Distillation is the process of separating two miscible liquids by using differences in their boiling points. There are two main methods of distillation used to separate alcohol from water after fermentation - pot still distillation and patent/Coffey/continuous still distillation. Pot still distillation uses a copper pot and produces spirit in three parts (head, heart, tail) with the heart being collected for a second distillation. The patent/Coffey/continuous still, patented by Aneas Coffey in 1830, allows for continuous distillation in a single operation.
3. DistillationDistillation
โข Distillation is the process of separation of
two miscible liquids by using difference in
their boiling point. In present context the
alcohol has to be separated from water
after fermentation.
โข The evaporating temp. of ethyl alcohol is
78.5C where as for water is 100C.
4. Method of DistillationMethod of Distillation
โข Traditionally there are two method of
distillation.
โข Pot still
โข Patent still/ Coffey still/ Continuous still.
5. Pot still DistillationPot still Distillation
โข The pot is made from Copper
โข Size differ from place to place
โข Alcohol vaporize at 78.5 c
โข The Vapours passes through Condenser and
converted to liquid
โข Liquid alcohol is collected into three parts
Head
Heart ( 30% Alcohol remaining water)
Tail
โข
6. Cont..Cont..
โข The head & tail is collected in a separate vessel.
โข The head contains a lot of methyl alcohol & not
suitable for consumption.
โข The head & tail are put back for re distillation
with a fresh batch of alcohol water mixture.
โข The heart will be taken for a second distillation.
The will also produce the same
Head
Heart ( 70% alcohol remaining water)
Tail
7. Cont..Cont..
โข The spirit produced by this method
contains lot of congener element, which
contributes to flavour & body of spirit.
โข Spirit, which produced, is Scotch malt
whisky, Cognac, Dutch gin, Dark Rum,
Tequila & some Polish vodka.
12. Patent Still/Coffey/ContinousPatent Still/Coffey/Continous
โข This is also known as Coffey still because
Mr. Aneas Coffey patented it in 1830.
โข Aneas Coffey patented an improvement
on an already existing model of which was
developed by Robert Stein.
โข This is also known as a continuous still
because the entire process of distillation
gets completed in one continuous
operation.