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Auro textile Trainning report
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Auro textile Trainning report

  1. AURO TEXTILE GROUP OF COMPANY SUBMITTED BY Mr. R.C. Mishra Guide by Mr. Debabrata Nandy Submitted to Jagmohan Roll no. – 10004260020 Govt. Polytechnic Hisar ACKNOWLEDGEMENT
  2. I thankful to all staff & workers of Auro Textile on Vardhman group of company, they helped me at every stage & moreover I feel here every place is neat & clean. This is very important for product quality & also for happiness. I especially thankful to: Mr. S.K.Ojha Mr. R.C.Mishra Mr. A.H.Ansari G.M. (Tech. deptt.) V.P. Auro Textile Dyeing Manager I shall also thankful to Mr. Rupak Mukherjee, Mr. Debabrata Nandy, Mr. Sunil Mahajan I also express to wish the same to: Mr. Tarun Arora HOD (H.R. department) For having suggest their valuable ideas and guide me to the maximum periphery in accordance with each and every aspect and for stretching their ideal second in de-coding the error to result in a colorful way. Greige Department
  3. INTRODUCTION: Greige fabric that buys from different weaving units comes in this department. In this department inspection of fabric is done. Accepted fabric is send to next department. There are two inspection systems that are mostly used, one in 10 point American systems and other is 4 points Japanese system is used. I-Inspection / Grading II-Lot making III-Mending I-Inspection / Grading: - The main purpose of the inspection is to check the Greige fabric for identify the faults. Weaving Faults: - Double Ends, Loose Ends, Broken Ends, Wrong Dent/Draw, Loose Selvedge, Double Pick, Miss Pick, Design Cut, Knots, Hanging Threads, Float, Mechanical Faults: - Starting Marks, Rapping Marks, Mending Marks, Hole /Cuts, Oil Stain Yarn Faults: - Cockled Yarn, Weft Slub, Slubby Weft, CEP, Count Variation, Hair, Jute, P Propylene, Black Ends. Others: - Oily Weft, Sizing Stain, Hard Size.
  4. Minor Faults: - The faults can be removed easily in further processing such as in scouring, bleaching and mercerizing etc. Major Faults: - Those faults that cannot be removed in further processing are major faults such as starting mark, rapping mark, whole etc. II-LOT MAKING: - Lot making is the process which is done before Pretreatment. Lot making is done for easy handling, transportation and dyeing facilities. Considerations for the lot making are: - 1.Fibre types 2.Constructions 3.Greige width 4. Greige lot 5. Convenience of processing and transportations. 6. Source 7. Customer needs this process is done after see the greige fabric from weaving (lots) then applies the above factors. Normally 2100 meter fabric easily handling. When fabric come from weaving then one number is write on the fabric by weavers in order to different looms, different firm yarns etc. but in the dyeing factories. They had done lot making fewer than 7 factors. III-MENDING:-
  5. The correction of the mendable class is called mending. It is also called repairing of faults. Mending is done by physically and chemically. I -PHYSICALLY MENDING: - In the physical mending these faults are removed broken ends, broken picks, knots, contaminations. II -CHEMICALLY MENDING: - In the chemical mending these faults are removed stains, oils, waxes, rust, soils, sighting colors. TYPES OF OIL AND STAINS Water Soluble Inorganic salts, urea, and sugar Pigments Carbon Black, Silicates, and Metal oxides. Fats and Oils Animals, Vegetables and minerals Proteins Blood, milk Bleachable dyes Fruits, vegetables etc.
  6. Preparatory Department Lead cloth It is used in a cleaning of machine. It is save the threading time on the machines. It is save the fabric in damaging stage on the machine. It is made by the polyester fiber. It is high
  7. temperature absorbs. Some companies are wastes fabric used in place of lead cloth. JUKI Stitching Machine It is used for stitching purpose of two fabric. In this machine five yarn is used. In the machine 3polyester and 2cotton yarn is used. This machine is manly used for peaching process on stitching of two fabric. PEGASUS Stitching Machine It is used for stitching purpose of two fabric. In this machine two yarn is used. In the machine 2cotton yarn is used. This machine is not used for peaching process on stitching of two fabric. Trolley In the trolley fabric is store. It is present in the industry three shapes (L-shape, U-shape and Box trolley). It is also used for transportation of the fabric on the machine. In the trolley 1700 – 2300 meter fabric store. Batch On the batch fabric is store. It is also used for transportation of the fabric on the machine. In the trolley 4500 – 5500 meter fabric store. It is save the space on the industry. STITCHING SECTION
  8. In stitching section we stitch the no of small lots to make a lot of required. This is divided into three parts 1. Plate form 2. Unfolding machine 3. Stitching machine 1-PLATE FORM: - This contain unstitch fabric in the form of rollers, bails, and pallets. 2-UNF OLDING MACHINE: - By using this machine fabric is unfolded and plaid in trolleys. 3- Stitching machine: - Now stitching machine is used to stitch the fabric width wise and store in trolleys. INTRODUCTION: - •Stitch should be straight. •Selvage of one lot is stitch on the selvedge of other lot. NOTE: - The fabric come from grey store, are sent in the bleaching department. The lot depends upon many rolls of fabric. In a bleaching department theses rolls are opened, unwind so that the fabric rolls could be stretched with each other for further process. The selvedge of a fabric of roll is stretched the selvedge of opened roll of fabric. Now the fabric is kept in trolleys. The numbers of trolleys are different with each other. A single trolley have unique number 1,2,3,4,5,6,7,-----------315, 316 so on, so that the fabric lot
  9. should be identified by trolley fabric is kept 1500 to 2100 Meters according to the quality of the fabric. We cannot keep fabric more than 2100 meter. After keeping fabric in a trolley a separate job card is allotted to a single trolley. There are following information mentioned on a job card e.g. date, contract, customer, constructions, shade, process department, grey Lot #, fabric type, proc Lt #, quality, fabric source, sub-batch #, sub-batch # Qty, grey width, M/c code, date, shift, start, End, Meters, trolley No, signature operator and comments. First of all write starting process Date, marketing persons allots separate Contract No # NDF/OG.3688. There are many lots may be in a single contract, Customer Name etc. Construction, 20.16 / 118.63 etc. Shade, what is a shade required black, blue, navy blue. Process Departments Bleaching, Mercerizing. Grey Lt #, the persons of grey store allot separate No# 16067 etc. SWASTIC Machine (Gray fabric washing machine) This machine is made in India. It machine speed and vertical drying range temperature are set according to the fabric quality. It is manly used washing of gray fabric. In this machine four washers, one VDR (vertical drying range) and dancer rollers is present. In this machine any chemical are not used. After by washing fabric lengths and hardness are decrease. The gray fabric fluffs are remove in the machine. WORKING First fabric is enter in the inlet section. The cloth guider rollers are guiding the fabric. The fabrics are enter in the washing chamber and wash it after by passing of cloth guider. The mangle is squeeze the fabric after by washing. The fabric is dry
  10. in the VDR. After by fabric is collect in the plaiter. The fabric is store in the trolley. In the trolley easily transportation of fabric. Process flow of Swastic Machine Inlet Section WASHING UNIT VERTICAL DRY RANGE PLAITER TROLLY Parts of Swastic Machine – Inlet section, Guide roller, 4 washers, Dancer rollers, 4 Padding mangles, VDR, Plaiter. Inlet section The fabrics are enter in this machine help of feed roller. It section is known as Inlet section. Feed roller It is give the motion of the fabric. Without feed roller fabric are not run to swastic machine. It is attach the starting and end point of machine. Guide roller It is guide the fabric on the machine. Without guider fabric is not possible to running of continuous process. It is stop the making of the crease. It is also known as cloth guider. Washer The gray fabric is wash in this chamber. The any chemical and soap are not use in the chamber.
  11. Padding mangle It is important part of machine. It is squeeze the fabric after by Washing. Without padding mangle fabric are not properly dry on the dryer. Dancer roller It is maintain the tension of the fabric. It is information speed of the motor. It is save the damaging of the fabric. VDR It is dry the fabric after by the washing. In the vertical dry range steam is used. It is give the heating of the cylinder. In the VDR hot and cold cylinder (27 hot and 3 cold cylinders) are used. Plaiter The fabrics are out on the plaiter. It is stop the making of creases. It is help collection of the fabric on the trolley. Singeing With this treatment fuzz and fibre ends are burnt off in order highlight the fabric weave. It is generally carried out on gray pieces and the residues are removed by a further washing process. An oxidizing flame, which does not leave any trace of sooty residue on fibres, is used to carry out this operation. The flame can be perpendicular to the fabric, and only rarely tangential; the fabric is positioned at a distance of 1.5 - 4 mm from the end of the flame and the machine is equipped with a suction device under the fabric, which attracts the flame and concentrates the heat on the fabric. The fabric speed can range from 60 to 150 metres per minute. The singeing process with perpendicular flame is the most common one, while the process with tangential flame is used for fine fabrics (light singeing). OSTHOFF SINGEING MACHINE
  12. It is a gas singeing machine. In this machine fabric are run four position. The speeds are set according to the fabric. This machine is made in Germany. The threading of singeing machine is 60 meter fabric used. In this machine short hairy fiber are remove on the fabric surface help of burner. In this machine two burners and four cylinders are used. PROCESS FLOW OF OSTHOFF SINGEING MACHINE FIRST BRUSHING UNIT SINGEING SECOND BRUSHING UNIT OR QUENCHING BATH PLAITER WORKING OF OSTHOFF SINGEING MACHINE First run the material starting of the singeing machine. After by running of the fabric machine is start. The fabrics are dry and go to the brushing unit. In the brushing unit bigger fibre are remove used of brush. The brushing unit three brushes are presents. The removing of the bigger fibre fabrics is going to singeing unit. In the singeing unit short fibre are remove by using of flame. The singeing unit fabrics are run four position. In the singeing unit two burners and four cylinders are used. After by singeing fabrics is come in the Cooling cylinder. It is decrease the fabrics temperature. The brushing
  13. unit flame and ash are remove on the fabrics surface. The fabrics are collect on the trolley help of plaiter. Picture 1 - Fabric singeing with perpendicular flame Picture 2 - Fabric singeing with tangential flame Parts of Osthoff Singeing Machine Guide roller, Pre-dryer, Brushing unit, Singeing unit, Beater, Exhauster, Cooling cylinder, Dancer roller, Quenching bath, Plaiter. Guide roller It is guide the fabric on the machine. Without guider fabric is not possible to running of continuous process. It is stop the making of the crease. It is also known as cloth guider.
  14. Pre-dryer It is dry the fabric before the washing. In the Pre- dryer steam is used. It is give the heating of the cylinder. In the Pre- dryer two hot cylinders are used. Brushing unit The brushes are made by the Nylon. It is remove the bigger fibre on the fabric surface. After by singeing it is remove the flame and ash on the fabric surface. Singeing unit The short hairy fibre are remove on the surface of fabric by using of flame. In the singeing unit two burners are used. The burners are burn help of propane gas. Beater It is beat the fabric and removes the fluff on the fabric surface. Exhauster It is exist the fluff and ash on the singeing machine by using of fan. Cooling cylinder It is decrease the fabric temperature in the singeing process. Without cooling cylinder fabric is burn on the singeing unit. In the singeing unit four cooling cylinder are used. Dancer roller It is maintain the tension of the fabric. It is information speed of the motor. It is save the damaging of the fabric. Quenching bath After by singeing fabric is dip in the water. It is known as Quenching process. In this process flame and ash are remove on the fabric surface. It is save the damaging of fabric. Plaiter The fabrics are out on the plaiter. It is stop the making of creases. It is help collection of the fabric on the trolley. Quality M: Bar Position Yarn dyed fabric & bottom 12 4 Shirting 10 4
  15. All 70s, 80s 10 2 Machine speed = 60 to 150m/min. Gas pressure = 12milibar Flame temperature = 1720 C Steam pressure = 0.1 to 0.5 PERBLE RANGE MACHINE It is made in Japan. In the Preble range machine brushing, singeing, desizing, scouring, bleaching are done. The machine speeds are set according to the fabric. The machine threading is 520 meters. It made
  16. by the stainless steel. It is continuous machine. In this machine lead cloth is used cleaning of the machine. In the new Preble range after by reaction chamber –A the multiple washer are used. Process flow of Perble range machine Fabric inlet Fabric tension setting bar Pre – dryer Brushing unit Singeing unit Quenching bath Washer no. – 1 to4 Desizing and scouring saturator Reaction chamber – A Washer no. – 5 to9
  17. Chlorite bleaching saturator Reaction Chamber – B Washer no. – 9 to14 H2O2 bleaching saturator Washer no. – 15 to19 Washer no. - 20 (Neutralization bath) Washer no. – 21 VDR Plaiter WORKING OF PERBLE RANGE SINGEING MACHINE: - First fabric is enter in the machine on the brushing unit. In this section bigger fibre are remove. In the brushing section 6 brush are used. After by the fabric is goes to the tension setting bar unit. In the
  18. section tension is apply on the fabric. After by fabric is go to the singeing unit. The singeing unit four burner are used. In the burner propane gas are used. Before the singeing unit fabric is pass through the pre-dryer. The end of singeing fabric is go to quenching bath. In the bath ash are remove. After by removing of ash fabric is go to the washer. The fabric is wash in the washer. In the washer cold water is used. It is decrease the fabric temperature. The fabric is going in the combine saturator of desizing and scouring. The fabric is go to the reaction chamber- A. In this chamber fabric is store 18 to 25mintues. After by storage fabric is wash in the washing chamber. The fabric is go to the chlorite bleaching saturator or Hydrogen per-oxide bleaching saturator. The fabric is go to the reaction chamber- B. It also fabric is store 18 to 25 minutes. After by storage fabric is wash in the washing chamber. The fabric is neutralized with acid or alkali. After by fabric is washed in the washer. The fabric is go to dryer. In the dryer steam is used. Name of chemical used in chlorite bleaching on Preble range Desizing and scouring agent:- SIRREX 2UDI, HOSTPAL MRZ, SODIUM PER-SULPHATE, CAUSTIC SODA LYE. Bleaching agent:- FORMIC ACID (HCOOH), METHYL ALCOHAL (CH3OH), SODIUM CHLORITE (NACLO2) Name of chemical used in H2O2 bleaching on Preble range Desizing & scouring agent:- SIRREX 2UDI, HOSTPAL MRZ, SODIUM PER-SULPHATE, CAUSTIC SODA LYE.
  19. Bleaching agent:- H2O2, Lufibrol MSD, Contab BRT, NaOH Parameters of Preble range on singeing process S. No. Location item Media Unit Working area Actual setting 1. Pre-dryer Steam pressure Mpa 1.0 to 1.7 1.2 2. Pre-brushing unit Angle Marked on machine 0 to18 11 3. Gap between roll and burner Distance mm 6 to 20 9 4. Post-brushing Angle Marked on machine 0 to 18 17 5. Flame width Distance mm 200 to 2000 1800 6. Dancer Air pressure Mpa 0.15 to 5 0.35 7. Pressure roll Air pressure Mpa 0.2 to 0.6 0.4 YARN DYED FABRIC PROCESS SINGING AND DESIZING PROCESS SINGING: -
  20. When the cloth comes from the loom it has small fibres which are called fuzz. It must be removed by singing process. Mostly common used method is gas singing by the help of gas burners. IMPORTANCE OF SINGING: - Singing helps us to minimize or reduce the pilling effect. Pilling give harsh or bed look to fabric. It must remove from fabric to get good quality DESIZING: - Starch remove from the fabric is called desizing. Desizing is reverse of sizing and is also called steeping. Its main objective is to degrade size into soluble product so that after washing sizes remove from fabric and ready for subsequent process. BRUSH SINGING The fabrics pass through Electromagnetic and Nomatic rollers, In Nomatic rollers air pressure and in electromagnetic rollers electricity these rollers control the width of the fabric the brushing rollers are moving by motor. Now the fabric pass through six brushing rollers three are move in clockwise direction and three are move in anticlockwise direction below brushing portion of machine present Dust Collector which is collecting the dust . Now the fabric pass through the Draw Rollers, these rollers are plastic coated the function of this rollers give grip to the fabric so that the fabric do not slip and full the fabric Draw Rollers are also moved by motor. The fabric come on a guide roller then fabric pass through the Dancer roller, the function of the dancer roller keep tight the fabric should be come tight next part of machine. GAS SINGING
  21. In gas singing cloth is passed over gas flames. Now the fabric come in gas singing portion, there are seven rollers in gas singing portion which have cold water inner portion so that the fabric do not burn. In this portion of machine there are Four burners which are removing the fuzz, four gas burners are used and are arranged so that first the face and then back side of the cloth singed in a single passage, above this machine Dust collector which is collecting the dust. Four rollers are driven by the four motors. Flame length can be controlled by proper setting of air pressure and its width should be adjusted according to the width of the fabric. Back side of gas singing machine pipes are present yellow pipes are giving gas to burners and white pipes are giving air to burners. COMMON FAULTS: - Uneven singing effect •Across the width •Across the length These effects appear in the form of horizontal and vertical strips. These faults of singing detect the dyeing and these faults are un- removable. NOTE: - A suitable guiding principle for singing is the shouter flame fabric contact. KYOTO GAS SINGING MACHINE: - The speed of machine is 120meter/minute. The total capacity of machine is 82meter fabric. Machine 120000 – 135000 meter fabric singed and desized in 24 hours.
  22. In continuous process the machine used for singing and desizing. In this machine singing and desizing is done same time after one another. MACHINE PARTS AND FUNCTIONS Entrance, Electromagnetic rollers, Nomatic rollers, Brushing rollers, Dust collector, Draw rollers, Dancer roller, Gas burners, Rotary filter, Saturators, Expenders, Padders, Winding roller, ENTERENCE : - From trolley the fabric enter in the machine by the help of tension roller. There are four pair of cloth guider in this section which help to minimize the crease. BRUSHING ROLLERS: - There are six brushing rollers in brushing portion of machine. Three are move clock wise direction and three are move anti clock wise direction. The main purpose of these brushing rollers is to remove fluff from fabric surface. It contains suction pump that sucks fluff and with the help of showers fluff is removed from suction pomp. DUST COLLECTORS: - There are two dust collectors in machine, which are collect dust from machine. First dust collector present below brushing portion of machine and second is present above gas singing portion of machine. DRAW ROLLERS:- These rollers are plastic coated. These rollers provide grip to the fabric so that fabric do not slip, pull the fabric. DANCER ROLLERS: -
  23. The function of these rollers keeps tight to the fabric. There are three dancer rollers are present in machine. 1st dancer roller is present between brushing and gas singing portion of machine above draw rollers. 2nd dancer roller is present between two saturator along above padder. 3Rd is present along above solution tank. GAS BURNERS: - There are four gas burner are present in machine. In these burners gas and air is present. Yellow pipes back side of gas singeing machine are providing gas to the burners and white pipes are providing air. Regulator distributes the air. With the help of two drawer sand one dancer, the fabric from brushing section enter into singing section. It contains four burners. Water flow through the burners so that fabric remain safe from burning. The maximum temperature of the burner is 750 C and the pressure of the gas is 4.1 – 40-.7 kpa, while air is 6.1 – 6.9 kpa. Blue flame is touched with surface of the fabric. Burners are controlled by control panel. The flame touch with fabric at 45 angles. It can be change according to the quality of the fabric. Flame size normally use is 5” for Lycra quality both lower burner are not used. ROTARY FILTER: - Rotary filter is present along with first saturator. Saturators are connected with each other by pipes for solution way. Rotary filter take solution from saturator and filter it, dirty solution is drained and clean solution is supplied to the saturator. Small motor revolve the rotary filter. SAURATORS: - There are two saturators are present in machine. Saturator has seven guide rollers are up an eight are down. Saturator solution capacity
  24. 1250 liter, temperature of saturator 75C fabric capacity of saturator is 17 – 20 meters, desizing is done with the help of the enzyme desizing which is applicable at 7 PH. EXPENDERS: - There are three expenders are present in machine. The shape of expender is like banana. The function of expender, expend the width of the fabric. 1St expender is present between two saturator and 2nd is present after second saturator and 3rd is present along winding roller. PADDERS: - The functions of Padders squeeze the extra desizing solution from fabric. There are two Padders in machine. 1st is present between two saturator. 2nd saturator is present after second saturator. The weight is 1 ton. WINDING ROLLER: - Winding roller is present in the last of machine. This is winding the fabric on batcher. The quantity of the fabric on one batcher according to the quality of the fabric. Winder is a main roller in winding zone. After completing or rotating time fabric is ready for bleaching. DESIZING It is a process in which we remove starch from the fabric in order to get good dyeing results. Following types of desizing are carried out, Rot steeping Acid steeping Enzyme desizing
  25. Commonly used desizing is enzymatic /bio desizing. Working of KYOTO machine on desizing process :- There are two saturators from which desized the fabric. Now the fabric comes in 1st saturator there are seven guide rollers are up and there are eight guide rollers are below. First saturator have three, motors 2nd 4th 6th rollers are driven by three motors, at the top of 1st saturator exhauster present which exhaust the heat. After this the fabric passes through the Padder which are squeeze the extra desizing solution from fabric then fabric pass through the Dancer roller. Now fabric comes in 2nd saturator, 2nd saturator similar to first saturator. These saturators are connected by pipe. Desizing is done with the help of the Enzyme Desizing which is application at 7 PH Advantage of singing come desizing •Short process •Cheap process •High production •Less labor cost •More impurities are removed PREPARATION OF DESIZING SOLUTION a. First of all wash the tank b. The tank fills by 400 liter water and then staring. C. First of all salt is added as a (catalyst) then S.E is added then K.D(detergent) is added and then L100(desizer) is added. d. Tank fills by 1000 liter water. Measure 1000 liter water by rod.
  26. e. Start the chemical feed pump and open flow meter according to the using of chemical. f. Make a record how much is using. RECIPE: - For heavy quality of cotton L100 (Enzyme desizer) = 14gm/l KD (Detergent) = 6gm/l SE (sequesting agent) = 4gm/l NaCl = 5gm/l For heavy quality of cotton L100 (Enzyme desizer) = 10gm/l KD (Detergent) = 5gm/l SE (sequesting agent) = 4gm/l NaCl = 5gm/l Note: - After desizing the fabric batcher is kept for 6-8 hours in rotation to keep the desizer within the fabric. It is so because bacteria’s produced by enzymes take some time to eat starch. If we will keep it for longer time than a limit then bacteria’s will start eating fabric after finishing the starch, and if it will keep for a shorter time then starch could not be eat completely by the bacteria’s. The PH is maintained from 7-8 and the RPM is usually keeping 100. SCOURING
  27. Scouring is a process of removing natural as well as synthetic impurities. In this process maximum cleaning effect is produced with minimum effect on cellulose natural fibres contains oils, fats, waxes, minerals, leafy matters and notes as impurities that interfere with dyeing and finishing. Synthetic fibres contain producer “spin finishes” coning oils and knitting oils. Mill grease uses to lubricate processing equipment shift on the processing fabric and contaminate it. “The process of removing these impurities is called scouring” even through these impurities are not soluble in water and can be removed by extraction, dissolving. The impurities in inorganic solvent, emulsification, forming stable suspension of the impurities in water and saponification converting contaminates into water soluble compounds. CHEMISTRY OF OILS, FATS AND WAXES Many of contaminates removed in scouring both natural and man- made are fats, oils or waxes. Many useful products, some used in scouring are derived from them. FATS: - Chemistry fats and waxes are esters of fatty acids: fats also known as triglyceride, are abundantly produces by natural s vegetable oils (corn, olive, coconut, linseed and soy bean oil) and as fatty deposit in animal ( mutton, pork and fish another source of waxes is vegetable matter, predominantly the hard shing outer coated tropic leaves. TRIGLYCERIDE: - Regardless of weather it is of vegetable or animal origins, a fat can be either liquid or semi-solid. A major factor in determining the physical nature of the fat in the make-up of fatty acid compounds.
  28. FATTY ACIDS: - Fatty acids are long chain alkyl – carboxylic acid. The alkyl radical can be either completely saturated (saturated fatty acid) or (UN saturated fatty acid)most common chain length in nature is C18. 1-Scouring section of L-Box: - In the opening of the machine the fabric passes through two Draw rollers are plastic coated. They grip the fabric otherwise pull the fabric now fabric passes through the dancer roller, dancer roller keep tight the fabric. Then fabric pass through the Nomatic rollers, there are four Nomatic rollers opening of the machine. These rollers control the width of fabric. These rollers have air pressure. Now fabric comes in washing portion of machine, there are six washers opening of the machine. There maining desizing chemical present on the fabric, that is removed in washers. The temperature of water in washers depends upon the quality of the fabric. Mostly the temperature of water in fist washer is kept 92C and the temperature of other washer are kept 95C . the temperature of water in fist washer is kept 92C so that do not become creases or shrinkage. A single washer has 21 guide rollers. There are 10 guide rollers are above and 11 are below. Five motors are present on a single washer, which are revolving the guide rollers. Heat exchange filter take water from washers and drain. Heat exchange pump take this cool water and gives to heat exchanger. Heat exchanger warms the water at 60 and gives to washers. Sensors valve sense the temperature of water in washers if temperature of water is not according to the requirement then auto valve automatically opened after automatically are closed. Steam pipes along with the washers. Booster pump is also connected with heat exchanger, it gives fresh water to heat exchanger so that the
  29. pressure of water in heat exchanger maintain. Now the fabric comes in scouring saturators. There are two saturators, in which scouring solution is present. PREPARATION OF SCOURING SOLUTION • 400 liter water takes in a tank and stirring it. • Soda ash added in water • KEB dissolved in water • After dissolving there are mentioned thinks, stop stirring. • Now added caustic and measured by scale. • Further take water in a tank and tank fill by 1000 liter water. • The concentration of caustic soda checked according to gm/liter. • Start the chemical feed pump. • Flow meter opened according to the uses of chemical. • Checking the concentration of caustic from saturator after 5 or 10 minutes. • Make a record of uses chemical and how much concentration of caustic in saturator. CHECKING CONCENTRATION OF CAUSTIC FROM SATURATORS First of all we take scouring solution from saturators. 100 ml water takes in a beaker and then two or three drops of indicators added. Now we added 1 ml scouring solution by pipette in this beaker and we will start to added 0.1 concentration of HCl by burette. We will be
  30. added the drops of HCl, at that point the colour of beaker solution will be changed. It will be noted. NOTE: - The concentration of caustic is kept in saturator according to the quality of the fabric. If concentration of caustic is increased according to the quality of the fabric then flow meter is decreased. If concentration of caustic is lower according to the quality of the fabric then flow meter is decreased. MACHINE PARTS AND FUNCTIONS The length of the machine is 120m Draw roller, Dancer roller, Stray, Nomatic roller, Padders, Washers, Heat exchanger, Exhaust, Scouring and Bleaching saturator, Steamers Heat exchange, Filter, Heat exchange, Pump, Booster pump, Air compressors, Liquid feed pump, Feeding pump, Dryer DRAW ROLLER: - Draw rollers are plastic coated. The functions of these rollers are grip the fabric and pull out the fabric. DANCER ROLLER: - The functions of dancer rollers are keep tight the fabric. SCRAY: -The function of scray is when small quantity of fabric remains on the batcher, we are used stray so that the edge of fabric on batcher do not mistake. The fabric is felled on the stray slowly – slowly so that the edge of batcher fabric could be caught. NOMATIC ROLLER: -
  31. Nomatic rollers have air pressure. The function of Nomatic rollers are control the width of fabric. There are four Nomatic rollers at the opening of the L-Box. PADDERS: - The function of Padders are squeeze he extra solution from the fabric WASHERS: - When fabric come from desizing machine, at that time it has enough quantity of desizing solution it is removed in washers. There are six washers at the opening of the machine. There are 21 rollers in a washer. There are 10 are above and 11 are below 2,4,6,8,10 rollers are driven by motors. There are 378 (Three Hundred Seventy Eight) rollers in 18 washers. The temperatures of washers are kept according to the quality of the fabric. The washers are connected with each other with pipes. HEAT EXCHANGER: - The function of heat exchanger, re-warm the water. The heat exchanger pump takes cool water and supply to the heat exchanger. The heat exchanger after taking cool water and after re-warm gives to the washers by pipe. Heat exchanger warms water temperature 60C. second heat exchanger present after first steamer. This heat exchanger is also supply warm water to others 12 washers. EXHAUSTS: - The function of exhaust is exhausts the heat. There are 10 exhausts present in L-Box.
  32. SCOURING AND BLEACHING SATURATORS: - There are two scouring saturators. In these saturators fabric is treated with scouring solution. Liquid feed pump supply scouring solution to the saturators from solution tank by piping. After five or ten minutes, we check concentration of caustic. Bleaching saturators presents after 7, 8, 9, 10, 11, 12 washers. There are also two saturators. In which fabric is also treated with bleaching solution. In these saturators we are also check the concentration of caustic and H2O2. STEAMERS: - First steamer in L-Box has 64 rollers. At upper portion of steamer 13Plaiter rollers. The running of fabric among these rollers in Zigzag form, Fabric comes on conveyer. The conveyer is perforated from bottom, at the top of conveyer gaseous phase the temperature of these gaseous is 102C. Liquid Phase, water temperature is 100 C. Water change into steam and convey to the fabric. After conveyer tension rod is present which give tension to the fabric, the function of expender in steamer spread the fabric, control the width of fabric. The shapes of steamer expender like a spring. Now fabric comes in Mini Washing, present Padders, expender and steel rollers. We supply the hot and cold water to Mini Washing. Second steamer in L-Box has 17 rollers, other function similar to first steamer. If the speed of machine is running 90 meter/minute then fabric present in fist steamer and second steamer. 90 meter/minute * 50 steamer time = 4500 meter Fabric in First Steamer 4500 meter 90 meter/minute * 30 steamer time = 2700 meter Fabric in First Steamer 2700 meter
  33. HEAT EXCHANGE FILTER: - Heat exchange filter is taking fluff water from washers. It is connected by motor. It is separate the fluff from water and through water below, from this place heat exchanger pump take water and supply to heat exchanger. HEAT EXCHANGER PUMP: - The function of heat exchanger pump takes cool water and supply to heat exchanger. BOOSTER PUMP: - The function of Booster pump supplies fresh water to heat exchanger so that the pressure of water maintain in heat exchanger. AIR COMPRESSOR: - The functions of air compressor maintain temperature in panel so that the working of panel do not disturb. For example: - Inner panel temperature 28.7C Outer panel temperature 45.5C LIQUID FEED PUMP: - Liquid feed pump supply scouring solution to the saturators from solution tanks by piping. FEEDING PUMP: -Mostly after maintenance of machine, a lot of solution is required in saturators in a single passage. Therefore for supply of solution from solution tank we use feeding pump it is also called a direct feeding. DRYERS: -
  34. There are 48 (Forty Eight) dryers are present at the end of the machine. These dryers arrange in 4 columns. Each column contains 8 dryers and a tension roller lie b/w two consecutive column to maintain the tension. After passing through 44 hot dryers then fabric pass through 4 cool dryers. In last four dryers cool water is present so that temperature maintains pressure in dryers 0.35 MPa. TYPES OF ROLLERSFEED ROLLERS: - Feed rollers used to control the speed of cloth in the machine. DANCER: - It is use to maintain the tension in fabric. It is also adjust according to the quality of the fabric. SEQUEEZ ROLLERS: - It is use to maintain the pickup of fabric. The pickup also adjusts according to the quality of the fabric. SPREAD ROLLERS: - It prevent the fabric from creasing
  35. MERCERIZER RANGE OBJECTIVES  To increase luster.  To increase the affinity for dyes.
  36.  To increase the tensile strength.  To give dimensional stability  Use of dye after mercerizing is less  Width control INTRODUCTION This is a typical treatment for cotton yarns and fabrics, which improves the fabric luster and wettability, ensures a covering effect for dead cotton improves dimensional stability and dyeing efficiency. This treatment is carried out using caustic soda (28 - 30° Bé), which determines the contraction and swelling of the fibres; they become translucent and increase their tensile strength, but reduce their flexural and torsion strength. The bean-like section of the fibre becomes first elliptic and then circular, allowing a better reflection of light with a consequent increase of luster. The treatment is usually carried out under tension, with caustic soda at 28°- 30° Bé (approx.270- 330 g/l). If the concentration is lower than 24° Bé, the treatment is called causticization and aims at enhancing the dyeing liquor penetration into the fabric. The liquor temperature usually ranges between 15- 20° C and its uniform absorption is assured by adding mercerising wetting agents stable in alkaline environment. Once the operation has been carried out, alkalinity must immediately be neutralised by means of a diluted acid solution. From a chemical point of view, alkalicellulose is the first material to form; the next material, which forms after repeatedly water washing is hydrocellulose, which is more reactive than natural cellulose. Cotton wetting entails shrinkage of the material, which must be kept under tension, to avoid a fuzzy appearance. Mercerising is carried out on yarns, fabrics.
  37. As far as yarns are concerned, before the mercerising process in special machines, they undergo a singeing treatment to remove the fuzz and end fibres. which could otherwise prevent the perfect reflection of light after mercerising. There are two different types of machines to be used for woven fabrics: a chain system and a cylinder system. Chain mercerising: with the chain mercerising process the fibres achieve perfect brightness thanks to optimum tension control. This system runs slowly and allows no flexibility when the width of the fabric varies. The sodium hydroxide concentration is brought down to approximately 4 ° Bé by means of a circular shower. The fabric is then washed, neutralised and rinsed. Another well-proven mercerising agent is liquid ammonia, which has to be applied for very short times (about half a second). There are very few systems based on liquid ammonia due to the difficulties connected to the use of liquid NH 3 (toxicity, formation of blends that can explode in presence of air and very strict regulations concerning the welding of steel sheets used to build these systems that operate at very high pressures since the boiling point of ammonia is usually -33°C). Chain Mercerizing Chain mercerizing is done on a range equipped with tenter chains for tension control. The range consists of a pad mangle followed by a set of timing cans and then a clip tenter frame. Fresh water cascades onto the fabric to remove the caustic soda as it is held tensioned in the tenter frame, . The length of the frame must match the range speed and assure that the caustic level is reduced below 3% before tensions are released. The tenter frame is followed by a series of open-width wash boxes which further reduces the caustic level. Acetic
  38. acid is in one of the last boxes to complete the neutralization of caustic. Procedure 1. Apply 22 to 25 % (48 - 54" Tw) caustic at the pad mangle at 100 wet pickup. 2. Pass fabric over timing cans. The number of cans must correspond to the range speed and provide at least one minute dwell time. 3. Clip fabric onto tenter chains and stretch filling-wise while maintaining warp tension. 4. Run fabric under cascade washers to remove caustic. Keep under tension until caustic level is less than 3% otherwise fabric will shrink in filling direction. This width loss is impossible to recover later. 5. Release tension and continue washing in open- width wash boxes, to further reduce the caustic. 6. Neutralize with acetic acid in the next to last wash box and rinse with fresh water in the last. It is important to control these steps because it is important, in down-stream processing, that the alkalinity remains consistent throughout all production. Chain Mercerizing Range Diagram
  39. Points of Concern and Control For best results, goods should be dry entering the liquid caustic impregnation unit. Need to get uniform and even caustic pick-up through out the fabric. Wet pickup must be at least 100 %. A certain amount of liquid caustic must surround each fiber to provide proper lubrication so that the fibers can be deformed. Caustic solution and impregnated fabric temperatures should be controlled between 70 - 100F. Above 110 F, there is a noticeable decrease in luster of the Mercerized goods. Below 70 F, there is no noticeable improvement. Proper framing during the washing step is crucial. The goods must be maintained at greige width to one inch over greige for maximum luster. The tensioned width must be maintained through out the caustic removal operations otherwise the fabric shrinks and luster is lost. If optimum washing is obtained. there will be only a slight loss in width as the goods come off the tenter clips. Caustic Concentration Units Caustic concentrations, expressed as percentages, are ratios calculated as weight caustic/weight solution. However the specific gravity or density of the solution(weight/volume) is directly related to the concentration. Calibrated hydrometers are used to determine specific gravity. The calibration scales most often used on caustic solutions are Twaddle (“Tw) and Baume’ (“Be’). Polyester/Cotton These can be handled under the same conditions as 100 % cotton. Even though polyester fibers are sensitive to caustic, the temperature and time the fibers are in contact with Mercerizing strength caustic are insufficient to cause fiber damage. One problem with polyester/cotton blends it that they may not be as absorbent as 100 % cotton fabrics coming to the caustic saturator. This is because they
  40. have not been given the same thorough scouring and bleaching as 100 % cotton. In this case, special penetrating agents are needed to help the caustic solution wet out the fabric. Machine make : Sando iron works, Wakayama Japan. Threading length: 350metre Process flow of mercerizer machine Fabric inlet Caustic Saturator 1 Timing cylinders Caustic Saturator 1 Timing cylinders Tenter chain Washing bath (4) Neutralizing bath Washing bath (3) Drying range Plaiter Parts of Mercerizer Machine Guide roller, Timing cylinders, Feed roller, Caustic Saturator, Tenter chain, Washing
  41. bath, Shower, chilling unit, Neutralizing bath , Dancer roller, VDR, Plaiter. Guide roller It is guide the fabric on the machine. Without guider fabric is not possible to running of continuous process. It is stop the making of the crease. It is also known as cloth guider. Tenter chain It is stretched the fabric on the mercerizer. The tensions are set according to the fabric. It is control the shrinkage on fabric. Without this chain fabric is easily shrink. Chilling unit The chilling unit is provided on the mercerizer to control the temperature of the caustic. Feed roller It is give the motion of the fabric. Without feed roller fabric are not run to machine. It is attach the starting and end point of machine. Caustic Saturators The caustic saturators only caustic are add 240gpl. The fabric are dip in the saturator and squeeze it. In the mercerizre two saturator are used. Timing cylinders After by dipping of caustic solution. Fabrics are passing through the cylinder and give the time. So it is known as timing cylinder. Shower It is spray the hot water on the fabric. In the mercerizer 5 showers is used. Neutralizing bath In this bath fabric is Neutralised used of Neutra acid or Green acid. It is save the damaging of the fabric. Washing bath In the washing process extra chemical is remove on the fabric surface. In the washer only water is used.
  42. VDR It is dry the fabric after by the washing. In the vertical dry range steam is used. It is give the heating of the cylinder. In the VDR hot and cold cylinder (27 hot and 3 cold cylinders) are used. Dancer roller It is maintain the tension of the fabric. It is information speed of the motor. It is save the damaging of the fabric. Plaiter The fabrics are out on the plaiter. It is stop the making of creases. It is help collection of the fabric on the trolley. MERCERIZER - 2 After mercerizing increase cost of fabric Rs 2.70 per meter In this process cotton is dipped in a solution of NaOH so that NaOH penetrated in to the fibre and then NaOH is washed out completely by neutralizing by dilute acid like sulphuric acid. When mercerizing fibre are examined under microscope. It is seen that each fibres in twisted ribbon like form. After mercerizing fibres become cylindrical and free from twists. To increase the luster cotton must be prevented from shrinkage. This can be achieved by stretching the yarn or fabric. Shrinkage of the fabric can also controlled by mercerization. INSTRUCTION FOR CHILLER OPERATOR 1-How much Be are required according to this Be prepared but for 28 Be, 26 Be or 20Be prepared according to program.2-In order to grey fabric 12, 18, 15 caustic Be prepared according to program] PREPARATION OF CAUSTIC 1-For preparation of 26 Be caustic, take 1200, 1200 liters 32 Be caustic in both tanks. 2- For preparation of 26 Be caustic in PIT, open the caustic valve and along with the water valve. When 26 Be should be prepared, circulation of caustic start so that caustic should be cool.
  43. 3- For preparation of 26 Be caustic, take 35 Be caustic and for preparation of 35Be caustic, 300 liters 48 Be caustic take in to 32 Be caustic. 4- CHANGE OF Be:- when Be of caustic is changed, for change 20 Be from 26Be, take 48 Be caustic and down the PIT and open the supply of water. Similarly 26 Be caustic should be prepared. 5- For preparation of 2o Be caustic, down the PIT and open the supply of water. Similarly 26 Be caustic should be prepared. 6 - When operate the machine, clean the filters at caustic supply. 7 - After each half hour note the Be of saturators, Titration and Temperature. 8 - During operation check the there is no problem in compressor and condenser and which is coming water from cooling tower, it is cool. CHECKING Be:- Take water into TIP from PIT and keep Be meter into TIP. Now reading noted. 9 - Temperature of chiller should be 25C. 10 - After every week wash out the Heat Exchanger. METHOD OF CHILLER OPERATING 1- First of all operate the cooling tower 2- After this operate the brine pump 3- After this operate the compressor during this check the all valve of operation.
  44. WORKING OF MACHINE There are two saturators of mercerizing machine. The solution capacity of each saturator is 700 liter. The solution comes from TIP. When solution above a limit again come into TIP. NaOH pump take solution from TIP and supply to the heat exchanger. Brine pump take water from chiller and supply to the Heat Exchanger, from heat exchange again solution come in to saturators by piping. When we required change the Be, take solution from TIP and give to third tank and again solution is prepared. When solution come from saturators Rotary Filters clean the solution. Fluff is drained and solution comes in to TIP. Similarly this circulation continues. After passing fabric from 2nd saturator come on stenter, at the beginning of the stenter Selvedge Guider, which are maintain the width of the fabric. Scale is present on chain, on this scale mentioned the width of the fabric according to the chain. There are Seven Shower Pump, these shower pump are supplying solution to the fabric. There are Seven Suction Pump, these pump suck the solution. Stenter wheel are revolving the chain. These are driven by motor. After this 11(Eleven) washers are present. The temperature of washers is 95C after these 48 Dryers are present. Last four dryers have cool water so that the temperature maintain. NOTE: - The capacity of machine is 480 meter fabric TYPES OF MACHINARY: There are two types of mercerizing machines. 1-Chain type mercerizing machine 2-Chain less type mercerizing machine.
  45. Chain type KOTO JAPAN MACHINE parts and their function are following MACHINE PARTS AND FUNCTIONS Enterence, Saturators, NaOH Pump, Be control valve, Brine Pump, Brine control valve, Recovery pumps, Rotary Filter, Chain Wheel, Selvedge Guider, Shower Pumps, Suction Pumps, Washers, Dryers, Heat Exchanger ENTERENCE: - After bleaching of the fabric is ready for mercerizing. Enterence section contains guider tension rollers and spreaders. Fabric passes all these rollers so that fabric contains no crease. Fabric passes through 4selvedge rollers so that stretch the fabric in order to remove selvedge crease. This zone also has a scray. It is also very important part of Enterence. It is used when there is need to change batch of fabric. When fabric of J- Scray runs the tension of cloth guider is increase because there is more chance of crease. 1- SATURATORS: - There are two saturators. The capacity of solution of each saturator is 700 liter. it contains caustic solution of required bombe. It contains three squeezing rollers and 2 spreaders and 8 Padders. 2- NaOH PUMP: - NaOH Pump is taking solution from TIP and supply to the Heat Exchanger, give solution by piping to the saturators.
  46. 3- BE CONTROL VALVE: - How much quantity of Be is required? It is taken in a TIP from mixers by operating Be control valve. It is being operated from panel 4- BRINE PUMP: - The function of brine pump is circulation of water. Brine pump supply water to the heat exchanger. 5- BRINE CONTROL VALVE: - Brine control valve control the quantity of water. The working of Brine control valve is automatically. It is being operated from panel. 6- RECOVERY PUMPS: - When we changed the Be of TIP, we take solution from TIP by first recovery pump and through into third tank. The second recovery pump is present below showers. This pump takes solution and give to the Recovery Pump. 7- ROTARY FILTER: - Rotary filter, filter the dirty water. It drains the fluff and again supplies water to the washers. 8- CHAIN WHEELS: - These wheels give direction to the revolving chain. The length of the chain section is 30 meter and total chain on one side is 60meters the chain having no of clips. At the start of clips of chain there is a circular plate that is also moving with the speed of chain or clips. The function of the circular plate is to open and closed the clips; in start we keep the width of the chain according to the width f the fabric. When fabric run some meter width of the chain is set to the required
  47. width of the fabric. Open the chain width wise very slowly because there is a large chance of fabric tear. After some distance chain contains 7 showers that shower caustic solution almost 8 bombe on fabric. This is come from 1st and 2nd washer of mercerizing machine. The purpose of these showers of caustic is to make sure the well penetration of caustic solution in fabric. 9- SELVEDGE GUIDER: - Selvedge Guider, control the selvedge of the fabric. 11- SHOWER PUMPS: - There are seven Shower Pumps are present. The function of shower pumps supply solution to the fabric. 12- SUCTION PUMPS: - There are seven suction pumps. The functions of suction pumps are sucking the solution. 13- WASHERS: - There are 11 (Eleven) suction pumps are present. There is difference between first 3 and remaining 8. There difference is their construction is change and their capacity of water is changed. First 3 having 5 rollers up and 6 down and other washer having 10 up and 11 down. The capacity of water in first three washers 1000 liter and other washer having capacity of water 1500 liter. The temperatures of all washers are 90 C for cotton and for cotton Lycra quality is 95 C . 25 meter fabric in single washer. 4-DRYERS: - There are 48 (Forty Eight) dryers are present at the end of the machine. The function of dryer is dry the fabric. These dryers arrange
  48. in 4 columns. Each column contains 8 dryers and a tension roller lie b/w two consecutive column to maintain the tension. After passing through 44 hot dryers then fabric pass through 4 cool dryers. In last four dryers cool water is present so that temperature maintains pressure in dryers. The dryer pressures are 0.35MPa. .15- HEAT EXCHANGER: - The function of Heat Exchanger, exchange the heat of the NaOH. IDENTIFICATION OF MERCERIZED COTTON Mercerized cotton can be identified by its microscopic view. Cotton fabric naturally flat and twisted (ribbon like) after mercerizing fibre swell, untwist and their cross section change in to round form. CONDITIONS • Cotton should be free from sizes and other impurities. If these are present then mercerized solution should not well penetrate completely in fabric. • Temperature required for caustic solution is 25 – 30 C. •NaOH is used for this purpose because it is cheap. KOH is also used but it is expensive. PRECAUTIONS • Concentration of NaOH • Machine temperature • Extraction of alkali • Steaming time • Time
  49. • Proper cleaning of machine • Same lot of fabric should run at same speed. • Concentration of alkali should be same for al lot of fabric. FAULTS 1. If a thread remain in a clip then clip disable to grip properly. 2. If alkali remains in fabric for long time then fabric will weak also white sport appear on fabric. NOTE: - If want to cure fabric before dyeing then we do mercerizing after curing because if we do mercerizing before curing then due to presence of alkali give yellowness to fabric. NAOH Be/Gpl Be G / L 6.7 48.9 12 86.7 18.8 157.9 19.8 169 20.9 181 22 194 23 206 24 219 25 231.8 26 244.9 26.9 258 27.9 271 28.8 285.2 29.7 299 30.6 312 38 450 50 772 Sueding (Peaching)
  50. This operation is often carried out before the raising process to reduce the friction between the fibres making up the cloth and consequently to facilitate the extraction of the fibre end. The sueding process is carried out on both sides of the fabric and modifies the appearance and the final hand of the cloth; when touched it gives a soft and smooth sensation similar to the one given by a peach-grain surface. The sueding machine is made up of some rotating rollers coated with abrasive paper, which emerise the cloth and produce a more or less marked effect depending upon the pressure exerted on the fabric by the abrasive rollers. The abrasive paper used can vary according to the desired sueding degree and must be replaced after a given number of operating hours, or when it does not properly carry out suitably the sueding function. In some cases, it is possible to use also metal rollers with the surface coated with uneven and rough grains or pumice rollers performing an excellent sueding action on both dry or wet fabrics. For a very superficial sueding, the natural abrasive power of pumice can be applied with successful results. Gray fabrics as well as dyed ones can be subjected to the sueding process; the cloth to be emerised must be completely free from any finishing resin or adhesive substance remaining on the fabric surface after desizing. The sueding process reduces mechanic and dynamometric resistance of the fabric, thus making it more subject to tearing and seaming. The fabric can run at different speeds inside the sueding unit; a smooth pressure is kept thanks to two balancing arms assembled at the entry and at the exit of the unit. The pieces of cloth must be sewn with abrasion-resistant material such as polyester or nylon. The gears must be suitably cleaned with compressed air jets since the presence of pile residues could clog the ball bearings or drop again on the fabric surface thus creating some problems with dyeing machines filters.  Variable of peaching :-
  51. 1. Fabric speed 2. Tension 3. Energy of pile 4. Energy of counter pile 5. Moisture of the fabric The speeds are increasing the peach less done. Some factor are depends upon the type of emery paper.  The emery paper is three type :- 150grid 220grid 600grid The diamond paper are to type :- 200grid 400grid  PEACHING In this process fabric is rubbed by emerising surface to raise hairs from surface, gives a unique softness and napped surface – technically known as PEACHING EFFECT.  CHECKING OF PEACH FABRIC Peach effect are judged by touching fabric surface by hand. Quality of peach is a subjective issue, varies from person to person.  ROOT CAUSES OF UN-EVEN PEACHING Un-even mercerization process change in process condition
  52. or concentration of caustic.Faulty batch preparation. Unwinding tension of batch at feeding end of peaching.Worn out emerizing surface.Side-wise shifting of fabric on emerizing drum-causes LMR(left, middle, right) peach variation.Moisture in fabric in case of trolley feeding very crucial. PARTS OF PEACHING MACHINE FEED ROLLER TENSION ROLLER DANDY DRUM PILE COUNTER PILE PRESSURE GAUGE BRUSHER EXHUAST COUNTER METER FLUFF CATCHER In the Auro textile Xetma and Lafer machine are used.
  53. Sueding machine diagram Xetma Machine It is made in Germany. In the machine 24rolls are used. In this 12rolls called pile and other rolls called counter pile. Pile are move in fabric direction and counter pile are move in the opposite direction. Pile is cut the surface of the fabric. Counter pile are make a smooth surface of the fabric. The pile and counter pile speed is not an equal. In the process fabric weight and strength are decrease. In this machine emery paper and brusher are also used. The brusher case six brushes and six counter piles are used. The exhaust is remove the fluff on the machine. The beater is remove the fluff on the fabric surface. The feed roller is given the motion of the fabric. The pressure gauge is given the tension of the belt. Without pressure gauge machine are not run. The dancer roller is maintain the tension of the fabric. In the xetma machine one dancer roller are used. The 3
  54. tension rollers are used in the xetma machine. It is give the tension of the fabric. Process flow of Xetma machine Batch Padding mangle Drying range Sueding unit Brusher and beating unit Plaiter Lafer machine It is made in Italy. In the machine 24rolls are used. In this 12rolls called pile and other rolls called counter pile. Pile are move in fabric direction and counter pile are move in the opposite direction. Pile is cut the surface of the fabric. Counter pile are make a smooth surface of the fabric. The pile and counter pile speed is not an equal. In the process fabric weight and strength are decrease. In this machine diamond paper and brusher are also used. The brusher case six brushes and six counter piles are used. The exhaust is remove the fluff on the machine. The beater is remove the fluff on the fabric surface. The feed roller is given the motion of the fabric. The pressure gauge
  55. is given the tension of the belt. Without pressure gauge machine are not run. The dancer roller is maintain the tension of the fabric. In the Lafer machine two dancer rollers are used. The 3 tension rollers are used in the Lafer machine. It is give the tension of the fabric. Process flow of Lafer machine Batch Sueding unit Brusher and beating unit Plaiter Soaper Machine It is made in Japan.The soaper machine only soaping and washing is don.It is remove the extrachemical on the fabric surface.In the soaper machine 9 washer is used.the first and last washer cold water is used.In the chamber only cold wash is done.The 4to5 no. washer soap solution is used. It machine is also used for gray washing. The gray fabric is wash at temperature 85-90 o c. In the soaper machine pH meter are used in washer no 8. PROCESS FLOW INLET SECTION WASHER
  56. SOAP SOLUTION BATH (washer no.4 to 5) NUTERLISATION BATH (WASHER NO. 8) WASHER VDR PLAITOR DYEING
  57. DEVELOPMEN T Pad-dry machine Introduction It is made in Japan. It is a continuous machine. The fabric threading is 160 meters. In the pad-dry machine the fabrics is pad in the dye and dry it. The dyes are not fixed on the fabric surface in the machine. After by padding the fabric go to the I.R.(Infradrol) unit. The fabrics are passing through the I.R. on the horizontal form. After by the fabric is going to the hot flue chamber.
  58. In the chamber steam is used drying purpose. The steam is passing through the chamber on the pipe. PROCESS FLOW OF PAD-DRY MACHINE INLET SECTION COOLING CYLINDER PADDING MANGLE IR HOT FLUE CHAMBER COOLING CYLINDER PLAITOR It is a machine which is used to pad, dry and cure to all kinds of fabrics. This machine is categorized under continuous process of dyeing. Machine details of pad-dry:- Pad-dry consists of following parts that dye and guide the fabric during dyeing
  59. Batcher, Guide rollers, Cooling drum, Cooling jacket, Trough, Squeezing rollers, Padder, VTG rollers, IR-dryers, Drying chambers, Radiator, Heat exchanger, Hot flue chamber and Plaitor. Now we will see these parts individually. Batcher:- When the fabric is taken to dye, it is in the form of batcher that is taken after mercerizing. The fabric width depends on the size of the batcher and the fabric of different length is winded on it . This length may vary from 100 to 70,000 meters. Guide rollers:- These are the rollers which are used to guide the fabric from different paths. Their function is only to direct the fabric toward it’s outlet. Cooling drums:- When the fabric is taken from the mercerization then its temperature is more than the limit. In this state the fabric cannot be react properly with dye in the trough. So we use cooling drums in which water is circulating and the temperature of fabric is decreasing gradually. Their diameter is large as cylindrical to other rollers that is ranges from 26’’ to 30’’. Cooling jacket:- This jacket has very important role in cooling the dye bath. It is necessary because in hot form dye cannot react with the fabric. Cool water circulate within this jacket Trough:-
  60. It is the first main part of this machine. This part is filled with liquor which is filled with dyes and chemicals. It’s capacity is nearly 1400lilres. It is dozed manually as well as automatically. The temperature of this bath is room temp. the fabric capacity is 1-1.5m within this dye bath or trough. following recipe is used in this trough, • Dyes • Urea (moisturizing agent) • Soda ash( for reactive dyes) • Sodium bicarbonate(for pigments) • Primazol FFAM (anti-migrating agent) • NF Cooling jacket:- It is a jacket that is used in outer side of the trough. This jacket is used to make the temperature of liquor cool down, because if it will not cool down then the dye liquor will not react properly. Squeezing rollers:- These rollers have function just to squeeze the fabric which is dipped in dye bath. In this way dye can react completely with the fabric. It is a pair of roller that moves in opposite direction and squeeze the dyed fabric. They are rubber coated and have diameter8’’. Padder:- This is the main part of the machine. All the pick-up of dye depends upon the padder. It is a pair of two rollers. Two rollers move in opposite direction to each other. These rollers are also rubber coated but have special type. L-C-R(left-center-right). This is the most sensitive factor that requires more concentration than any other part.
  61. Basically L-C-R fault means that the fabric dye is varying from left, right and center. We can say that there are three parts of padder on which pressure is adjusted to avoid L-C-R fault. This pressure varies according to the width of the fabric and pickup of dye. Usually pick- up is 60%. VTG-rollers:- These are called vertical tensioner guide rollers. These are the rollers that give tension and rest to the dyed fabric and fabric contact with air. There are 9 rollers that are used for this purpose,5 above(driver) and 4 down (driven). The structural diagram is shown in the following fig. These rollers contain 9-10 m fabric within their area. The time taken by the fabric on these rollers is 10-12seconds.
  62. IR dryers:- These are called infra-red dryers. IR-dryers are also called pre-dryers. 30% of fabric is dry in this section. The temperatures of these dryers vary from 1000-1300 0 C. These dryers have very important role in dyeing the fabric uniformly. The fig. of IR is shown as follows, when the fabric is passed from the padder then there is an uneven dyeing that causes the face-back problem on the fabric. The structural diagram of the dye particles shown in the figure after padding as Two IR are used for heavy quality and one is used for light quality. And when the fabric is passed through the IR dryers the dye par2ticles migrate from surface to the core of the fabric with help of infra-red rays. After passing through IR the dye particles are shown above on the fabric surface,
  63. Drying chambers:- There are two drying chambers used for thermo-soling .These are the chambers where thermo-soling is done. The fabric passes through the rollers in the chamber and thermic oil react with fabric in these chambers. The diagram is shown in the following fig. The thermic oil is given to the chambers in pipes attached to the radiator and it circulates within the chamber with the help of circulating fans. The fig. of heat exchanger is shown in the following fig The temperature of these dryers vary with quality of the fabric and dye stuff used because different dye stuff have different range of temperature for its fixation , 20% fabric is dry in these chambers.
  64. Plaitor :- This is a device that converts the straight fabric into pile form. It is used for the trolley outlet. If there is batcher at delivery then it is not used, but usually trolley is used after scary. Light box:- When the fabric is delivering then it is checked in a light box after 500m or 700mdepends on the requirement. L-C-R (left-center-right) of the fabric is checked in this box to avoid shade variation from all sides. There are few kinds of lights under which fabric is checked, it is also depends on the requirement of the customer. Day light D-65Sun light Ultra violet Fluorescent light Pad-steam It is a machine that can dye, steam and wash the fabric. It is an important part of continuous dyeing. When the fabric is dyed then washing is required so we use pad-steam after thermo-sol range. In case of polyester/ cellulose blended fabrics we use this machine for developing, steaming and washing of the fabric. Parts of machine There are following parts of machine that are responsible to handle the fabric during pad-steam processing, • Feed rollers • Cooling cylinders
  65. • Padder • Trough • Steamer • Washing boxes • Drying cylinders some parts are studied in pad-steamer topic remaining’s are given as follows, Steamer:- It comes right after padder it is a main part of the machine which is used for steam the dyed fabric. The temperature of this section is 100°C. the fabric remains here according to the dye stuff given as follows Washers:- There different amount of boxes in different machines prepared by the companies. These washers are suitable for Washing, Rinsing, Soaping, Oxidation and Soaping is necessary to remove unfix dye particles from the fabric and then it is washed. Oxidation is the Pigment dyes not required Direct dyes 60sec Vat dyes 30-40sec.(103-105 °C) Reactive dyes 40-6-sec (102-110°C) Sulpher dyes 30-45sec (102-110°C) Combination of disperse and vat dyes 30-40sec.(102-105 °C) Combination of disperse and reactive dyes 30-40sec.(102-105 °C)
  66. process in which the vat dyes are developed. In first padder reduction is done and in second padder of pad-steam oxidation is carried out to resize the dye particle of vat dyes. That is why vat dyes have very good washing fastness. The temperatures of these washers are set according to the process and dye stuff. It will discuss in last topic. Objectives of the washing concept and recycling systems The most important objectives during the realization of the new washing concept are reduction of the wastewater load (COD) and simultaneously lowering washing water and steam consumption. Referred to here is the water consumption of the entire system and not that of the washing machine alone. In spite of the latest washing machine technology and already extremely low water consumption values, further significant reduction of the effective water consumption can be still achieved by wastewater circulation. Recycling the waste water is therefore an important derivative of the main objectives. A further objective of this project, originating from the fact that re-using the wastewater requires the impurities to be separated from the water, was to produce concentrates. Concentrates can be produced either directly at the place of origin (washing machine) or indirectly on the membrane plant. The concentrate quantities formed should be small or thermal disposal should be possible. Large quantities of effluent sludge are undesirable. The machine concept The installation referred to is a BENNINGER high-efficiency washing machine, operating with the counter flow principle. This means that the fabric and the washing water flow in opposite directions. The machine concept includes the following standard modules:· High humidity impregnation (with variable liquor application)· Bi-functional React a roller-steamer, used as either a washing compartment for pre-washing the dyed fabric or as a steamer
  67. for pre-treatment processes· 6 vertical roller vat washing compartments with Extractible-on rollers· 2 Hydrovacvacuum suction stations The special features of this technology lie in the combination and operation of the components and the design of the washing liquor guidance The BENNINGER EXTRACTA roller vat high-efficiency washing machine is especially suitable for counter flow washing since each washing compartment contains up to 7additional washing chambers (fig. ). The fabric is squeezed through pneumatically loaded lay-on rollers situated between each washing chamber. The washing liquor meanders with in the compartment according to the counter flow principle, meaning that the liquor flow is guided in the opposite direction to the fabric run. This method of processing results in a high concentration of wastewater ingredients accumulating contrary to the fabric run. Other well-known washing systems such as horizontal or diagonal washing machines, which circulate the liquor, are not suitable for this application because there are only a maximum of 2 chambers per-washing compartment. The concentration variations in the washing water are therefore considerably less. Diagram: - High-efficiency washing machine with bi-functional steamer The parameters of the washing machine can be set at will and are maintained thanks to the modern control system. This enables the
  68. various tasks in respect of water, counter flow and process guidance to be realized. Physical problems in continuous dyeing PROBLEMS IN DYEING 1. General Problems / Non -Technical Problems 2. Process Dependent / Technical Problems 1-General Problems / Non- Technical Problems: - These problems occur due to wring calculation, wrong recipe, not good stirring, tint and water marks etc. Stains: - Due to aggregation Due to dirty machine Chemical and dye solution aggregation. Improper dye dissolution Non uniform dispersion Tint: - 1-Tint occur due to dirty machine 2-Process Dependent / Technical Problems CONTINUOUS METHOD: - LISTING: - This is (L.C.R) left center right problem. Shade different from left to right reason may be migration, uneven squeezing. BACK FACE: -I.
  69. Mechanical Problem: - I.R pre-drying not well Pick up should be 65% Should be control air circulation II. Chemical Problem: - Anti-migrating agents Thickeners TAILING: - This is major problem shade difference from start to end. I.Tone Tailing: - When fabric run on a machine after some meters there is a tone difference from start and after some running. Reason is affinity difference. II Depth Tailing: - This is a depth (light or dark) shade variation is a fabric. Affinity Dyes Depth Tailing Non-affinity Dyes Reactive dyes are affinity dyes and vat dyes are non-affinity dyes. NOTE: -Yellow more affinity then blue, yellow rush to fabric. There is more yellow% age in solution. To avoid this same class of dye like Ramazol is use. PENETRATION PROBLEM: -
  70. For good penetration Moisture Content, pressure, temperature, time should be same. If penetration is good washing, rubbing and light fastness is good. Normally (40 – 60 sec)1050 C is required. It is controlled in steamer. FIXATION FAILURE: -  Not required chemical concentration if we get.  Not proper temperature  Not proper pressure UN – EVEN DYEING: -  Shade variation occurs if dry chamber temperature is not well.  Speed variation  Error of dye weight  Not proper color mixing  Wrong chemical formulation  Temperature of chemical solution not maintained  If washing is not done with proper soap concentration In continuous dyeing there are so many chemical and physical problems occurs during continuous dyeing. Continuous dyeing is divided into following parts .Some of physical problems are given in details in the following, 1. Padding process 2. The drying process 3. Fixation process 4. Washing process for unfixed dye particles
  71. 1-Padding process In this process the fabric is passed from padder after passing through trough containing dye sand chemicals. There are four rollers in the trough. There is one pair of squeezing roller center. The special designed rollers are slightly different in diameter which is technically called as crowning. 2-Drying process The padded fabric should be immediately applied “drying” to satisfy the next fixation treatment of the padded fabric. Since dye stuffs have not yet fixed with the fibres in this process, the migration phenomenon is occurred where by dyes tend to move alongside Moisture evaporating during drying not only from the inside of fabric to the surface but also from center to the both sides. Even if dye is applied to the fabric uniformly in a padding process, migration during drying process is liable to create such problems as un-levelness listing and poor appearance. It is necessary to formulate padding recipes and drying conditions that will minimize the migration as much as possible. Drying machines:- There are two drying machines that are used for drying purpose • Hot flue dryer • Infrared dryer Hot flue dryers are generally work on jet system. Hot air is fall uniformly over the fabric through jet. They are also called drying chambers their diagram is shown as follows, Whereas infrared dryers are basically rays that across the fabric from both sides and it is vary
  72. use full in migration of the dye particles from the core to surface of the fibre. Although they have no high efficiency as the movement of the water particles over the fabric surface is rather slow. The infrared dryers are shown as follows, so for having high efficiency we use hot flue and infrared dryers combined. 2- Phenomenon of migration:- Migration is the process by which a dye moves around the fibre or level itself. The migration process comprises adsorption of dye onto the fibre surface, migration through the dye liquor, re-adsorption onto the fibre structure. Migration itself is also heavily influenced by temperature. The phenomenon of dye migration on polyester/cellulose blended fabric is classified into two phenomenons 1-The movement of dye particles to the surface of fibre during drying process. 2-The movement of individual dye molecules into the interior of fibre during thermo-soling process. Relation b/w drying mechanism after padding of dye solution and phenomenon of migration of dye molecules to the surface of the fabric is considered as follows. First the water evaporates from the surface of the fabric by the thermal energy from heat source and the water content decreases on the surface of the fabric. The difference of water content b/e the surface of fabric and the interior causes the water movement from the interior of the fabric to the surface by capillary action. The water begins to evaporate when reaching the surface but the dye particles moving along with remain and accumulate on the surface. Some of the vapors produce near the surface of fabric begin to evaporate as result of the difference in vapor pressure. The rest of three vapors move into the interior of
  73. fabric and transmission of heat happens quickly inside of the fabric. The vapors moves into the interior of fabric are recommenced to liquid and move again to the surface of fabric. After consistent drying is repeated, the movement of water from the interior of fabric to the surface eventually ends. 3-Factors affecting migration:- Air speed In hot air drying, air speed provides the most prominent influence on the rate of drying and simultaneously influences upon migration. Temperature:- The temperature of hot air for drying is not as effective on migration as air speed. In general the effect of temperature difference on migration decreases considerably at temperatures higher than 1000 C. Humidity:- Humidity has no effect on migration practically. On the other hand, the moisture in the hot air is liable to lower drying efficiency by slowing the drying speed and simultaneously create a difference in concentration between the surface and the backside of the dyeing’s. Consequently dyeing should be carried out under low humidity as much as possible. Infra-red dryer:- In hot flue drying, the temperature of padded fabric cannot reach over 50-600 C on wet bulb until the water completely evaporates from the padded fabric. In infra-red drying, on the other hand, the temperature of the padded fabric can be in crease to boiling point. The material is swelled and the dye penetration into the structure if
  74. the fibre is improved., more over since the bound water in cellulosic fibre become larger by increasing temperature. The volume of free water in the fibre decreases and the migration become smaller. However an excessive radiation of infrared ray will result in drying under boiling conditions , by which the drying is accelerated and simultaneously migration become larger , therefore the proper radiation of infra-red ray should be applied. The most effective drying method generally follow this sequence , 20-30%water of pick-up ratio of the padded fabric is generally dried by the radiation of infra-red rays. Relation between water contents and migration: In this stage, free water constantly moves from interior of fabric to the surface and the dyes migrate to the surface with water on fabric. When the drying enters into the falling drying-rate period, only the bound water remains inside of fabric, there for the diffusion of water to the surface decreases. Relation between pick-up and migration property: However, if the percentage of pick-up is lowered too much, the water retained mechanically in the fibre structure may not diffuse sufficiently throughout the interior of fabric and cause irregular distribution, thus resulting in poor appearance of dyeing. Consequently, besides adding migration inhibitor to the padding solution , it is necessary to determine the optimum condition for pick- up according to the sort of fibre. Migration inhibitors: The migration property of dyes is largely influenced by the type of migration inhibitors and by the amount applied. As common migration inhibitors, sodium alginate and synthetic thickening type
  75. agents of vinyl acetate or acrylic acid types are used. Of these migration inhibitors, synthetic thickening type agents are inferior to sodium alginate in migration inhibiting effects but, on the other hand, they generally show favorable results in appearance of dyeing because of their better adhesive effect of dyes on polyester. Sodium alginate synthetic thickening type agent Thin fabric 0.4-0.6g/l 5-10g/l Thick fabric 0.8-1.0g/l 15-20g/l Particle size of dyes:- In case of water insoluble dyes such as disperse dyes and vat dyes; the degree of migration varies according to the particle size of dye as shown in the following table, Size of dye particle Migration index(M) Without thickening agent Over 2micron Ca.1micron 0.4-0.6micron 0.1-0.3 micron 0.03-0.07 micron Under o.o3 micron 1.47 1.71 1.86 1.88 1.91 1.93 Fixation process:- The following processes are applied from fixing disperse dyes on polyester fibres, 1. Thermo-sol method 2. High pressure steaming method
  76. 3. High temperature (HT) steaming method Thermosol method:- This method , applying drying heating to fix disperse dyes on polyester fibres, is generally used for fixation in continuous dyeing of polyester /cellulosic blended fabric. High pressure steaming method:- This method applies the continuous high pressure to fix disperse dyes on to the polyester fibre. In comparison with thermo-soling method and high temperature steaming method, this method has advantages of high fixation and less staining on cellulosic fibres, but on the other hand is liable to show poor reproducibility unless water contents and pH controlled accurately. High temperature steaming method:- This method, applies super-heated steam to fix the disperse dyes on polyester fibres, is gaining popularity, especially recently, for fixation of print on polyester woven fabric. Continuous dyeing of polyester/ cellulosic fabrics with disperse dyes and vat dyes Method: - Pad-developing For continuous dyeing of polyester /cellulosic blends with disperse dyes and vat dyes. Two methods are usually adopted, One bath method Two bath method
  77. One bath method:- In one bath method, blends is padded through the solution containing disperse dyes and dispersed type vat dyes, after drying, disperse dyes are developed on polyester fibres by thermo-soling and vat dyes are developed on cellulosic fibres. Two bath process:- In two bath method, disperse dyes are first applied on polyester fibre. By thermo-sol dyeing and then vat dyes are applied on cellulosic fibres in a separate process. Procedure of disperse dyes in continuous dyeing There are so many combinations of blended fabrics. Each blended fabric has its own process to dye. Disperse dye is purely used for polyester fabric and vat for cotton. Now we will study about the process and behavior of these dyes during process. 1. Behavior of disperse dyes in padding process:- The padding process is very important in continuous dyeing. In order to obtain dyed fabrics of superior quality and good reproduce ability, it is necessary to pad dye solution evenly on fabric in padding process. To meet these requirements there are many parameters that should be taken into account. •Tailing: The phenomena called tailing will vary depending upon the kinds of fibres and substantively, particle size and disperse-ability of dyes.
  78. On the good hydrophilic fibres like cellulosic fibres, water with primarily absorbed on fibres. The concentration of padding solution increases as time elapses, and eventually reaches equilibrium at level of concentration about20% higher than that of original padding solution. In contrast on hydrophobic fibres such as polyester, the hydrophobic dyes is absorbed primarily as shown in curve [2] , the concentration of padding solution increases as time elapses , and eventually reaches equilibrium at level of concentration about 20% higher than that of original padding solution This behavior to minimize tailing in blends, though depending upon blending ratio, May distributed to the mutual reaction between the hydrophobic of cellulosic fibres, and also to use of thickening agent with a high degree of hydration as migration inhibitor in practical padding solution. •Speck:- The formation of speck during padding is largely influenced by particle of size of dyes, the compatibility of these dyes with migration inhibitors and penetrating agents etc. though depending upon the structure and density of woven fabric, the dye particle which will be larger than 3 micron causes formation of specks in case of polyester / cellulosic blended poplin fabric. If dye disperse ability caused by poor compatibility between dyes and auxiliaries remarkably deteriorates, it leads not only formation of specks on the fabric but also tailing problem. furthermore , dispersion solution are sometimes applied or stored for a longer time after preparation until padding finished, and dispersed dyes which stain the wall of pad trough are dried and then drop back into the padding solution., there disperse-ability of dyes is one of the important factor for the formation of speck on fabric. • Listing:-
  79. The phenomenon called listing refers to differences in color strength and shades on the dyed fabrics as a result of unleveled dyeing from selvedge to selvedge and from selvedge to center; the following are points reasoning the listing.  Uneven drying of fabric prepared from padding from selvedge to center and selvedge to selvedge variation.  Uneven temperature of material.  Uneven pressure of squeezing.  Uneven temperature of padding solution.  Uneven feeding of padding solution.  Difference in dye migration due to air viscosity.  Differences of temperature dependency of disperse dyes during their thermo-soling. 2-Behaviour of disperse dyes during drying: Problems during IR drying and hot flue drying include the migration of disperse dyes and the influence on the chemical structure of disperse dyes by oxidation gases. Concerning migration of dyes, this problem should be comparatively easy to solve when one dye will be used alone. There for it is important to select similar dyes inn migration properties in order to avoid listing, shade difference of between surface and backside of fabric. Regarding the chemical change caused by oxidizing gases, partially no problem ever occurs when steam or elasticity is applied. In contrast, the major problem occur when IR dryers or hot flue dryers directly heated with gas is applied. 3-Behaviour of disperse dyes during thermo-soling process:
  80. In padding of polyester /cellulosic blended fabric with disperse dye solution because of difference between hydrophobic and hydrophilic property of the blend, distribution of disperse dyes tends to be more on cellulosic fibres than on polyester fibres. To obtain good levelness and appearance of the dyed fabric, however, disperse dyes should be distributed as uniformly as possible on both polyester and cellulosic fibre in padding solution. In thermo-sol process , the disperse dye particle on both fibres are vaporized into molecular form by heating, and ,the molecular movement of polyester fibre area simultaneously stimulated by this heat, and then disperse dyes which is mean while vaporized into molecules are dissolved an exhausted into amorphous region of polyester , of which inter molecular linkage was already loosed. On the other side, disperse dyes on cellulosic fibres also vaporized and migrate onto polyester fibres, but in this case , the color yield ratio lower than that of disperse dyes on polyester fibres. Consequently , in thermo-sol dyeing of polyester /cellulose blended fabric (65/35) with disperse dyes , a fixation ratio is only 70-80% and rest of 20-30% either sublimate and diffuse into atmosphere or else remain on the cellulose fibres are also called staining on cellulose. Procedure of vat dyes in continuous dyeing The processes of vat dye in continuous dyeing show the following behaviors during dyeing process. 1-Behaviour of vat dyes in padding solution: The behavior of vat dye is similar to disperse dye. There are following precautions that should be taken into account, Precautions during padding The following precautions are necessary to get uniform padding with dye solution on blended fabrics.—disperse ability of dyes and stability
  81. of dispersion.--compatibility of dye dispersion (including compatibility of disperse dyes) Precaution during drying process: The most important point to keep mind during drying is to avoid problems such as listing, color difference from back to face, and poor surface appearance, caused by dye migration. 2-Behaviour of vat dyes during thermo-soling of process In one bath dyeing of blended fabric, disperse dyes are developed by thermo-sol treatment. In this thermo-sol process vat dyes are not chemically influenced, but a certain type of vat dye is stained polyester fibre. When the degree of staining of vat dyes on polyester fibre becomes high, dyeing strength and shade of polyester fibre portion and light fastness are liable to be influenced. This property depends upon not only the chemically constitution of vat dyes but also impurities contained in these dyes. Due to the difficulty to prevent staining on polyester by vat dyes through using auxiliary and modification of dyeing procedure. It is necessary to select vat dyes which have the least staining on polyester fibres. Furthermore staining on polyester by vat dyes in thermo-soling become higher ratio in paler shade. In contrast, the ratio of staining in deep shades, does not increase therefore it is necessary to be mined in pale dyeing. 3-Behaviour of vat dyes during in chemical padding process:- The chemical padding process in the proper application of caustics soda and hydro sulphate that are necessary for reducing dyeing of vat dyes. The proper amount of then is required depending on kinds of vat dyes and dyeing depth. When formulation of chemical solution
  82. is not properly prepared and /or temperature of it increases. The vat dyes padded on the fabric are liable to drop and thus lead to such problems as tailing and high level dyeing’s. The temperature of chemical bath should therefore be kept in around 20 0 C or preferably bellow 15 0 C. Furthermore, it is possibly dangerous that temperature of chemical solution increases by excess steam of if the chemical tank is mounted too close to the steamer. To avoid this risk, therefore, the tank should be equipped with cooling system. Beside above mentioned control of temperature of a chemical bath. Another preventive to avoid bleeding of vat dyes into a chemical bath are (a) an increase of the amount of migration inhibitors. Vat dyes are padded to minimize migration of dyes to the fabric surface and (b) not strong nip pressure during chemical padding the pick-up of chemical padding should be recommended from 15-20% more than the pick-up of padding at any rate. It is necessary that should be strength chemical solution for developing of vat dyes are padded and also that appropriate adjustment of padding solution should be made not to flow out to surface of fabric during subsequent steaming. In continuous dyeing of polyester/cellulose blends will disperse dye sand a vat dyes. 4-Behaviour of vat dyes during in steaming process: Immediately after chemical padding the fabric is padded into a steamer and steamed under saturated steam. In the steaming process the vat dyes immediately form water soluble leuco salt which has strong affinity to cellulosic fibres and then immediately dye cellulosic fibres. In case it takes longer time to introduce the fabric into a steamer of a chemical padding or if air accidently enter into a steamer ,H2S on the fabric is liable to be consumed much and normal reduction and dyeing of vat dyes cannot be obtained. In addition in case of super-heated steam in a steamer or if pick-up ratio of
  83. chemical padding is lower. The moisture retained in fabrics is liable to accurate, and reduction and dissolution of vat dyes become insufficient and result in insufficient dyeing. the most recommendable steaming time is 30-40 sec. a steaming for more than 40 sec. will cause over reduction of vat dyes, and the normal dyeing will not be obtain. A shorter steaming is also resulted in insufficient dyeing. The reduction and dyeing mechanism of vat dyes , behavior of leuco salt and kinds of vat dyes will be described in the following, 1-Basic reaction of reduction and dyeing of vat dyes are shown in the following table, Oxide leucoacid leucosalt oxide Solubility In water insoluble insoluble soluble insoluble Dye ability on cellulosic fibres non non excellent non dye ability onto polyester fibre trace trace non trace Vat dyes, in general, require a reduction potential between -650mv and -1,000mV to convert into leuco acid. To reduce all kinds of vat dyes , a reducing agent which has a reduction potential of lower than -1,000 mV is necessary . from this point of view hydro-sulphite is the most suitable reducing agent.2-Chemical change of leuco salt: As stability of leuco salt of vat dyes is poor , when application temperature amount of caustic soda and hydro-sulphite, or quality of water are improper. The following chemical change are liable to occur thus causing color change ,decreasing of color value and poor reproduce ability •Over reduction When temperature is too high or concentration of hydro-sulphite is abnormally high, over reduction is liable to occur.
  84. •Hydrolysis When temperature is too high or concentration of caustic soda is abnormally high, over reduction is liable to occur. De-halogenation When temperature is too high or concentration of caustic soda and hydro-sulphite is a normally high, de-halogenation is liable to occur. 5-Behaviour of vat dyes in oxidizing and washing process After steaming, the fabric moves into washers through a water seal, but, the temperature of water in water seal tends to increase and easily to be different in temperature distribution. As they may cause un-level dyeing, it is necessary to keep overflow in a water seal.H2O2 is the most common oxidizing agent, when potassium dichromate is applied as oxidizing agent, chrome ions are liable to be absorbed onto the fabric, and these ions cannot be eliminated completely during washing. Since soaping time in an open width washer is generally short, it is necessary to apply higher temperature as possible to eliminate impurities and dispersing agents from fabric. Continuous dyeing of polyester/cellulose blended fabrics with disperse and reactive dyes. Method: pad-dry-pad-steam One bath method Two bath method In one bath process, both disperse and reactive dyes are padded in the same bath and developed either together or separately onto the respective fibres. The former is called one bath one step dyeing method and the later is called one bath two step dyeing method.
  85. In two bath method, disperse dyes and reactive dyes are applied onto polyester fibres and cellulosic fibres respectively. 2We have studied the procedure of disperse dyes in last topic so now we will study about the procedure and behavior of reactive dyes during continuous dyeing. 1- Reactivity of reactive dyes: The reactivity of reactive dyes mainly depends upon the reactive group. For example, di-chlorotriazine dyes which exhibit high reactivity (procion MX) are said to be 1000-100000 times than that of tri-chloro pyrimidine dyes which are low reactive. Reactivity of the reactive dyes which contains the same reactive group vary depending upon the structure of dye chromophore . A -Affinity of reactive dyes Since continuous dyeing is carried out at remarkably shorter liquor ratio than exhaust dyeing, deep shades can be obtained with low affinity dyes. The simple washing can be only applied in continuous dyeing. After dyeing. B -Diffusion of reactive dyes into inside of the finer. Due to their relatively low molecular weight, reactive dyes generally show good diffusion properties. When the affinity is almost same as others, the dyes with higher diffusion show higher color yield onto fibre. One bath pad dry thermo-fix method Padding drying thermo-soling washing Disperse dyes
  86. Reactive dyes Alkali Conditions Urea 50-100g/l Migration inhibitors 0.5-1.0g/l Penetrating agent 1-3ml/l Sodium bicarbonate 10-20g/l Padding 20-25°C Pick-up 50-70% Drying 110-130°C Thermo-soling 190-220°C Time 60-120sec. Washing open width soaped Pad-steam Box Process conditions 1 cold rinsing 20-30°C with over flow 2 warm rinsing 40-50°C with over flow 3 hot rinsing 60-70°C with over flow 4 boiled rinsing 80-100°C 5, 6, 7 soaping 95°C, 1-3g/l surfactant 8 warm rinsing 50-80°C
  87. 9 cold rinsing 20-30°C with over One bath-two step pad thermo-sol alkali pad steam method Padding drying thermo-soling padding steaming washing Disperse dyes Reactive dyes Conditions Migration inhibitors 0.5-1g/l Penetrating agent 1-3ml/l Mono sodium phosphate (pH adjustment) 1g/l Padding 20-25°C Pick-up 50-70% Drying 110-130°C Thermo-soling 190-220°C Time 60-120sec. Glauber’s salt 250g/l Caustic soda 10-20ml/l Soda ash 0-20g/l Reduction inhibitors 10g/l Steaming 100-105°C
  88. Time 20-30sec. 2Washing open width soaper JET DYEING MACHINE MLR’s of Various Jet based Machines: Old Jet 1:8 Rapid Jet 1:6 Super Rapid Jet 1:4-1:5 Soft flow 1:1-1:1.5 Over flow 1:4-1:5 Air Flow 1:1 Jet Pressure: Jet pressure: 15-20 psi. Adjust jet pressure according to the quality. In case of soft flow dyeing machine pressure is very low from 3psi to 10psi. Because in this machine fabric is moved mechanically and jets are used only to penetrate the dye liquor in fibres. NECESSARY ACTION: Adjusting the jet pressure according to the quality. Recipe: No standard for recipe it is as per the quality of fabric. pH: During dyeing it is checked by pH meter or pH paper, 4.5-5.5 is the standard. NECESSARY ACTION: Adjust the concentration of acid buffer. Temperature:
  89. STANDARD: The standard is set during dyeing as per the requirement with the help of thermometer. NECESSARY ACTION: Ensure uniform heating rate as per the dyeing program. Maintain uniform steam pressure, and conform effective working of thermostat. Dyeing time: Dyeing time is kept as per the previous records in record book. Ensure desired holding time for the dyeing. Rapid jet takes 1 hour, old jet and beam take 2.5 hours, soft flow also takes 2- 2.5 hours for completion of dyeing. Vessel Pressure: During dyeing, pressure gauge reading on jet should be 25psi, for soft flow it should be 20-25 psi. So ensure optimum pressure. JIGGER DYEING MACHINE Fabric preparation: POINTS TO CHECK: Absorbency, whiteness, pH of core fabric, creases of the fabric and the selvedges. STANDARD: Uniform whiteness, Ph must be neutral, and fabric should be crease free. NECESSARY ACTION: Give two acetic acid or formic acid wash. If the absorbency is not proper then rescouring is to be done. If uniform whiteness is not there then segregate the fabric. If creases are there then pass through the stenter to remove the creases. Batching: STANDARD: Knife cut batching (very even batching). If batching is not even, then segregate the fabric or dry the fabric on the stenter.
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