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Senior/Graduate
                                     HMA Course




  Quality Control / Quality Assurance

        Obtaining a representative sample




Construction    QC/QA Representative Samples
                                        1
Sample Size

•   Mixture Component Variability
•   Confidence Level
•   Error or Bias From True Value
•   Effect on Performance




Construction     QC/QA Representative Samples
                                         2
Frequency of Sampling/Testing

•    Mixture Production Variability
•    Effect on Performance
•    Previous History
•    Compliance With Specifications



Construction    QC/QA Representative Samples
                                        3
SAMPLING
• Preliminary Investigation of the Potential
  Source
• Control of Product at the Source of Supply
• Control of Operations at the Site of Use
• Acceptance or Rejection of Material




  Construction    QC/QA Representative Samples
                                          4
SIZE AND NUMBER OF
                 SAMPLES
D 3665 Random Sampling of Construction
     Materials

E 105   Probability Sampling of Materials

E 122 Choice of Sample Size to Estimate the Average
Quality of a Lot or Process

E 141 Acceptance of Evidence Based on the Result of
Probability of Sampling


 Construction    QC/QA Representative Samples
                                         5
SAMPLE SIZE
  Nominal
Maximum Size                 Minimum Mass, lbs.

      No. 8                          4
      No. 4                          4
      3/8                            8
      1/2                           12
      3/4                           16
      1                             20



 Construction   QC/QA Representative Samples
                                        6
Types of samples to be taken

         • Aggregate

         • Asphalt binder

         • HMA mixture




Construction   QC/QA Representative Samples
                                       7
Sampling at
           Point of Shipment Delivery
• By bleeder valve or tap in transfer line or at back of truck
   – During unloading, center 1/3 of load



Safety equipment
    is a must




  Construction       QC/QA Representative Samples
                                             8
Sampling Truck

        • Draw and discard at least a gallon of
          binder to clear line




Construction     QC/QA Representative Samples
                                         9
Sampling Truck

 • Immediately take at least a quart sample




Construction    QC/QA Representative Samples
                                        10
Protection and Preservation
  • Take care not to contaminate containers
  • Fill and immediately seal
     – Don’t immerse in solvent




Construction    QC/QA Representative Samples
                                        11
Protection and Preservation

• Store so that emulsions are protected from freezing
• Avoid transferring from one container to another
• Retain samples not tested (point of delivery)
• Take precautions to avoid contamination during
  sampling, handling, shipping and storage




    Construction    QC/QA Representative Samples
                                            12
Sampling at Plant Tank
• Same sampling directions apply to sampling the plant tank




  Construction     QC/QA Representative Samples
                                           13
Sampling Bituminous Paving Mixtures


• Accurate test results depend upon a uniform,
  representative sample being collected.




Construction   QC/QA Representative Samples
                                       14
Sample Location

• At the plant
  – From the truck – most common
  – From plant discharge
  – From cold feed (gradation only)
• At the roadway
  – Behind the paver (11 states)
  – From the windrow


Construction      QC/QA Representative Samples
                                          15
Which is the best
          location?

                  WHY?

Construction   QC/QA Representative Samples
                                       16
Truck sampling




Construction   QC/QA Representative Samples
                                       17
Loose HMA
               RTSD




Construction    QC/QA Representative Samples
                                        18
Construction   QC/QA Representative Samples
                                       19
Sampling – Roadway

     • Approximately equal increments
     • Make vertical face with shovel
        
          750 mm (30 in.) parallel to centerline
     • Pull material back 300 mm (12 in.)




Construction      QC/QA Representative Samples
                                          20
Sampling – Roadway
          (continued)
     • Place scoop on pavement next to vertical face
       and fill scoop
         Obtain material to full depth


     • Close lid and remove scoop when full
     • Repeat to obtain required sample size




Construction     QC/QA Representative Samples
                                         21
Sampling from the roadway




Construction   QC/QA Representative Samples
                                       22
Sampling – Paver
    • Obtain samples at end of auger using
      square shovel
    • Place shovel in front of auger extension
      with blade flat on surface
    • Allow front face of auger stream to cover
      shovel




Construction     QC/QA Representative Samples
                                         23
Sampling – Paver
                 (continued)

 • Remove shovel before auger reaches it
    Lift shovel vertically


 • Repeat until sample size reached




Construction     QC/QA Representative Samples
                                         24
Sampling from Paver




WHAT ARE THE
 PROBLEMS
 WITH THIS?


Construction   QC/QA Representative Samples
                                       25
“Sampling The Windrow”




     Solution
Construction    QC/QA Representative Samples
                                        26
Sampling Loose HMA?




          See any problems with this?

Construction    QC/QA Representative Samples
                                        27
Effect of Sampling Location on
                               Gradation Variability
Standard Deviations




                      6                                                   Coldfeeds (n=45)
                      5                                                   Loose HMA (n=45)
                      4                                                   Cores (n=46)
                      3
                      2
                      1
                      0
                                                #4

                                                      #8

                                                           #16

                                                                  #30

                                                                        #50

                                                                              #100

                                                                                     #200
                           3/4"

                                  1/2"

                                         3/8"




                                                     Sieve Size

           Construction                     QC/QA Representative Samples
                                                                    28
Sample Splitting




Construction    QC/QA Representative Samples
                                        29
Sample Splitting




Construction    QC/QA Representative Samples
                                        30
Segregated Samples from the
             Same Mix




      Coarse Portion             Fine Portion
  3.79% Asphalt Binder       5.21% Asphalt Binder
Construction     QC/QA Representative Samples
                                         31
Questions?




Construction   QC/QA Representative Samples
                                       32

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Block 24 Obtaining Samples 13

  • 1. Senior/Graduate HMA Course Quality Control / Quality Assurance Obtaining a representative sample Construction QC/QA Representative Samples 1
  • 2. Sample Size • Mixture Component Variability • Confidence Level • Error or Bias From True Value • Effect on Performance Construction QC/QA Representative Samples 2
  • 3. Frequency of Sampling/Testing • Mixture Production Variability • Effect on Performance • Previous History • Compliance With Specifications Construction QC/QA Representative Samples 3
  • 4. SAMPLING • Preliminary Investigation of the Potential Source • Control of Product at the Source of Supply • Control of Operations at the Site of Use • Acceptance or Rejection of Material Construction QC/QA Representative Samples 4
  • 5. SIZE AND NUMBER OF SAMPLES D 3665 Random Sampling of Construction Materials E 105 Probability Sampling of Materials E 122 Choice of Sample Size to Estimate the Average Quality of a Lot or Process E 141 Acceptance of Evidence Based on the Result of Probability of Sampling Construction QC/QA Representative Samples 5
  • 6. SAMPLE SIZE Nominal Maximum Size Minimum Mass, lbs. No. 8 4 No. 4 4 3/8 8 1/2 12 3/4 16 1 20 Construction QC/QA Representative Samples 6
  • 7. Types of samples to be taken • Aggregate • Asphalt binder • HMA mixture Construction QC/QA Representative Samples 7
  • 8. Sampling at Point of Shipment Delivery • By bleeder valve or tap in transfer line or at back of truck – During unloading, center 1/3 of load Safety equipment is a must Construction QC/QA Representative Samples 8
  • 9. Sampling Truck • Draw and discard at least a gallon of binder to clear line Construction QC/QA Representative Samples 9
  • 10. Sampling Truck • Immediately take at least a quart sample Construction QC/QA Representative Samples 10
  • 11. Protection and Preservation • Take care not to contaminate containers • Fill and immediately seal – Don’t immerse in solvent Construction QC/QA Representative Samples 11
  • 12. Protection and Preservation • Store so that emulsions are protected from freezing • Avoid transferring from one container to another • Retain samples not tested (point of delivery) • Take precautions to avoid contamination during sampling, handling, shipping and storage Construction QC/QA Representative Samples 12
  • 13. Sampling at Plant Tank • Same sampling directions apply to sampling the plant tank Construction QC/QA Representative Samples 13
  • 14. Sampling Bituminous Paving Mixtures • Accurate test results depend upon a uniform, representative sample being collected. Construction QC/QA Representative Samples 14
  • 15. Sample Location • At the plant – From the truck – most common – From plant discharge – From cold feed (gradation only) • At the roadway – Behind the paver (11 states) – From the windrow Construction QC/QA Representative Samples 15
  • 16. Which is the best location? WHY? Construction QC/QA Representative Samples 16
  • 17. Truck sampling Construction QC/QA Representative Samples 17
  • 18. Loose HMA RTSD Construction QC/QA Representative Samples 18
  • 19. Construction QC/QA Representative Samples 19
  • 20. Sampling – Roadway • Approximately equal increments • Make vertical face with shovel  750 mm (30 in.) parallel to centerline • Pull material back 300 mm (12 in.) Construction QC/QA Representative Samples 20
  • 21. Sampling – Roadway (continued) • Place scoop on pavement next to vertical face and fill scoop  Obtain material to full depth • Close lid and remove scoop when full • Repeat to obtain required sample size Construction QC/QA Representative Samples 21
  • 22. Sampling from the roadway Construction QC/QA Representative Samples 22
  • 23. Sampling – Paver • Obtain samples at end of auger using square shovel • Place shovel in front of auger extension with blade flat on surface • Allow front face of auger stream to cover shovel Construction QC/QA Representative Samples 23
  • 24. Sampling – Paver (continued) • Remove shovel before auger reaches it  Lift shovel vertically • Repeat until sample size reached Construction QC/QA Representative Samples 24
  • 25. Sampling from Paver WHAT ARE THE PROBLEMS WITH THIS? Construction QC/QA Representative Samples 25
  • 26. “Sampling The Windrow” Solution Construction QC/QA Representative Samples 26
  • 27. Sampling Loose HMA? See any problems with this? Construction QC/QA Representative Samples 27
  • 28. Effect of Sampling Location on Gradation Variability Standard Deviations 6 Coldfeeds (n=45) 5 Loose HMA (n=45) 4 Cores (n=46) 3 2 1 0 #4 #8 #16 #30 #50 #100 #200 3/4" 1/2" 3/8" Sieve Size Construction QC/QA Representative Samples 28
  • 29. Sample Splitting Construction QC/QA Representative Samples 29
  • 30. Sample Splitting Construction QC/QA Representative Samples 30
  • 31. Segregated Samples from the Same Mix Coarse Portion Fine Portion 3.79% Asphalt Binder 5.21% Asphalt Binder Construction QC/QA Representative Samples 31
  • 32. Questions? Construction QC/QA Representative Samples 32

Notas do Editor

  1. All statistically-oriented specifications must address the sample size and frequency of sampling clearly in order to determine compliance with the specifications. First, Sample Size: 1. The size of the sample depends on the variability of the population or lot. The greater the variability, the larger the sample size. 2. The higher the desired level of confidence, the larger the required sample size. 3. The smaller the error that can be tolerated, the larger the required sample size. 4. The size of the sample also depends on how important the material property being tested affects overall performance. The more important or critical the property, the larger the sample size.
  2. Second, the Frequency of Sampling: 1.Materials that are highly variable should be sampled more frequently. Critical materials or materials properties that have a significant effect on performance should be sampled more frequently Materials or production procedures that do not have previous experience, should be sampled more frequently. When results and/or inspection suggest non-compliance with specifications, the sampling frequency should be increased.
  3. Remember, sampling and testing programs are intended to provide an overall estimate of quality. They are not intended to replace proper inspection of materials and workmanship to identify mistakes.
  4. Guides that can be used for selecting the size and number of samples are given. AASHTO R9 is also a general guide.
  5. The size of field samples is determined by the requirements of the test procedure and the nominal maximum size of the aggregate in the mixture.
  6. Always sample the center of the load. Note the sample spigot is located in the center of the back of this truck. Asphalt binders are shipped HOT. Personal safety protection equipment such as face and eye shields, long sleeves, and gloves are a must.
  7. Always draw and discard at least 1 gallon of asphalt binder before taking the sample to be either retained or tested. This prevents the possibility of contamination and old material in the line from being sampled rather than the fresh shipment.
  8. Once the line has been flushed, take at least a quart sample.
  9. Immediately cover and seal the containers. Note that the cans are not completely filled.
  10. Once the samples are covered, make sure that they are stored so that they are protected from freezing. This is especially important if the sample is an emulsion which is a water-based product. Avoid pouring from one container to another. This is to minimize the potential for contamination.
  11. The plant tank can be sampled using the preceding directions for discarding, sampling, sealing, labeling, and storing.
  12. Mix that is obtained by this method is used to determine the asphalt binder content, density, and aggregate gradation for a given lot of mix. All of these tests are used to adjust the contractor’s pay based on how close the results are to the specified values. In order to obtain accurate results, it is very important to obtain a representative sample to test.
  13. If you are taking a sample from the roadway – it is essential that the entire lift be sampled. The steps outlined above can be used.
  14. Also samples can be taken directly from the paver.
  15. Sampling location must be considered when specification writing! Sample the MAT