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Ny spildevandsforskning: Mistrapharma Identifikation og fjernelse af miljøskadelige lægemiddelstoffer i spildevand
Disposition ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
North: 114 plants > 10.000 PE without nitrogen removal South: 100 plants > 10.000 PE with extended nutrient removal
Biological treatment at Swedish WWTPs
 
Pharmaceutical removal at WWTPs with  activated sludge and N-removal Compound  (n=X1:X2) Number of WWTPs with at least one pair of samples Number of WWTPs with at least one pair of samples and at least one influent concentration that exceeds the limit of quantification
Pharmaceutical removal at WWTPs with  activated sludge without N-removal
Pharmaceutical removal at WWTPs with  trickling filter
Activated sludge  with N-removal and without N-removal Compound  (n=X1:X2) Number of WWTPs with activated sludge and N-removal  Number of WWTPs with activated sludge without N-removal
Activated sludge with N-removal and Trickling filter
Modelstoffer ,[object Object]
Ide bag mistrapharma projektet Lægemidler som kan være miljøskadelige Alle lægemidler Sorberes  til  slam Bionedbrydes i  Rislefilter renseanlæg med  delvis nitrifikation Bionedbrydes i fuldt udbygget  Bio-de-nitro renseanlæg Fjernes med  5 g/m 3  ozon  Sorberes med 50 g/m 3  aktivt  kul pulver ©Henrik Andersen Ethinylestradiol Dichlofenak Ibuprofen
 
Identifikation af skadelige lægemidler ,[object Object]
Aktivt kul
Percentage   residual concentrations of APIs after treatment with different PAC doses. Sorption to PAC in combination with biological treatment
Behandling med aktivt kul
Ozon behandling
Ozone treatment of wastewater effluent O 3 Figure from ITT/WEDECO sales material with permission by Achim Reid
Scheme of an ozone system Figure from ITT/WEDECO sales material with permission by Achim Reid ozone generator energy (400 V) cooling water 5 - 32 °C feed gas O 3 grounded air / O 2 electrodes 5,5 kV offgas reaction tank
The ozone experiments ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Resultater med ozon
Proposed ClO 2  or PAA treatment step 2-4 g ClO 2 /m 3   ~ 0.01 – 0.03 €/m 3 Patent Application No. 08163303.4-1213
ClO 2  generator from Alldos
Results: Oxidant Fig. 2  ClO 2  concentration profile of samples before and after treatment (initial ClO 2  dose: 0.5 – 20 mg/l) Fig. 3  PAA concentration profile of samples before and after treatment (initial PAA dose: 2.5 – 50 mg/l)
Experiment A: ClO 2  reactivity of sewage
Oxidation with ClO 2 Percentage   residual concentrations of APIs in an nitrified effluent after treatment with different ClO 2  doses.
Oxidation with ClO 2 Percentage   residual concentrations of APIs in an non-nitrified effluent after treatment with different ClO 2  doses.
Experiment B: Steroid Estrogens Lundtofte effluent (medium COD) Lynetten effluent (high COD)
Konklusion
Er det noget teoretisk pjat som aldrig vil blive brugt? ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Det er for dyrt!
Running cost and benefits of treatment (Excluding investment costs) Politically feasible ? Politically feasible ? Consumers pay ~ 30 - 80 kr/m 3  for supply and disposal of water to Danish households! Pathogens and endocrine disruptors > 99 % Heavy metals ~ 0 0.25 kr/m 3 Chlorine dioxide (4 mg/L) 0.1 – 1 kr/m 3 0.12 kr/m 3   0.30 kr/m 3   5 kr/m 3 0.12 kr/m 3 0.20 kr/m 3 Cost Heavy metals and endocrine disruptors > 90 % Pathogens ~ 0 ,[object Object],[object Object],[object Object],Pathogens >> 99.9 % Endocrine disruptors > 99 % Heavy metals ~ 0 UV combined with oxidants - Ozone + UV - UV/O 3 - UV/H 2 O 2 Pathogens >> 99.9 % Heavy metals and endocrine disruptors ~ 0 % UV (traditional desinfection) Pathogens and endocrine disruptors > 99 % Heavy metals ~ 0 Ozone (8 mg/L) Effect Method Institute of Environment & Resources Technical University of Denmark

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Døgnkursus 2009 - Ny Spildevandsforskning

  • 1. Ny spildevandsforskning: Mistrapharma Identifikation og fjernelse af miljøskadelige lægemiddelstoffer i spildevand
  • 2.
  • 3. North: 114 plants > 10.000 PE without nitrogen removal South: 100 plants > 10.000 PE with extended nutrient removal
  • 4. Biological treatment at Swedish WWTPs
  • 5.  
  • 6. Pharmaceutical removal at WWTPs with activated sludge and N-removal Compound (n=X1:X2) Number of WWTPs with at least one pair of samples Number of WWTPs with at least one pair of samples and at least one influent concentration that exceeds the limit of quantification
  • 7. Pharmaceutical removal at WWTPs with activated sludge without N-removal
  • 8. Pharmaceutical removal at WWTPs with trickling filter
  • 9. Activated sludge with N-removal and without N-removal Compound (n=X1:X2) Number of WWTPs with activated sludge and N-removal Number of WWTPs with activated sludge without N-removal
  • 10. Activated sludge with N-removal and Trickling filter
  • 11.
  • 12. Ide bag mistrapharma projektet Lægemidler som kan være miljøskadelige Alle lægemidler Sorberes til slam Bionedbrydes i Rislefilter renseanlæg med delvis nitrifikation Bionedbrydes i fuldt udbygget Bio-de-nitro renseanlæg Fjernes med 5 g/m 3 ozon Sorberes med 50 g/m 3 aktivt kul pulver ©Henrik Andersen Ethinylestradiol Dichlofenak Ibuprofen
  • 13.  
  • 14.
  • 16. Percentage residual concentrations of APIs after treatment with different PAC doses. Sorption to PAC in combination with biological treatment
  • 19. Ozone treatment of wastewater effluent O 3 Figure from ITT/WEDECO sales material with permission by Achim Reid
  • 20. Scheme of an ozone system Figure from ITT/WEDECO sales material with permission by Achim Reid ozone generator energy (400 V) cooling water 5 - 32 °C feed gas O 3 grounded air / O 2 electrodes 5,5 kV offgas reaction tank
  • 21.
  • 23. Proposed ClO 2 or PAA treatment step 2-4 g ClO 2 /m 3 ~ 0.01 – 0.03 €/m 3 Patent Application No. 08163303.4-1213
  • 24. ClO 2 generator from Alldos
  • 25. Results: Oxidant Fig. 2 ClO 2 concentration profile of samples before and after treatment (initial ClO 2 dose: 0.5 – 20 mg/l) Fig. 3 PAA concentration profile of samples before and after treatment (initial PAA dose: 2.5 – 50 mg/l)
  • 26. Experiment A: ClO 2 reactivity of sewage
  • 27. Oxidation with ClO 2 Percentage residual concentrations of APIs in an nitrified effluent after treatment with different ClO 2 doses.
  • 28. Oxidation with ClO 2 Percentage residual concentrations of APIs in an non-nitrified effluent after treatment with different ClO 2 doses.
  • 29. Experiment B: Steroid Estrogens Lundtofte effluent (medium COD) Lynetten effluent (high COD)
  • 31.
  • 32. Det er for dyrt!
  • 33.

Notas do Editor

  1. 21-04-11 Identification of pharmaceuticals of environmental concern MistraPharma will contribute to identifying the active pharmaceutical ingredients on the Swedish market most likely to cause adverse effects in the aquatic environment. The programme will also generate data on which molecular structure elements that are important for biodegradability of pharmaceutical compounds. Recommendations to improve wastewater treatment technologies   MistraPharma will identify and develop wastewater treatment technologies that will help improve the elimination of high-risk pharmaceuticals from waste water treatment plants. Any recommendations to improve waste water treatment will be based on an integrated analysis taking into account what is environmentally motivated, technically feasible and economically realistic.   Improved risk identification strategies   MistraPharma will develop new tools for detecting environmental effects of human pharmaceuticals based on the compounds´ expected pharmacological mechanisms or using explorative methods covering a broad range of biological interactions. Based on these methods MistraPharma will propose new approaches to ecotoxicological testing of  pharmaceuticals. Stakeholder communication   MistraPharma will ensure that the stakeholders, such as the pharmaceutical industry, national, regional and local authorities and health care, are actively informed about and given access to the new knowledge and expertise that will enable them to limit the effects of human pharmaceuticals in the aquatic environment.
  2. 21-04-11 Identification of pharmaceuticals of environmental concern MistraPharma will contribute to identifying the active pharmaceutical ingredients on the Swedish market most likely to cause adverse effects in the aquatic environment. The programme will also generate data on which molecular structure elements that are important for biodegradability of pharmaceutical compounds. Recommendations to improve wastewater treatment technologies   MistraPharma will identify and develop wastewater treatment technologies that will help improve the elimination of high-risk pharmaceuticals from waste water treatment plants. Any recommendations to improve waste water treatment will be based on an integrated analysis taking into account what is environmentally motivated, technically feasible and economically realistic.   Improved risk identification strategies   MistraPharma will develop new tools for detecting environmental effects of human pharmaceuticals based on the compounds´ expected pharmacological mechanisms or using explorative methods covering a broad range of biological interactions. Based on these methods MistraPharma will propose new approaches to ecotoxicological testing of  pharmaceuticals. Stakeholder communication   MistraPharma will ensure that the stakeholders, such as the pharmaceutical industry, national, regional and local authorities and health care, are actively informed about and given access to the new knowledge and expertise that will enable them to limit the effects of human pharmaceuticals in the aquatic environment.
  3. 21-04-11 Identification of pharmaceuticals of environmental concern MistraPharma will contribute to identifying the active pharmaceutical ingredients on the Swedish market most likely to cause adverse effects in the aquatic environment. The programme will also generate data on which molecular structure elements that are important for biodegradability of pharmaceutical compounds. Recommendations to improve wastewater treatment technologies   MistraPharma will identify and develop wastewater treatment technologies that will help improve the elimination of high-risk pharmaceuticals from waste water treatment plants. Any recommendations to improve waste water treatment will be based on an integrated analysis taking into account what is environmentally motivated, technically feasible and economically realistic.   Improved risk identification strategies   MistraPharma will develop new tools for detecting environmental effects of human pharmaceuticals based on the compounds´ expected pharmacological mechanisms or using explorative methods covering a broad range of biological interactions. Based on these methods MistraPharma will propose new approaches to ecotoxicological testing of  pharmaceuticals. Stakeholder communication   MistraPharma will ensure that the stakeholders, such as the pharmaceutical industry, national, regional and local authorities and health care, are actively informed about and given access to the new knowledge and expertise that will enable them to limit the effects of human pharmaceuticals in the aquatic environment.
  4. 21-04-11
  5. 21-04-11
  6. EP08163303 Use of clorine dioxide for removal of estrogenic substances in wastewater .
  7. 21-04-11
  8. 21-04-11