ICWES15 - Reclamation of Oilfield Produced Water using Hydrophilic Pervaporative Membrane. Presented by May N Sule, Imperial College, London, United Kingdom

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Reclamation of Oilfield Produced Water using a Hydrophilic Pervaporative Membrane May Sule (PhD Candidate)*, Dr Michael R. Templeton (Supervisor) Department of Civil and Environmental Engineering, Imperial College London m.sule08@imperial.ac.uk

Project Aims ,[object Object],[object Object]

Why oilfield produced water? ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],http://www.amcol.com/ http://www.jccp.or.jp/english/ ;

Current treatment methods ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],http://www.unep.org/conflictsanddisasters/ ; www.veoliawaterst.com

What is Pervaporation? Membrane Evaporation Permeate vapour Feed liquid Dissolution δ Diffusion

Pervaporation theory ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Ref: Mullerplathe, 1994 Schematic representation of penetration of solvent molecules in the polymer matrix

Physical properties of solvents at 25 o C Ref: Haxo and Lahey, 1988, Peng et al., 2003, Islam and Rowe, 2009 Material Molecular weight (g/mol) Solubility in water (mg/L) Molar volume (cm 3 /G.Mole) Water Benzene Toluene Ethylbenzene o-Xylene m-Xylene p-Xylene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethylene 18 78.11 92.13 106.17 106.17 106.17 106.17 133 133 132 1,780 515 152 175 196 190 1,320 1,318 1,100 18 89.11 106.847 123.064 121.193 123.456 123.919 99.2 92.4 90.4

H-bonding, polar and dispersion coefficients ,[object Object],[object Object],Ref: Shao and Huang, 2007 Hansen solubility parameters HSP δ 2 = (δ D ) 2 + (δ P ) 2 + (δ H ) 2

Current study ,[object Object],[object Object],[object Object],Illustration : Lindsay Todman

Methodology immersion/sorption tests (bottle tests) permeation/diffusion tests

Initial Results ,[object Object],Ave water uptake= 4.51 x 10 -4 m 3 /m 2 /d Diffusion coefficient = 3.3 x 10 -3 m 2 /d =

Initial Results Volume sorbed using NaCl Volume sorbed using humic acid solution

Initial Results Volume sorbed using MgCl 2 Volume sorbed using NaCl

Current / Future work ,[object Object],[object Object],[object Object],[object Object]

References ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]

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ICWES15 - Reclamation of Oilfield Produced Water using Hydrophilic Pervaporative Membrane. Presented by May N Sule, Imperial College, London, United Kingdom

1. Reclamation of Oilfield Produced Water using a Hydrophilic Pervaporative Membrane May Sule (PhD Candidate)*, Dr Michael R. Templeton (Supervisor) Department of Civil and Environmental Engineering, Imperial College London m.sule08@imperial.ac.uk

5. What is Pervaporation? Membrane Evaporation Permeate vapour Feed liquid Dissolution δ Diffusion

7. Pervaporation theory

8. Physical properties of solvents at 25 o C Ref: Haxo and Lahey, 1988, Peng et al., 2003, Islam and Rowe, 2009 Material Molecular weight (g/mol) Solubility in water (mg/L) Molar volume (cm 3 /G.Mole) Water Benzene Toluene Ethylbenzene o-Xylene m-Xylene p-Xylene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethylene 18 78.11 92.13 106.17 106.17 106.17 106.17 133 133 132 1,780 515 152 175 196 190 1,320 1,318 1,100 18 89.11 106.847 123.064 121.193 123.456 123.919 99.2 92.4 90.4

10.

11. Methodology immersion/sorption tests (bottle tests) permeation/diffusion tests

12.

13. Initial Results Volume sorbed using NaCl Volume sorbed using humic acid solution

14. Initial Results Volume sorbed using MgCl 2 Volume sorbed using NaCl

15.

16.

17. Questions???

ICWES15 - Reclamation of Oilfield Produced Water using Hydrophilic Pervaporative Membrane. Presented by May N Sule, Imperial College, London, United Kingdom

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ICWES15 - Reclamation of Oilfield Produced Water using Hydrophilic Pervaporative Membrane. Presented by May N Sule, Imperial College, London, United Kingdom