric fluids are used in the EDM process to analyze the EDM 
parameter like MRR  TWR of EN-31 tool steel material. Till now, no work has been carried out by 
using CNT mixed dielectric machining. CNT based nano fluid is used to improve the Material 
removal rate  tool wear rate The collection of experimental data adopted Full Factorial using Table 
5 coded level of three machining parameters. ANOVA and regression model and to determine the 
significant parameter affecting the Material removal rate and tool wear rate Later the En-31 tool steel 
was analyzed and the parameters are optimized using design expert software and regression equation 
are compared with and without multiwall carbon nanotubes used in EDM process. 
Figure 1: Micro structure of CNT 
DIELECTRIC CYCLING SYSTEM 
Due to the larger size of the in built container in the EDM machine, it is not appropriate to 
mix the powder in the bigger container. So we need to design the container to avoid the mixing of 
powder particles in the bigger container of the machine. More over, filter of machine might clog due 
to presence of powder particles and debris when using existing circulation system of machine itself. 
So a new container with capacity of 6.0 liters was developed in the workshop for the dielectric fluid. 
It was placed in the existing container of EDM machine and experiments were performed in this 
container. Special types of two stirrers are fixing with proto type new tank for proper circulation of 
powder mixed dielectric fluid into discharge gap between tool electrode and work piece material, 
Mixed 0.5 g/l CNT in dielectric fluid, Fig 2 show the mechanism of proto type tank and Fig 3 shown 
the proto type tank is using in EDM machine.
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
 
187 
 
Figure 2: double stirrers for powder circulation 
Figure 3: EDM with proto type tank 
Evaluation of MRR 
The material MRR is expressed as the ratio of the difference of weight of the work piece 
before and after machining to the machining time and density of the material. 
MRR = 
 
Whereas Wjb = Weight of work piece before machining. 
Wja = Weight of work piece after machining. 
t = Machining time 
 = Density of EN-31 steel material 
Evaluation of tool wear rate 
TWR is expressed as the ratio of the difference of weight of the tool before and after 
machining to the machining time. That can be explaining this equation. 
TWR =
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
Whereas Wtb = Weight of the tool before machining. 
188 
 
Wta = Weight of the tool after machining. 
t = Machining time. 
Conduct of Experiments 
The work piece material as EN-31 was particulate using Aluminum tool with 15 mm 
diameter and work piece dimension were 30 x 30 x 30 mm square cube. JOEMARS - Made: Z 50 
JM-322 EDM machine was used for conducting experiment. Commercial kerosene and also 
MWCNT mixed kerosene used as dielectric fluid. In this experiment three EDM parameters such 
as pulse on time, pulse off time and peak current are varied at three levels of each. For a three factor 
are tackled with a total number of 27 experiments performed on die sinking EDM. Three responses 
such as material removal rate and surface roughness and tool were ratios are measure as output 
parameters. The material removal rate and tool were ratio are calculated by using weight machine 
having the capacity of 200 gram and accuracy is 0.01 gram. 
RESULTS AND DISCUSSION 
Table 3: Comparison of regression model with experiment measurements 
Sr 
no 
With CNTs MRR Without CNTs MRR 
With CNTs TWR Without CNTs MRR 
Experiment 
data 
Regression 
data 
Experiment 
data 
Regression 
data 
Experiment 
data 
Regression 
data 
Experiment 
data 
Regression 
data 
1 20.528 19.120 17.363 16.025 1.967 1.755 2.129 1.896 
2 58.977 52.600 49.407 43.799 6.451 6.371 6.962 6.913 
3 45.026 43.809 37.885 36.630 5.03 5.684 5.438 6.173 
4 23.925 21.362 19.867 18.111 3.294 3.059 3.591 3.332 
5 34.093 32.799 27.996 27.387 4.507 3.705 4.882 4.017 
6 22.506 24.637 19.127 20.653 2.647 2.750 2.871 2.984 
7 24.413 24.008 20.649 20.218 3.271 3.018 3.529 3.277 
8 16.064 14.725 13.503 12.441 0.956 1.411 1.045 1.526 
9 21.696 22.887 18.197 19.175 2.654 2.366 2.886 2.559 
10 26.480 27.283 21.968 22.759 2.723 2.709 2.931 2.929 
11 46.854 42.688 38.611 35.587 4.867 5.032 5.262 5.455 
12 38.897 37.172 32.261 30.960 3.531 4.037 3.826 4.367 
13 13.539 10.329 11.535 8.8571 1.165 1.068 1.258 1.157 
14 30.198 33.920 25.566 28.430 4.661 4.357 5.092 4.735 
15 40.150 41.567 33.414 34.544 3.907 4.380 4.189 4.737 
16 35.386 38.3161 29.789 32.014 5.264 4.700 5.727 5.105 
17 18.822 15.846 15.974 13.484 1.953 2.063 2.124 2.244 
18 26.237 25.758 22.254 21.696 2.11 3.402 2.257 3.702 
19 19.110 18.492 16.044 15.591 2.724 2.023 2.956 2.189 
20 27.983 30.153 23.292 25.280 2.855 3.745 3.126 4.072 
21 21.232 20.241 17.853 17.068 1.898 2.407 2.056 2.614 
22 29.156 32.776 24.63 27.375 3.001 3.694 3.257 3.997 
23 45.055 47.084 37.49 39.171 5.645 5.375 6.148 5.825 
24 52.084 48.205 43.038 40.214 6.39 6.027 6.985 6.543 
25 25.101 29.525 21.108 24.845 4.489 4.013 4.881 4.365 
26 32.947 38.293 27.636 32.003 4.86 4.689 5.273 5.085 
27 25.541 28.404 21.675 23.802 4.396 3.361 4.779 3.647
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
189 
 
Design-Expert® Software 
MRR 
X1 = A: peak current 
X2 = B: pulse on time 
Actual Factor 
C: pulse off time = 30 
A: B: pulse on time peak current 
17 
21 
28 
45 
55 
65 
45 
37.75 
30.5 
23.25 
16 
MRR 
Design-Expert® Software 
MRR 
X1 = A: peak current 
X2 = B: pulse on time 
Actual Factor 
C: pulse off time = 60 
B: pulse on time A: peak current 
17 
21 
28 
45 
55 
65 
38 
30.75 
23.5 
16.25 
9 
MRR 
Fig 4 Graph of without CNT for MRR Fig 5 Graph of with CNT for MRR 
Effect of carbon nano tube on MRR 
The mean MRR for CNT + kerosene was 58.977 mm3/min and that of pure kerosene was 
49.407 mm3/min at 28A and pulse on time 65 micro sec. and pulse off time 30 micro sec. The 
experimental results show that the CNT powder concentration of 0.5 g/l .high concentrations of CNT 
powder in the gap often made the EDM process unstable. ”c.mai. Hong et. [25] It is observed from 
the graph the MRR is increase with respect to increase in Peak current and pulse on time. This 
increase of MRR with concentration could be attributed in kerosene. Spark gap is filled with additive 
particles which reduces the insulating strength of the dielectric fluid and increased spark gap between 
the tool and work piece. It was also possible that the best combination of particle striking and powder 
density take place at this concentration. 
Design-Expert® Software 
twr cnt 
X1 = A: peak current 
X2 = B: pulse on time 
Actual Factor 
C: pulse off time = 30 
B: pulse on time A: peak current 
17 
21 
28 
45 
55 
65 
6.2 
5 
3.8 
2.6 
1.4 
twr cnt 
Design-Expert® Software 
twr cnt 
X1 = A: peak current 
X2 = B: pulse on time 
Actual Factor 
C: pulse off time = 60 
B: pulse on time A: peak current 
17 
21 
28 
45 
55 
65 
5.5 
4.3 
3.1 
1.9 
0.7 
twr cnt 
Fig 6 Graph of without CNT for TWR Fig 7 Graph of with CNT for TWR 
Effect of carbon nano tube on TWR 
The means TWR for CNT + kerosene was 0.956mm3/min and that of pure kerosene was 
1.045mm3/min at 17A and pulse on time 45 micro sec. and pulse of time 45 micro sec. The 
experimental results show that the CNT powder concentration of 0.5 g/l. It is clear from the graph 
that the peak current and pulse on time and CNT concentration are the main influencing factor in the 
tool wear rate. Pulse off time and polarity are less influencing factor for tool wear rate .when CNT 
mixed with kerosene than created lubricant layer around tool and work piece this mixer keep cool 
the electrode and that’s why the tool wear rate is decrease.
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
190 
CONCLUSION 
 
 Process parameters do not have same effect for every response. Significant parameters and its 
percentage contribution changes as per the behavior of the parameter with objective response 
 Finding the result of MRR the most significant factor was found to be peak current followed 
by pulse on time and the least significant was pulse off time. The MRR increased linearly 
with the increase in current. For pulse on time the MRR first increased with linearly with 
increase in pulse off time, MRR decreased insignificantly. 
 In the case of Tool wear rate the most important factor is peak current then pulse on time and 
after that pulse off time. 
 Effect of carbon nano tube on MRR for CNT + kerosene was 58.977 mm3/min and that of 
pure kerosene was 49.407 mm3/min from experimental result with carbon nano tube the 
average 19% of MRR increased with respect to input parameter. 
 Effect of carbon nano tube on TWR for CNT + kerosene was 0.956mm3/min and that of pure 
kerosene was 1.045mm3/min from experimental result with carbon nano tube the average 
8.51% of TWR decreased with respect to input parameter. 
Table 1: Major properties of EN-31  Chemical Composition and grades: GCr15, 102Cr6, 
L1/L3/52100, SUJ2 
Material Thermal conductivity 
(W/mk) 
Density (g/cc) Electrical 
resistivity 
Specific heat 
capacity 
(J/g-‘c) 
EN-31 46.6 7.81 o.oooo218 0.475 
C si Mn Cr p V Fe 
1.07 0.32 0.58 0.03 0.04 1.12 Balance 
Table 2: specification of MWCNT 
Aspect Ratio ˜1000 
Specific Surface Area 350 m2/g 
Purity –wt% 95% 
Metallic Impurity 5% 
Average outer Diameter 20-40nm 
Average inner diameter 5 nm 
Number of Walls 5-15 
Length 50μm
International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), 
ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 
191 
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Experiment investigation of edm parameter mrr and twr with multi wall carbon

  • 1. International INTERNATIONAL Journal of Mechanical JOURNAL Engineering OF and MECHANICAL Technology (IJMET), ISSN ENGINEERING 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME AND TECHNOLOGY (IJMET) ISSN 0976 – 6340 (Print) ISSN 0976 – 6359 (Online) Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME: www.iaeme.com/IJMET.asp Journal Impact Factor (2014): 7.5377 (Calculated by GISI) www.jifactor.com 184 IJMET © I A E M E EXPERIMENT INVESTIGATION OF EDM PARAMETER MRR AND TWR WITH MULTI WALL CARBON NANO TUBES Prof. Yashesh Darji1, Prof. Pankaj L Koradiya2, Prof. Jigesh R.Shah3 1, 2(C U Shah College of Engineering Technology, Mechanical Department, Wadhwancity surendranagar, Gujarat, India) 3(C U Shah College of Engineering Technology, Automobile Department, Wadhwancity surendranagar, Gujarat, India) ABSTRACT Electric discharge machining is non conventional machining process used for machining of hard materials which cannot be machined by conventional machining process. Electric discharge machining is an electro sparking method of metal working involving an electric erosion effect. A pulse discharge occurs in a small gap between the work piece and the electrode and removes the unwanted material from the parent metal through melting and vaporizing. Powder-mixed electrical discharge machining is one of the latest techniques for improving material removal rate and also decreased tool wear ratio, How ever its utilization in the manufacturing industry is very low because many fundamental issues of this new development such as machining mechanism cost effectiveness of powder and powder concentration in the working fluid together with safety and environmental impact among other are not well understood. This work investigation the machining characteristics of EN-31 with aluminum as tool electrode during EDM process, The multi wall carbon nano tube is mixed with dielectric fluids in EDM process to analyze the MRR, TWR. Regression model were developed to predict the out put parameter in EDM process. In the development of predictive models, machining parameter of peak current, pulse on time and pulse off time were considered as model variables. The collection of experimental data adopted full factorial method. Analysis of variance (ANOVA) to determine the significant parameter affecting the out put parameter. Later EN-31 steel was analyzed and the parameters are optimized using design expert software, regression equations are compared with and without MWCNT using EDM process. The average 19% of MRR was improved where TWR was 8.51% decreased with respect to input parameter. Keywords: Electrical discharge machining (EDM), Carbon nanotubes (CNT), Material removal rate, tool wear rate, full factorial method, Regression Analysis.
  • 2. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 185 INTRODUCTION Electrical discharge machining (EDM) is one of the most successful and widely accepted processes for production of complicated shapes and tiny apertures with high accuracy. This method is commonly used for profile truing of metal bond diamond wheel, micro nozzle fabrication, drilling of composites and manufacturing of moulds, and dies in hardened steels. These hard and brittle materials fabricated by conventional machining operation cause excessive tool wear and expense. The mechanical properties of tool steels have been studied extensively for many years. During EDM, the tool and the work piece are separated by a small gap, and submerged in dielectric fluid. The discharge energy produces very high temperatures on the surface of the work piece at the point of the spark. The specimen is subject to a temperature rise of up to 40,000 K causing a minute part of the work piece to be melted and vaporized. The top surface of work piece subsequently resolidifies and cools at very high rate. EDM technology is increasingly being used in tool, die and mould making industries, for machining of heat treated tool steels and advanced materials (super alloys, ceramics and metal matrix composites) requiring high precision, complex shapes and high surface finish. Traditional machining technique is often based on the material removal tool wear rate. carbon nanotubes (CNTs). Ozlem and Cengiz (2008) pro-posed roughness values obtained from the experiments that have been modeled by using the genetic expression programming (GEP) method and a mathematical relationship has been suggested between the GEP model and SR and parameters affecting it. Moreover, EDM has been used by applying copper, copper–tungsten (W–Cu) and graphite electrodes to the same material with experimental parameters designed in accordance with the Taguchi method. Yan-Cherng et al. (2009) developed the force assisted standard EDM machine. The effects of magnetic force on EDM machining characteristics were explored. Moreover, this work adopted an L18 orthogonal array based on Taguchi method to conduct a series of experiments and statistically evaluated the experimental data by analysis of variance (ANOVA). Ko-Ta et al. (2007) proposed a methodology for modeling and analysis of the rapidly resolidified layer of spheroidal graphite (SG) cast iron in the EDM process using the response surface methodology. The results of ANOVA indicate that the proposed mathematical model obtained can adequately describes the performance within the limits of the factors being studied. ABOUT CARBON NANO TUBE CNTs are related to graphite. The molecular structure of graphite resembles stacked, one-atom- thick sheets of chicken wire, a planar network of interconnected hexagonal rings of carbon atoms. In conventional graphite, the sheets of carbon are stacked on top of one another, allowing them to easily slide over each other. That is why graphite is not hard, but it feels greasy and can be used as a lubricant. When grapheme sheets are rolled into a cylinder and their edges joined, they form MWCNT (Table 3). Only the tangents of the graphitic planes come into contact with each other, and hence their properties are more like those of a molecule as mentioned in the above passage clearly. Furthermore, the high-frequency carbon-carbon bond vibrations provide an intrinsic thermal conductivity higher than even diamond. The TEM images of multi wall carbon nano tubes are shown in Figure 1 were received from Cheap tubes Inc., USA. CNT nano fluids, is of special interests to researchers because of the novel properties of CNTs -extraordinary strength, unique electrical properties and efficient conductors of heat. CNTs are fullerene-related structures that consist of either a grapheme cylinder or a number of concentric cylinders (Wen and Ding, 2004). Choi et al. (2001) measured the effective thermal conductivity of MWCNTs dispersed in synthetic (poly-- olefin) oil and reported the enhancement up to a 150% in conductivity at approximately 1 vol% CNT, which is by far the highest thermal conductivity enhancement ever achieved in a liquid (Lockwood and Zhang, 2005). Solid lubricants are useful for conditions when conventional liquid
  • 3. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME lubricants are inadequate such as high temperature and extreme contact pressures. Their lubricating properties are attributed to a layered structure on the molecular level with weak bonding between layers. Such layers are able to slide relative to each other with minimal applied force, thus giving them their low friction properties. CNT is having high strength to weight ratio used in aero space industry. Young’s modulus of CNT is over 1 TPa versus 70 GPa for aluminium, steel 200 Gpa and 700 GPa for C-fibre. The strength to weight ratio is 500 times greater than aluminium. Maximum strain will be 10% much higher than any material. Thermal conductivity of 3,000 W/mK in the axial direction is with small values in the radial direction. Conductivity of CNTs is 109 A/cm2 and copper is 106 A/cm2. CNT’s having very high current carrying capacity, excellent field emitter and high aspect ratio. Model Hommel Tester TR500 SR tester is a multi-application measuring instrument for component surface quality evaluation. It is capable of checking the work piece SR on plane, cylinder, groove and bearing raceway. 186 In this paper, CNT mixed dielectric fluids are used in the EDM process to analyze the EDM parameter like MRR TWR of EN-31 tool steel material. Till now, no work has been carried out by using CNT mixed dielectric machining. CNT based nano fluid is used to improve the Material removal rate tool wear rate The collection of experimental data adopted Full Factorial using Table 5 coded level of three machining parameters. ANOVA and regression model and to determine the significant parameter affecting the Material removal rate and tool wear rate Later the En-31 tool steel was analyzed and the parameters are optimized using design expert software and regression equation are compared with and without multiwall carbon nanotubes used in EDM process. Figure 1: Micro structure of CNT DIELECTRIC CYCLING SYSTEM Due to the larger size of the in built container in the EDM machine, it is not appropriate to mix the powder in the bigger container. So we need to design the container to avoid the mixing of powder particles in the bigger container of the machine. More over, filter of machine might clog due to presence of powder particles and debris when using existing circulation system of machine itself. So a new container with capacity of 6.0 liters was developed in the workshop for the dielectric fluid. It was placed in the existing container of EDM machine and experiments were performed in this container. Special types of two stirrers are fixing with proto type new tank for proper circulation of powder mixed dielectric fluid into discharge gap between tool electrode and work piece material, Mixed 0.5 g/l CNT in dielectric fluid, Fig 2 show the mechanism of proto type tank and Fig 3 shown the proto type tank is using in EDM machine.
  • 4. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 187 Figure 2: double stirrers for powder circulation Figure 3: EDM with proto type tank Evaluation of MRR The material MRR is expressed as the ratio of the difference of weight of the work piece before and after machining to the machining time and density of the material. MRR = Whereas Wjb = Weight of work piece before machining. Wja = Weight of work piece after machining. t = Machining time = Density of EN-31 steel material Evaluation of tool wear rate TWR is expressed as the ratio of the difference of weight of the tool before and after machining to the machining time. That can be explaining this equation. TWR =
  • 5. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME Whereas Wtb = Weight of the tool before machining. 188 Wta = Weight of the tool after machining. t = Machining time. Conduct of Experiments The work piece material as EN-31 was particulate using Aluminum tool with 15 mm diameter and work piece dimension were 30 x 30 x 30 mm square cube. JOEMARS - Made: Z 50 JM-322 EDM machine was used for conducting experiment. Commercial kerosene and also MWCNT mixed kerosene used as dielectric fluid. In this experiment three EDM parameters such as pulse on time, pulse off time and peak current are varied at three levels of each. For a three factor are tackled with a total number of 27 experiments performed on die sinking EDM. Three responses such as material removal rate and surface roughness and tool were ratios are measure as output parameters. The material removal rate and tool were ratio are calculated by using weight machine having the capacity of 200 gram and accuracy is 0.01 gram. RESULTS AND DISCUSSION Table 3: Comparison of regression model with experiment measurements Sr no With CNTs MRR Without CNTs MRR With CNTs TWR Without CNTs MRR Experiment data Regression data Experiment data Regression data Experiment data Regression data Experiment data Regression data 1 20.528 19.120 17.363 16.025 1.967 1.755 2.129 1.896 2 58.977 52.600 49.407 43.799 6.451 6.371 6.962 6.913 3 45.026 43.809 37.885 36.630 5.03 5.684 5.438 6.173 4 23.925 21.362 19.867 18.111 3.294 3.059 3.591 3.332 5 34.093 32.799 27.996 27.387 4.507 3.705 4.882 4.017 6 22.506 24.637 19.127 20.653 2.647 2.750 2.871 2.984 7 24.413 24.008 20.649 20.218 3.271 3.018 3.529 3.277 8 16.064 14.725 13.503 12.441 0.956 1.411 1.045 1.526 9 21.696 22.887 18.197 19.175 2.654 2.366 2.886 2.559 10 26.480 27.283 21.968 22.759 2.723 2.709 2.931 2.929 11 46.854 42.688 38.611 35.587 4.867 5.032 5.262 5.455 12 38.897 37.172 32.261 30.960 3.531 4.037 3.826 4.367 13 13.539 10.329 11.535 8.8571 1.165 1.068 1.258 1.157 14 30.198 33.920 25.566 28.430 4.661 4.357 5.092 4.735 15 40.150 41.567 33.414 34.544 3.907 4.380 4.189 4.737 16 35.386 38.3161 29.789 32.014 5.264 4.700 5.727 5.105 17 18.822 15.846 15.974 13.484 1.953 2.063 2.124 2.244 18 26.237 25.758 22.254 21.696 2.11 3.402 2.257 3.702 19 19.110 18.492 16.044 15.591 2.724 2.023 2.956 2.189 20 27.983 30.153 23.292 25.280 2.855 3.745 3.126 4.072 21 21.232 20.241 17.853 17.068 1.898 2.407 2.056 2.614 22 29.156 32.776 24.63 27.375 3.001 3.694 3.257 3.997 23 45.055 47.084 37.49 39.171 5.645 5.375 6.148 5.825 24 52.084 48.205 43.038 40.214 6.39 6.027 6.985 6.543 25 25.101 29.525 21.108 24.845 4.489 4.013 4.881 4.365 26 32.947 38.293 27.636 32.003 4.86 4.689 5.273 5.085 27 25.541 28.404 21.675 23.802 4.396 3.361 4.779 3.647
  • 6. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 189 Design-Expert® Software MRR X1 = A: peak current X2 = B: pulse on time Actual Factor C: pulse off time = 30 A: B: pulse on time peak current 17 21 28 45 55 65 45 37.75 30.5 23.25 16 MRR Design-Expert® Software MRR X1 = A: peak current X2 = B: pulse on time Actual Factor C: pulse off time = 60 B: pulse on time A: peak current 17 21 28 45 55 65 38 30.75 23.5 16.25 9 MRR Fig 4 Graph of without CNT for MRR Fig 5 Graph of with CNT for MRR Effect of carbon nano tube on MRR The mean MRR for CNT + kerosene was 58.977 mm3/min and that of pure kerosene was 49.407 mm3/min at 28A and pulse on time 65 micro sec. and pulse off time 30 micro sec. The experimental results show that the CNT powder concentration of 0.5 g/l .high concentrations of CNT powder in the gap often made the EDM process unstable. ”c.mai. Hong et. [25] It is observed from the graph the MRR is increase with respect to increase in Peak current and pulse on time. This increase of MRR with concentration could be attributed in kerosene. Spark gap is filled with additive particles which reduces the insulating strength of the dielectric fluid and increased spark gap between the tool and work piece. It was also possible that the best combination of particle striking and powder density take place at this concentration. Design-Expert® Software twr cnt X1 = A: peak current X2 = B: pulse on time Actual Factor C: pulse off time = 30 B: pulse on time A: peak current 17 21 28 45 55 65 6.2 5 3.8 2.6 1.4 twr cnt Design-Expert® Software twr cnt X1 = A: peak current X2 = B: pulse on time Actual Factor C: pulse off time = 60 B: pulse on time A: peak current 17 21 28 45 55 65 5.5 4.3 3.1 1.9 0.7 twr cnt Fig 6 Graph of without CNT for TWR Fig 7 Graph of with CNT for TWR Effect of carbon nano tube on TWR The means TWR for CNT + kerosene was 0.956mm3/min and that of pure kerosene was 1.045mm3/min at 17A and pulse on time 45 micro sec. and pulse of time 45 micro sec. The experimental results show that the CNT powder concentration of 0.5 g/l. It is clear from the graph that the peak current and pulse on time and CNT concentration are the main influencing factor in the tool wear rate. Pulse off time and polarity are less influencing factor for tool wear rate .when CNT mixed with kerosene than created lubricant layer around tool and work piece this mixer keep cool the electrode and that’s why the tool wear rate is decrease.
  • 7. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 190 CONCLUSION Process parameters do not have same effect for every response. Significant parameters and its percentage contribution changes as per the behavior of the parameter with objective response Finding the result of MRR the most significant factor was found to be peak current followed by pulse on time and the least significant was pulse off time. The MRR increased linearly with the increase in current. For pulse on time the MRR first increased with linearly with increase in pulse off time, MRR decreased insignificantly. In the case of Tool wear rate the most important factor is peak current then pulse on time and after that pulse off time. Effect of carbon nano tube on MRR for CNT + kerosene was 58.977 mm3/min and that of pure kerosene was 49.407 mm3/min from experimental result with carbon nano tube the average 19% of MRR increased with respect to input parameter. Effect of carbon nano tube on TWR for CNT + kerosene was 0.956mm3/min and that of pure kerosene was 1.045mm3/min from experimental result with carbon nano tube the average 8.51% of TWR decreased with respect to input parameter. Table 1: Major properties of EN-31 Chemical Composition and grades: GCr15, 102Cr6, L1/L3/52100, SUJ2 Material Thermal conductivity (W/mk) Density (g/cc) Electrical resistivity Specific heat capacity (J/g-‘c) EN-31 46.6 7.81 o.oooo218 0.475 C si Mn Cr p V Fe 1.07 0.32 0.58 0.03 0.04 1.12 Balance Table 2: specification of MWCNT Aspect Ratio ˜1000 Specific Surface Area 350 m2/g Purity –wt% 95% Metallic Impurity 5% Average outer Diameter 20-40nm Average inner diameter 5 nm Number of Walls 5-15 Length 50μm
  • 8. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 191 REFERENCES Research Papers [1] M.Kiyak, Department of Mechanical Engineering, Yildiz Technical University, 34349 Istanbul, Turkey Journal of Materials Processing Technology 191 (2007) 141–144. [2] “shailesh kumar” Experimental Investigation of Machining Parameters for EDM Using U-shaped Electrode of AISI P20 Tool Steel thesis (2010). [3] Module 9 “Non conventional Machining”, Version 2 ME, IIT Kharagpur. [4] J.L Lin, C.L. Lin, the use of orthogonal array with grey relational analysis to optimize the EDM process with multiple performance characteristics, international journal of machine tools manufacture 42(2002) 237-244. [5] M. Mahardika and K. Mitsui, Total energy of discharge pulse calculation by stochastic methods, Proceeding of the International Conference of the 10th AUN/SEED.Net Field Wise Seminar, Hanoi, Vietnam in 28th– 29th August 2007. [6] Poddar Ayush “Experimental Investigation of Mrr, Surface Roughness and Overcut of AISI 304 Stainless Steel in EDM” a thesis submitted to NIT (2012). [7] M. Mahardika and K. Mitsui, A new method for monitoring micro-electric discharge machining processes, International Journal of Machine Tools Manufacture (2007) doi:10.1016/j.ijmachtools.2007.08.023. [8] M. Mahardika and K. Mitsui, Total energy of discharge pulse calculation by stochastic methods, Proceeding of the International Conference of the 10th AUN/SEED.Net Field Wise Seminar, Hanoi, Vietnam in 28th– 29th August 2007. [9] “s prabhu1, b k vinayagam” Nano surface generation of grinding process using carbon nano tubes S¯ adhan¯ a Vol. 35, Part 6, December 2010, pp. 747–760. [10] “Hyun-Seok TAK, Chang-Seung HA”, Characteristic evaluation of Al2O3/CNTs hybrid materials for micro-electrical discharge machining. elsevier (2011)s28-s38. [11] “C. Mai Hong Hocheng” Advantages of carbon nanotubes in electrical discharge machining Int J Adv Manuf Technol DOI 10.1007/s00170-011-3476-2 (2011). [12] “Gautam kocher1, Karan Chopra”, Investigation of Surface integrity of AISI D3 tool steel After EDM International Journal of Emerging Technology and Advanced Engineering (ISSN 2250-2459, Volume 2, Issue 4, April 2012). [13] S Velusamy, U.O Bidwai, “Effect of Titanium Carbide particle addition in the aluminum composite on EDM process parameters”. Journal of Manufacturing Processes (2011) 60-66 [14] P. Janmanee A. Muttamara,” Performance of difference electrode materials in EDM of Tungsten carbide”. Science publication, (2010) 87-90. [15] M.P.Mohan, Y.S.Wong, “A study of Fine finishing die sinking Micro EDM of Tungsten Carbide using different electrode materials”. Journal of Material processing technology (2009) 3956-3967. [16] H.C. Tsai, B.H. Yan,” EDM performance of Cr/Cu-based composite electrodes”. International Journal of Machine Tools Manufacture (2003) 245-252. [17] A. A. Khan,” Electrode wear and MRR during EDM of aluminum and mild steel using copper and brass electrodes”. International journal of advance manufacturing (2008) 482-487. [18] Y.S.Wong, Y.H. Fuh,” EDM performance of TIC/Copper based Sintered electrode”. Material Design (2001) 669-678. [19] “yan. Cheng”Machining characteristics and optimization of machining parameters of SKH57 high-speed steel using electrical-discharge machining based on Taguchi method. Materials and Manufacturing Processes, 21(8), 922-929.
  • 9. International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 7, July (2014), pp. 184-192 © IAEME 192 [20] “J. Simao, H.G. Lee”. Workpiece surface modification using electrical discharge machining, 43 (2003) 121–128(2003). [21] “Khalid Hussain SYED, Kuppan PALANIYANDI”, Performance of electrical discharge machining using aluminums powder suspended distilled water Turkish J. Eng. Env. Sci (2012). [22] S.H Tomadi, M.A Hussain, “Analysis of influence of EDM Parameters on Surface quality, MRR, EWR on Tungsten carbide”. IMECS, (2009). [23] C J Luis, I. Puertas, “MRR and EW study on the EDM of Silicon carbide”, Journal of Material processing technology (2005) 889-896. [24] Nixon Kuruvila and H. V. Ravindra,” Parametric influence and optimization of wire EDM of hot die steel,” Machining Science and Technology (2011), 15:47–7. [25] Puertas, I. And Luis, C.J., 2004.” A study of optimization of machining parameters for Electrical discharge machining of boron carbide” Materials and Manufacturing Processes. [26] Bhautik Patel, CFD Analysis of Laser Ablation of Graphite Target in Three Dimensional Grid thesis from Ganpat University. [27] H. Theil, Principles of Econometrics 622– 27 (1971); G. Chow, Econometrics 320– 47 (1983). [28] Techniques for the estimation of nonlinear regressions have been developed. See, e.g., G.Chow, supra note 9, at 220– 51. [29] Statistical method for social scientists II0 – I6 johnston econometric method 1972. [30] A. Parshuramulu, K. Buschaiah and P. Laxminarayana, “A Study on Influence of Polarity on the Machining Characteristics of Sinker EDM”, International Journal of Advanced Research in Engineering Technology (IJARET), Volume 4, Issue 3, 2013, pp. 158 - 162, ISSN Print: 0976-6480, ISSN Online: 0976-6499. [31] P.B.Wagh, R.R.Deshmukh and S.D.Deshmukh, “Process Parameters Optimization for Surface Roughness in EDM for AISI D2 Steel by Response Surface Methodology”, International Journal of Mechanical Engineering Technology (IJMET), Volume 4, Issue 1, 2013, pp. 203 - 208, ISSN Print: 0976 – 6340, ISSN Online: 0976 – 6359. [32] Mane S.G. and Hargude N.V., “An Overview of Experimental Investigation of Near Dry Electrical Discharge Machining Process”, International Journal of Advanced Research in Engineering Technology (IJARET), Volume 3, Issue 2, 2012, pp. 22 - 36, ISSN Print: 0976-6480, ISSN Online: 0976-6499. [33] S. K. Sahu and Saipad Sahu, “A Comparative Study on Material Removal Rate by Experimental Method and Finite Element Modelling in Electrical Discharge Machining”, International Journal of Mechanical Engineering Technology (IJMET), Volume 4, Issue 5, 2013, pp. 173 - 181, ISSN Print: 0976 – 6340, ISSN Online: 0976 – 6359.