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1
GUJARAT TECHNOLOGICAL UNIVERSITY
Chandkheda, Ahmedabad.
Affiliated
L.D. College of Engineering
A report on
Gas-Liquid Chemical Reactions
Under the subject of
DESIGN ENGINEERING – 1A
B. E., Semester-II
Chemical Engineering
Submitted by: -
Sr. Name of student Enrolment No.
1. Patil Mayur 160283105009
2. Chetan Rohit 160283105010
3. Sindhav Jaydrath 160283105011
4. Vasava Yogesh 160283105012
Guided By:
Prof. Dr. Purvi Shukla
Academic Year
(2016-2017)
2
L.D. ENGINEERING COLLEGE –AHMEDABAD
Certificate
Date:
This is to certify that the project entitled “Gas-Liquid Reactions” has been
carried out by Patil Mayur (160283105009), Chetan Rohit (160283105010),
Sindhav Jaydrath (160283105011) and Vasava Yogesh (160283105012) under
my guidance in fulfillment of the Degree of Bachelor of Engineering in Chemical
Engineering – Semester-III of Gujarat Technological University, Ahmadabad
during the academic year 2016-2017.
Name of Guide Head of Department
Prof. Dr. Purvi Shukla Dr. Sachin Parikh
Chemical Engineering Chemical Engineering
3
ACKNOWLEDGEMENT
We would like to extend our heartily thanks with a deep sense of gratitude and
respect to all those who has provided us immense help and guidance during our
project.
We would like to express our sincere thanks to our internal guide Dr. Purvi
Shukla for providing a vision about the system and for giving us an opportunity
to undertake such a great challenging and innovative work. We are grateful for
the guidance, encouragement, understanding and insightful support given in the
development process.
We would like to extend my gratitude to Dr. Sachin Parikh, Head of Chemical
Engineering department.
Last but not the least we would like to mention here that we are greatly indebted
to each and everybody who has been associated with our project at any stage but
whose name does not find a place in this acknowledgement.
Yours Sincerely,
Patil Mayur (160283105009)
Chetan Rohit (160283105010)
Sindhav Jaydrath (160283105011)
Vasava Yogesh (160283105012)
4
INDEX
Sr.no. Contents Page no.
1. Introduction 5
2. Mind mapping 6
3. AEIOU summary 7
3.1 Environment 8
3.2 Interaction 8
3.3. Objects 9
3.4 Activities 9
3.5 Users 9
4 Empathy Mapping 10
4.1 User 11
4.2 Stakeholders 11
4.3 Activities 11
4.4 Story Boarding 12
5. Ideation Canvas 13
5.1 People
Activities
14
5.2 Activities 14
5.3 Situation /Location /context 14
5.4 Possible Solutions 15
6. Product Development Canvas 16
6.1 Purpose 17
6.2 Product Experience & Product Features & Product functions 17
6.3 People 18
6.4 Components 18
6.5 Customer Revalidation 19
6.6 Reject, Redesign, Retain 19
5
1. INTRODUCTION
Gas-liquid reactions, it’s one the most important heterogeneous reactions. when it comes to
gas-liquid reactions, there are two broad application areas where these reactions are used.
One is the gas purification processes and these are important not only from the environmental
point of view, but quite often when we want to use certain gases for reactions and we do not
want any impurities associated with it. We have a gas purification process as a most important
part of any reactor system.
We have things like carbon dioxide removal from synthesis gas. for example, using aqueous
solution of hot ammonia and hot potassium carbonate or ethanoamines we can scrub the CO2
gas. So, CO2 removal essentially is useful with the synthesis gas or with the thermal power
plant flue gases.
The idea is that we want to remove CO2 in hot potassium carbonate or ethanolamine. Now,
why hot why potassium carbonate? Because the carbon dioxide will react with it very easily
in suitable conditions.
Then another common polluting agent is sulphur. So, we want to remove it in hydrogen
sulphide or by sodium hydroxide or reacting ethanolamines and so on. So, there are broad
classes of reactions, we can say that these reactions are more of a purification step than any
production step.
The production processes where gas-liquid reaction occur, on the other hand as a target
product. For example, air oxidation of aldehydes to acids or oxidation of cyclohexane to atopic
acid, which is an important monomer. Chlorination of benzene formation of or production of
nitric acid, sulphuric acid and so on. Where product namely acids or chlorobenzenes or
sulphuric acid, these are important products which we want to manufacture using gas-liquid
reactions.
6
2.Mind Mapping
The image of mind mapping is given below
7
3.AEIOU SUMMARY
First, we started working in AEIOU summary.
• A: Activities
• E: Environment
• I: Interactions
• O: Objects
• U: Users
This canvas is totally based on the observations. Activities as the name suggests we have
to describe all the activities we observed like if we are in chemical plant we have seen
like…
The image of AEIOU summary is Given below.
8
3.1) Environment:
• It can be noisy due to certain operations
are going on simultaneously.
• Here if we are working in the chemical
industry, obviously, there will be Chemical
smell.
• Apart of the equipment’s in which
gas-liquids are going on there is another
processes are also going on with it so all
the processes are considered as the process
industrial environment.
• There are no. of employee are working in
the industry around and industry, so work
environment of workers can be seen around.
3.2) Interactions:
• there are interactions between engineers and
worker outside the reaction system.
Workers like ITI, technicians etc.
• other interactions are between worker to
their helpers
• HR-department to all employees of company
for improvement of the production, financial
states and for other matters.
• Industrial meetings: it’s one of the most
way in industry for the interaction.
 Other important interaction is between
employee with supplier and buyers of the
company.
9
3.3) Objects:
We have to describe observed object and
user to correspondingly object frame and
user framework. In our case, there is
chemical plant, so objects are
• LAB
• Equipment
• Flow-charts
• Power supply
• Safety instruments
3.4) Activities:
In this section, we have to mention the
things happening around the system
• Raw material to procedure
• Research and Development
• maintenance
 Employer’s work
 Mass transfer operations (industrial)
3.5) Users:
The main user of gas-liquid industries
are given below
• Customer
• Other industries
• Chemist
 Pollution control department
10
4.EMPATHY MAPPING
11
Basically, there are four sections in Empathy Canvas,
1. User
2. Stakeholders
3. Activities
4. Story Boarding
To fill empathy canvas, we have studied problems related gas-liquid industries and the people
affected with it, their activities and experience.
4.1) User
• Customer
• Other industries
• Chemist
 Pollution control department
4.2) Stakeholders:
Due to Gas-liquid operation, people
that would be indirectly affected are
• Customer
• Engineer
• Workers
 Helper
 H.R. Department
4.3) Activities:
The activities carried out by stakeholders are
• Raw material to procedure
• Research and Development
• Maintenance
 Employer’s work
 Mass transfer operations (industrial)
 Plant controlling
 Testing of material
12
4.4) Story Boarding
• There are two happy experience and two sad experience which are given below: first happy
experience is about the how the gas-liquid operation is useful for purification purpose and
second experience is about the product, which can be useful the other industries.
 There are two bad experience also, which is related to hazards and another story is about the
not complete removal of some material.
13
5. IDEATION CANVAS
• Ideation Canvas contain main four sections
1. People
2. Activities
3. Situation/Context/Location
4. Possible Solution
• If we talk about Ideation Canvas then it is something near to our main problem which we want
to find. In people part, only those people mention which is only related to our problem only.
• In Activities means during which you are facing problem. In location/Situation means in
which situation and location problem become in picture that things must be maintained.
• The thought for context/location/situation and finally for possible solutions is at last we have
to find problem and that can be possible solution and way that things can be mentioned.
14
5.1) People:
So, people we have mentions different peoples like which are direct related to our problem
• Engineer
• Workers
 Helper
 H.R. Department
 Customer
 Suppliers
 Manager
 Chemist
5.2) Activities:
In activities like studying, operating,
testing electrical material means these
activities come in picture when we are
talking about our mentioned problem
• Machine Breakdown
• Power failure
• Maintenance
 Impurities in Raw-material
 Shortage of Raw-material
 Over production
 Shortage of employee
 Process conditions not maintained
5.3) Situation/Context/Location:
In this section, we have mentions the
Situations in which the problem
occurs
• Heavy Rainfall
• Earthquake
• Storm
• Fire
• Hazards
• Wastage of material
• Strikes
• Unavailability of area for
Plant expansion
15
5.4) Props/Possible solutions:
In this section, the possible solutions are given for above mentioned problems
• Proper maintenance of machine
• Save electricity and use of Generators
• Proper availability of Raw-material
• Increase capacity of storage tank
• Find good quality Raw-material
• New recruitment of employees
 Maintain the process condition properly
 Flood control system
 Fire extinguishers
 Controlling the production
 Proper material handling
 Healthy Working environment
 Installations of safety equipments.
16
6.PRODUCT DEVLOPMENT CANVAS
Product Development Canvas contain
1. Purpose
2. People
3. Product Experience & Product Function & Product Features
4. Components
5. Customer Revalidation
6. Reject, Redesign & Retain
Now, when we are discussing about the product development canvas we have to define the main
problem after completion of user canvas and Ideation Canvas.
17
6.1) Purpose:
The purpose of our project is to design a product
that should perform the following functions
• To provide finished product as per the requirement
of the customer
• To provide good quality Raw material to industries
• For purification of materials
• Good mass transfer so product can obtain in short time
and easily
6.2) Product Experience & Product Features & Product functions:
6.2.1) Product Experience
• Satisfy with quality of product
• Satisfy with cost and quantity of the product
• Product should be ease in application
18
6.2.2) Product Features
• Safety
• High efficiency
• Increase in working capacity
 Maintain operating conditions
6.2.3) Product functions
• Newer technology equipments
• Easily prepare and less time consuming
• Good quality
 Available in different-different requirements
6.3) Customer Revalidation : 6.4) People:
In this section the review of our products The people to whom our product may
which are taken from the customers be useful are
 Good quality Customer
 Comfortibility Chemist
 Ease in application Other industries
19
6.5) Components:
In this we have to mentions all the components used in our gas-liquid operations
• Reactor
• Storage tank
• Pipelines
• Types of packing
• Valves
• Trays
• Condensers and Heat exchanger
6.6) Reject, Redesign, Retain
In this section the improvements are
mentioned, which are based costumer’s
review and their suggestions:
 Low diffusibility
 Unavailability of product in large amount
 High product cost
REFERANCE:
1. Mass Transfer Operations by Robert E Treybal
2. Unit Operations of Chemical Engineering by McCabe Smith
THANK YOU
DESIGN ENGINEERING - I on GAS - LIQUID

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DESIGN ENGINEERING - I on GAS - LIQUID

  • 1. 1 GUJARAT TECHNOLOGICAL UNIVERSITY Chandkheda, Ahmedabad. Affiliated L.D. College of Engineering A report on Gas-Liquid Chemical Reactions Under the subject of DESIGN ENGINEERING – 1A B. E., Semester-II Chemical Engineering Submitted by: - Sr. Name of student Enrolment No. 1. Patil Mayur 160283105009 2. Chetan Rohit 160283105010 3. Sindhav Jaydrath 160283105011 4. Vasava Yogesh 160283105012 Guided By: Prof. Dr. Purvi Shukla Academic Year (2016-2017)
  • 2. 2 L.D. ENGINEERING COLLEGE –AHMEDABAD Certificate Date: This is to certify that the project entitled “Gas-Liquid Reactions” has been carried out by Patil Mayur (160283105009), Chetan Rohit (160283105010), Sindhav Jaydrath (160283105011) and Vasava Yogesh (160283105012) under my guidance in fulfillment of the Degree of Bachelor of Engineering in Chemical Engineering – Semester-III of Gujarat Technological University, Ahmadabad during the academic year 2016-2017. Name of Guide Head of Department Prof. Dr. Purvi Shukla Dr. Sachin Parikh Chemical Engineering Chemical Engineering
  • 3. 3 ACKNOWLEDGEMENT We would like to extend our heartily thanks with a deep sense of gratitude and respect to all those who has provided us immense help and guidance during our project. We would like to express our sincere thanks to our internal guide Dr. Purvi Shukla for providing a vision about the system and for giving us an opportunity to undertake such a great challenging and innovative work. We are grateful for the guidance, encouragement, understanding and insightful support given in the development process. We would like to extend my gratitude to Dr. Sachin Parikh, Head of Chemical Engineering department. Last but not the least we would like to mention here that we are greatly indebted to each and everybody who has been associated with our project at any stage but whose name does not find a place in this acknowledgement. Yours Sincerely, Patil Mayur (160283105009) Chetan Rohit (160283105010) Sindhav Jaydrath (160283105011) Vasava Yogesh (160283105012)
  • 4. 4 INDEX Sr.no. Contents Page no. 1. Introduction 5 2. Mind mapping 6 3. AEIOU summary 7 3.1 Environment 8 3.2 Interaction 8 3.3. Objects 9 3.4 Activities 9 3.5 Users 9 4 Empathy Mapping 10 4.1 User 11 4.2 Stakeholders 11 4.3 Activities 11 4.4 Story Boarding 12 5. Ideation Canvas 13 5.1 People Activities 14 5.2 Activities 14 5.3 Situation /Location /context 14 5.4 Possible Solutions 15 6. Product Development Canvas 16 6.1 Purpose 17 6.2 Product Experience & Product Features & Product functions 17 6.3 People 18 6.4 Components 18 6.5 Customer Revalidation 19 6.6 Reject, Redesign, Retain 19
  • 5. 5 1. INTRODUCTION Gas-liquid reactions, it’s one the most important heterogeneous reactions. when it comes to gas-liquid reactions, there are two broad application areas where these reactions are used. One is the gas purification processes and these are important not only from the environmental point of view, but quite often when we want to use certain gases for reactions and we do not want any impurities associated with it. We have a gas purification process as a most important part of any reactor system. We have things like carbon dioxide removal from synthesis gas. for example, using aqueous solution of hot ammonia and hot potassium carbonate or ethanoamines we can scrub the CO2 gas. So, CO2 removal essentially is useful with the synthesis gas or with the thermal power plant flue gases. The idea is that we want to remove CO2 in hot potassium carbonate or ethanolamine. Now, why hot why potassium carbonate? Because the carbon dioxide will react with it very easily in suitable conditions. Then another common polluting agent is sulphur. So, we want to remove it in hydrogen sulphide or by sodium hydroxide or reacting ethanolamines and so on. So, there are broad classes of reactions, we can say that these reactions are more of a purification step than any production step. The production processes where gas-liquid reaction occur, on the other hand as a target product. For example, air oxidation of aldehydes to acids or oxidation of cyclohexane to atopic acid, which is an important monomer. Chlorination of benzene formation of or production of nitric acid, sulphuric acid and so on. Where product namely acids or chlorobenzenes or sulphuric acid, these are important products which we want to manufacture using gas-liquid reactions.
  • 6. 6 2.Mind Mapping The image of mind mapping is given below
  • 7. 7 3.AEIOU SUMMARY First, we started working in AEIOU summary. • A: Activities • E: Environment • I: Interactions • O: Objects • U: Users This canvas is totally based on the observations. Activities as the name suggests we have to describe all the activities we observed like if we are in chemical plant we have seen like… The image of AEIOU summary is Given below.
  • 8. 8 3.1) Environment: • It can be noisy due to certain operations are going on simultaneously. • Here if we are working in the chemical industry, obviously, there will be Chemical smell. • Apart of the equipment’s in which gas-liquids are going on there is another processes are also going on with it so all the processes are considered as the process industrial environment. • There are no. of employee are working in the industry around and industry, so work environment of workers can be seen around. 3.2) Interactions: • there are interactions between engineers and worker outside the reaction system. Workers like ITI, technicians etc. • other interactions are between worker to their helpers • HR-department to all employees of company for improvement of the production, financial states and for other matters. • Industrial meetings: it’s one of the most way in industry for the interaction.  Other important interaction is between employee with supplier and buyers of the company.
  • 9. 9 3.3) Objects: We have to describe observed object and user to correspondingly object frame and user framework. In our case, there is chemical plant, so objects are • LAB • Equipment • Flow-charts • Power supply • Safety instruments 3.4) Activities: In this section, we have to mention the things happening around the system • Raw material to procedure • Research and Development • maintenance  Employer’s work  Mass transfer operations (industrial) 3.5) Users: The main user of gas-liquid industries are given below • Customer • Other industries • Chemist  Pollution control department
  • 11. 11 Basically, there are four sections in Empathy Canvas, 1. User 2. Stakeholders 3. Activities 4. Story Boarding To fill empathy canvas, we have studied problems related gas-liquid industries and the people affected with it, their activities and experience. 4.1) User • Customer • Other industries • Chemist  Pollution control department 4.2) Stakeholders: Due to Gas-liquid operation, people that would be indirectly affected are • Customer • Engineer • Workers  Helper  H.R. Department 4.3) Activities: The activities carried out by stakeholders are • Raw material to procedure • Research and Development • Maintenance  Employer’s work  Mass transfer operations (industrial)  Plant controlling  Testing of material
  • 12. 12 4.4) Story Boarding • There are two happy experience and two sad experience which are given below: first happy experience is about the how the gas-liquid operation is useful for purification purpose and second experience is about the product, which can be useful the other industries.  There are two bad experience also, which is related to hazards and another story is about the not complete removal of some material.
  • 13. 13 5. IDEATION CANVAS • Ideation Canvas contain main four sections 1. People 2. Activities 3. Situation/Context/Location 4. Possible Solution • If we talk about Ideation Canvas then it is something near to our main problem which we want to find. In people part, only those people mention which is only related to our problem only. • In Activities means during which you are facing problem. In location/Situation means in which situation and location problem become in picture that things must be maintained. • The thought for context/location/situation and finally for possible solutions is at last we have to find problem and that can be possible solution and way that things can be mentioned.
  • 14. 14 5.1) People: So, people we have mentions different peoples like which are direct related to our problem • Engineer • Workers  Helper  H.R. Department  Customer  Suppliers  Manager  Chemist 5.2) Activities: In activities like studying, operating, testing electrical material means these activities come in picture when we are talking about our mentioned problem • Machine Breakdown • Power failure • Maintenance  Impurities in Raw-material  Shortage of Raw-material  Over production  Shortage of employee  Process conditions not maintained 5.3) Situation/Context/Location: In this section, we have mentions the Situations in which the problem occurs • Heavy Rainfall • Earthquake • Storm • Fire • Hazards • Wastage of material • Strikes • Unavailability of area for Plant expansion
  • 15. 15 5.4) Props/Possible solutions: In this section, the possible solutions are given for above mentioned problems • Proper maintenance of machine • Save electricity and use of Generators • Proper availability of Raw-material • Increase capacity of storage tank • Find good quality Raw-material • New recruitment of employees  Maintain the process condition properly  Flood control system  Fire extinguishers  Controlling the production  Proper material handling  Healthy Working environment  Installations of safety equipments.
  • 16. 16 6.PRODUCT DEVLOPMENT CANVAS Product Development Canvas contain 1. Purpose 2. People 3. Product Experience & Product Function & Product Features 4. Components 5. Customer Revalidation 6. Reject, Redesign & Retain Now, when we are discussing about the product development canvas we have to define the main problem after completion of user canvas and Ideation Canvas.
  • 17. 17 6.1) Purpose: The purpose of our project is to design a product that should perform the following functions • To provide finished product as per the requirement of the customer • To provide good quality Raw material to industries • For purification of materials • Good mass transfer so product can obtain in short time and easily 6.2) Product Experience & Product Features & Product functions: 6.2.1) Product Experience • Satisfy with quality of product • Satisfy with cost and quantity of the product • Product should be ease in application
  • 18. 18 6.2.2) Product Features • Safety • High efficiency • Increase in working capacity  Maintain operating conditions 6.2.3) Product functions • Newer technology equipments • Easily prepare and less time consuming • Good quality  Available in different-different requirements 6.3) Customer Revalidation : 6.4) People: In this section the review of our products The people to whom our product may which are taken from the customers be useful are  Good quality Customer  Comfortibility Chemist  Ease in application Other industries
  • 19. 19 6.5) Components: In this we have to mentions all the components used in our gas-liquid operations • Reactor • Storage tank • Pipelines • Types of packing • Valves • Trays • Condensers and Heat exchanger 6.6) Reject, Redesign, Retain In this section the improvements are mentioned, which are based costumer’s review and their suggestions:  Low diffusibility  Unavailability of product in large amount  High product cost
  • 20. REFERANCE: 1. Mass Transfer Operations by Robert E Treybal 2. Unit Operations of Chemical Engineering by McCabe Smith THANK YOU