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Definitions

  Steam economy
 Kilograms of solvent evaporated per
  kilogram of steam used
  Evaporator capacity
 Number of kilograms of water vaporized
  per hour.
 Steam Consumption
 Capacity divided by economy (steam
  used/hr)
Single Effect Evaporators
   When a single evaporator is used , the
    vapor from boiling liquid is condensed
    and discarded. This method is single effect
    evaporation

   It is simple, but use steam ineffectively i.e.
    steam economy is low, so to evaporate
    one kg of water from solution 11.3 kg
    steam is required
Cont…




        Thick Liquor



                       Condensed vapor
Where single effect are used

   Single-effect evaporators are used when the
    throughput is low
   when a cheap supply of steam is available
   when expensive materials of construction
    must be used as is the case with corrosive
    feed stocks
   when the vapor is so contaminated so that it
    cannot be reused
   For liquids that boil at high temperatures
    (high boiling-point elevation liquors)
Operation of single effect evaporator
  Single effect units may be operated in batch, semi-
  batch or continuous batch modes or continuously
  Batch Operation
 Batch units require that filling, evaporating and
  emptying are consecutive steps

   Such a method of operation is rarely used since it
    requires that the vessel is large enough to hold
    the entire charge of feed and that the heating
    element is low enough to ensure that it is not
    uncovered when the volume is reduced to that of
    the product
Cont…

  Semi-Batch Operation
 Semi-batch is the more usual mode of
  operation in which feed is added
  continuously in order to maintain a
  constant level until the entire charge
  reaches the required product density
  Continuous-Batch Operation
 Have a continuous feed and, over at least
  part of the cycle, a continuous discharge
Cont…
 often a feed drawn from a storage tank is
  returned until the entire contents of the
  tank reach the desired concentration
 The final evaporation is then achieved by
  batch operation
Continuous Evaporator
 continuous      evaporators     have    a
  continuous feed and discharge and
  concentrations of both feed and discharge
  remain constant
Multiple Effect Evaporators
  Three methods are available which enable
  the performance to be improved, either
  by direct reduction in the steam
  consumption or by improved energy
  efficiency of the whole unit
 Multiple effect operation
 Recompression of the vapor rising from
  the evaporator
 Evaporation at low temperatures using a
  heat pump cycle
Multiple Effect Operation
 If vapor generated from the first effect is
  used for heating in the 2nd effect, and then
  vapor from the 2nd effect is sent to a
  condenser, the operation becomes double
  effect. Addition effects can be added
  similarly
 Method of increasing the evaporation/kg
  of steam by using a series of evaporators
  b/w steam supply and condenser is called
  multiple-effect evaporation.
Cont…
Cont…
 First Effect, in which steam is fed and in
  which the pressure in the vapor space is
  the highest (for liquid transfer b/c no
  pump used) and in last effect it is
  minimum. Thick liquid out from last effect
  but it depends on feeding arrangement
 The boiling point in 2nd effect must be
  reduced, b/c by concentrating, solution
  B.P increases, also vapor heat content
  reduces going from first effect to 2nd. B.P.
  can be reduced by reducing pressure or
  applying vacuum.
Calculations for forward feed system
Cont…
 For three evaporators arranged as shown
  in Figure, in which the temperatures and
  pressures are T1,T2,T3, and P1, P2, P3,
  respectively, in each unit, then the heat
  transmitted per unit time across each
  effect is
Effect 1 Q1 =U1A1∆T1, ∆T1= (T0 − T1)
Effect 2 Q2 = U2A2 ∆ T2, ∆ T2=(T1 − T2)
Effect 3 Q3 = U3A3∆ T3, ∆ T3 = (T2 − T3)
T0 is steam température
Cont…

 Neglecting the heat required to heat the
  feed from Tf to T1, the heat Q1 transferred
  across where A1 appears as latent heat in the
  vapor D1 and is used as steam in the second
  effect, so
  Q1 = Q2 = Q3
  U1A1∆T1 = U2A2∆T2 = U3A3∆T3
 If, as is commonly the case, the individual
  effects are identical,
  A1 = A2 = A3, Then
 U1∆T1 = U2∆T2 = U3∆T3
Cont…
 The latent heat required to evaporate 1
  kg of water in 1, is approximately equal to
  the heat obtained in condensing 1 kg of
  steam at T0.
 Thus 1 kg of steam fed to 1 evaporates 1
  kg of water in 1. Again the 1 kg of steam
  from 1 evaporates about 1 kg of steam in
  2. Thus, in a system of N effects,1 kg of
  steam fed to the first effect will evaporate
  in all about N kg of liquid, so economy
  increase with number of effects
Cont…
 The water evaporated in each effect is
  proportional to Q, since the latent heat is
 approximately constant. Thus the total
  capacity is:
 Q = Q1 + Q2 + Q3
     = U1A1∆T1 + U1A2∆T2 + U3A3∆T3
 If an average value of the coefficients Uav
  is taken, then:
 Q = Uav(∆T1 + ∆T2 + ∆T3)A
 Q = UavA∆T
Heat Balance on Forward Feed

 Effect 1:
 D0λ0 = GFCp(T1 − Tf ) + D1λ1
 D0 is steam flow rate to 1st effect, at λ0 latent
  heat of vaporization

   Effect 2:
    D1λ1 + (GF − D1)Cp(T1 − T2) = D2λ2

   Effect 3:
    D2λ2 + (GF − D1 − D2)Cp(T2 − T3)= D3λ3
Feeding Arrangement
 Forward Feed
 Conc. of liquid increase from 1st effect to
  last effect
 Pump is required to feed dilute solution
  to 1st effect & for thick liquid in last effect
 Transfer b/w effects can be done with out
  pumps b/c its in decreasing order
Cont…

 Backward Feed
 Dilute feed is fed to last effect and
  pumped back to 1st effect
 Additional pumps b/w effects are required
  b/c flow is from low pressure to high
  pressure
 Gives higher capacity for viscous feed
 Gives low economy for cold feed
Cont…
Cont…

 Mixed Feed
 Dilute liquid enters in intermediate effect
 Flow back to first effect, where final conc.
  Is done at highest temp
 It eliminate some of the pumps required
  b/w effects
Cont…
Cont…

 Parallel Feed
 For crystallization operation, where slurry
  crystals and mother liquor is drawn,
  parallel feed arrangement is used.
 No transfer of liquid b/w effects and no
  pumps required
Cont…
Thank You
     for
Your Attention

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Evaporators

  • 1. Definitions Steam economy  Kilograms of solvent evaporated per kilogram of steam used Evaporator capacity  Number of kilograms of water vaporized per hour.  Steam Consumption  Capacity divided by economy (steam used/hr)
  • 2. Single Effect Evaporators  When a single evaporator is used , the vapor from boiling liquid is condensed and discarded. This method is single effect evaporation  It is simple, but use steam ineffectively i.e. steam economy is low, so to evaporate one kg of water from solution 11.3 kg steam is required
  • 3. Cont… Thick Liquor Condensed vapor
  • 4. Where single effect are used  Single-effect evaporators are used when the throughput is low  when a cheap supply of steam is available  when expensive materials of construction must be used as is the case with corrosive feed stocks  when the vapor is so contaminated so that it cannot be reused  For liquids that boil at high temperatures (high boiling-point elevation liquors)
  • 5. Operation of single effect evaporator Single effect units may be operated in batch, semi- batch or continuous batch modes or continuously Batch Operation  Batch units require that filling, evaporating and emptying are consecutive steps  Such a method of operation is rarely used since it requires that the vessel is large enough to hold the entire charge of feed and that the heating element is low enough to ensure that it is not uncovered when the volume is reduced to that of the product
  • 6. Cont… Semi-Batch Operation  Semi-batch is the more usual mode of operation in which feed is added continuously in order to maintain a constant level until the entire charge reaches the required product density Continuous-Batch Operation  Have a continuous feed and, over at least part of the cycle, a continuous discharge
  • 7. Cont…  often a feed drawn from a storage tank is returned until the entire contents of the tank reach the desired concentration  The final evaporation is then achieved by batch operation Continuous Evaporator  continuous evaporators have a continuous feed and discharge and concentrations of both feed and discharge remain constant
  • 8. Multiple Effect Evaporators Three methods are available which enable the performance to be improved, either by direct reduction in the steam consumption or by improved energy efficiency of the whole unit  Multiple effect operation  Recompression of the vapor rising from the evaporator  Evaporation at low temperatures using a heat pump cycle
  • 9. Multiple Effect Operation  If vapor generated from the first effect is used for heating in the 2nd effect, and then vapor from the 2nd effect is sent to a condenser, the operation becomes double effect. Addition effects can be added similarly  Method of increasing the evaporation/kg of steam by using a series of evaporators b/w steam supply and condenser is called multiple-effect evaporation.
  • 11. Cont…  First Effect, in which steam is fed and in which the pressure in the vapor space is the highest (for liquid transfer b/c no pump used) and in last effect it is minimum. Thick liquid out from last effect but it depends on feeding arrangement  The boiling point in 2nd effect must be reduced, b/c by concentrating, solution B.P increases, also vapor heat content reduces going from first effect to 2nd. B.P. can be reduced by reducing pressure or applying vacuum.
  • 13. Cont…  For three evaporators arranged as shown in Figure, in which the temperatures and pressures are T1,T2,T3, and P1, P2, P3, respectively, in each unit, then the heat transmitted per unit time across each effect is Effect 1 Q1 =U1A1∆T1, ∆T1= (T0 − T1) Effect 2 Q2 = U2A2 ∆ T2, ∆ T2=(T1 − T2) Effect 3 Q3 = U3A3∆ T3, ∆ T3 = (T2 − T3) T0 is steam température
  • 14. Cont…  Neglecting the heat required to heat the feed from Tf to T1, the heat Q1 transferred across where A1 appears as latent heat in the vapor D1 and is used as steam in the second effect, so Q1 = Q2 = Q3 U1A1∆T1 = U2A2∆T2 = U3A3∆T3  If, as is commonly the case, the individual effects are identical, A1 = A2 = A3, Then U1∆T1 = U2∆T2 = U3∆T3
  • 15. Cont…  The latent heat required to evaporate 1 kg of water in 1, is approximately equal to the heat obtained in condensing 1 kg of steam at T0.  Thus 1 kg of steam fed to 1 evaporates 1 kg of water in 1. Again the 1 kg of steam from 1 evaporates about 1 kg of steam in 2. Thus, in a system of N effects,1 kg of steam fed to the first effect will evaporate in all about N kg of liquid, so economy increase with number of effects
  • 16. Cont…  The water evaporated in each effect is proportional to Q, since the latent heat is approximately constant. Thus the total capacity is: Q = Q1 + Q2 + Q3 = U1A1∆T1 + U1A2∆T2 + U3A3∆T3  If an average value of the coefficients Uav is taken, then: Q = Uav(∆T1 + ∆T2 + ∆T3)A Q = UavA∆T
  • 17. Heat Balance on Forward Feed  Effect 1: D0λ0 = GFCp(T1 − Tf ) + D1λ1  D0 is steam flow rate to 1st effect, at λ0 latent heat of vaporization  Effect 2: D1λ1 + (GF − D1)Cp(T1 − T2) = D2λ2  Effect 3: D2λ2 + (GF − D1 − D2)Cp(T2 − T3)= D3λ3
  • 18. Feeding Arrangement  Forward Feed  Conc. of liquid increase from 1st effect to last effect  Pump is required to feed dilute solution to 1st effect & for thick liquid in last effect  Transfer b/w effects can be done with out pumps b/c its in decreasing order
  • 19.
  • 20. Cont…  Backward Feed  Dilute feed is fed to last effect and pumped back to 1st effect  Additional pumps b/w effects are required b/c flow is from low pressure to high pressure  Gives higher capacity for viscous feed  Gives low economy for cold feed
  • 22. Cont…  Mixed Feed  Dilute liquid enters in intermediate effect  Flow back to first effect, where final conc. Is done at highest temp  It eliminate some of the pumps required b/w effects
  • 24. Cont…  Parallel Feed  For crystallization operation, where slurry crystals and mother liquor is drawn, parallel feed arrangement is used.  No transfer of liquid b/w effects and no pumps required
  • 26. Thank You for Your Attention